WO2007030254A3 - Methods of producing tungsten nanoparticles - Google Patents

Methods of producing tungsten nanoparticles Download PDF

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Publication number
WO2007030254A3
WO2007030254A3 PCT/US2006/031098 US2006031098W WO2007030254A3 WO 2007030254 A3 WO2007030254 A3 WO 2007030254A3 US 2006031098 W US2006031098 W US 2006031098W WO 2007030254 A3 WO2007030254 A3 WO 2007030254A3
Authority
WO
WIPO (PCT)
Prior art keywords
methods
nanoparticles
producing tungsten
tungsten nanoparticles
tungsten
Prior art date
Application number
PCT/US2006/031098
Other languages
French (fr)
Other versions
WO2007030254A2 (en
Inventor
Liufeng Xiong
Ting He
Original Assignee
Honda Motor Co Ltd
Liufeng Xiong
Ting He
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Honda Motor Co Ltd, Liufeng Xiong, Ting He filed Critical Honda Motor Co Ltd
Priority to JP2008529996A priority Critical patent/JP5368094B2/en
Publication of WO2007030254A2 publication Critical patent/WO2007030254A2/en
Publication of WO2007030254A3 publication Critical patent/WO2007030254A3/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G41/00Compounds of tungsten
    • C01G41/02Oxides; Hydroxides
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05Metallic powder characterised by the size or surface area of the particles
    • B22F1/054Nanosized particles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/16Making metallic powder or suspensions thereof using chemical processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/16Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/20Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from solid metal compounds
    • B22F9/22Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from solid metal compounds using gaseous reductors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2999/00Aspects linked to processes or compositions used in powder metallurgy
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/31504Composite [nonstructural laminate]
    • Y10T428/31855Of addition polymer from unsaturated monomers
    • Y10T428/31859Next to an aldehyde or ketone condensation product
    • Y10T428/31877Phenol-aldehyde

Abstract

The present teachings are directed methods of producing tungsten-containing nanoparticles, specifically tungsten nanoparticles and tungsten oxide nanoparticles with an average particle size of less than about five nanometers.
PCT/US2006/031098 2005-09-09 2006-08-09 Methods of producing tungsten nanoparticles WO2007030254A2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2008529996A JP5368094B2 (en) 2005-09-09 2006-08-09 Method for producing tungsten nanoparticles

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US11/221,779 2005-09-09
US11/221,779 US8173166B2 (en) 2005-09-09 2005-09-09 Methods of producing tungsten nanoparticles

Publications (2)

Publication Number Publication Date
WO2007030254A2 WO2007030254A2 (en) 2007-03-15
WO2007030254A3 true WO2007030254A3 (en) 2008-01-17

Family

ID=37836324

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2006/031098 WO2007030254A2 (en) 2005-09-09 2006-08-09 Methods of producing tungsten nanoparticles

Country Status (3)

Country Link
US (1) US8173166B2 (en)
JP (1) JP5368094B2 (en)
WO (1) WO2007030254A2 (en)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102006025770A1 (en) * 2006-05-31 2007-12-13 Jürgen Dr. Dornseiffer Production of coating solutions together with manufactured products
WO2009102429A2 (en) * 2008-02-11 2009-08-20 University Of North Dakota Method for producing nanoparticles of a selected size
US20100175984A1 (en) * 2009-01-15 2010-07-15 General Electric Company Method for making nanoparticles
DE102009060835A1 (en) * 2009-12-29 2011-06-30 Leibniz-Institut für Neue Materialien gem. GmbH, 66123 Synthesis of nanoparticles using ionic liquids
US8372177B1 (en) * 2010-05-05 2013-02-12 Sandia Corporation Method of synthesizing tungsten nanoparticles
CN102963935A (en) * 2012-11-13 2013-03-13 江西稀有金属钨业控股集团有限公司 Method for preparing ultrafine tungsten trioxide
CN103302300B (en) * 2013-06-24 2015-08-19 朱兰英 A kind of preparation method of tungsten nanometer powder
JP6811515B2 (en) * 2017-03-28 2021-01-13 日本新金属株式会社 Manufacturing method of fine tungsten powder
US11008220B2 (en) 2017-08-21 2021-05-18 University Of Science And Technology Of China Photochromic nanomaterial capable of blocking ultraviolet rays, production method and use thereof
CN107684917A (en) * 2017-09-05 2018-02-13 广西科技师范学院 A kind of Mn1Cd3S4The preparation method of photochemical catalyst

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0800883A2 (en) * 1996-04-12 1997-10-15 Rutgers, The State University Of New Jersey Method for producing amorphous based metals
US5770172A (en) * 1992-01-15 1998-06-23 Battelle Memorial Institute Process of forming compounds using reverse micelle or reverse microemulsion systems
US20020034675A1 (en) * 2000-07-29 2002-03-21 Karl-Anton Starz Noble metal nanoparticles, a process for preparing these and their use
WO2005051435A2 (en) * 2003-11-28 2005-06-09 Amersham Health As Tungsten particles as x-ray contrast agents

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4672090A (en) * 1984-04-04 1987-06-09 Calgon Corporation Surfactant system for emulsion polymers
US4758534A (en) * 1985-11-13 1988-07-19 Bell Communications Research, Inc. Process for producing porous refractory metal layers embedded in semiconductor devices
JPH0437610A (en) * 1990-05-30 1992-02-07 Ricoh Co Ltd Hyperfine tungsten oxide particles
US5149596A (en) * 1990-10-05 1992-09-22 The United States Of America As Represented By The United States Department Of Energy Vapor deposition of thin films
US5897945A (en) * 1996-02-26 1999-04-27 President And Fellows Of Harvard College Metal oxide nanorods
US5772978A (en) * 1996-04-24 1998-06-30 Minnesota Mining And Manufacturing Company Process for producing tungsten oxide
US6855749B1 (en) * 1996-09-03 2005-02-15 Nanoproducts Corporation Polymer nanocomposite implants with enhanced transparency and mechanical properties for administration within humans or animals
US6162530A (en) * 1996-11-18 2000-12-19 University Of Connecticut Nanostructured oxides and hydroxides and methods of synthesis therefor
US6413489B1 (en) * 1997-04-15 2002-07-02 Massachusetts Institute Of Technology Synthesis of nanometer-sized particles by reverse micelle mediated techniques
EP1167462B1 (en) * 1999-01-11 2010-12-22 Showa Denko K.K. Cosmetic preparation, surface-hydrophobized silica-coated metal oxide particles, sol of surface-hydrophobized silica-coated metal oxide, and processes for producing these
US6290859B1 (en) * 1999-11-12 2001-09-18 Sandia Corporation Tungsten coating for improved wear resistance and reliability of microelectromechanical devices
US20020009411A1 (en) * 2000-02-08 2002-01-24 Zucker Gordon L. Method for producing tungsten carbide
US6827796B2 (en) * 2000-11-02 2004-12-07 Composite Tool Company, Inc. High strength alloys and methods for making same
US6502991B2 (en) * 2001-03-14 2003-01-07 The Timken Company Rotary fluid bearing coatings and coining and processes for manufacturing the same
US20030113447A1 (en) * 2001-12-13 2003-06-19 Sherwood Walter J. Process and compositions for making ceramic articles
KR100985677B1 (en) * 2002-04-25 2010-10-05 제너럴 일렉트릭 캄파니 Preparation of nanosized copperi compounds
US7708974B2 (en) * 2002-12-10 2010-05-04 Ppg Industries Ohio, Inc. Tungsten comprising nanomaterials and related nanotechnology
JP4812233B2 (en) * 2003-02-28 2011-11-09 トヨタ自動車株式会社 Method for producing composite oxide
JP2005111336A (en) * 2003-10-06 2005-04-28 Nissan Motor Co Ltd Heat-resistant catalyst and manufacturing method therefor
US7455886B2 (en) * 2005-08-22 2008-11-25 Eastman Kodak Company Nanocomposite materials and an in-situ method of making such materials

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5770172A (en) * 1992-01-15 1998-06-23 Battelle Memorial Institute Process of forming compounds using reverse micelle or reverse microemulsion systems
EP0800883A2 (en) * 1996-04-12 1997-10-15 Rutgers, The State University Of New Jersey Method for producing amorphous based metals
US20020034675A1 (en) * 2000-07-29 2002-03-21 Karl-Anton Starz Noble metal nanoparticles, a process for preparing these and their use
WO2005051435A2 (en) * 2003-11-28 2005-06-09 Amersham Health As Tungsten particles as x-ray contrast agents

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
TAKAYUKI HIRAI, HIROSHI SATO AND ISAO KOMASAWA: "Mechanism of Formation of Titanium Dioxide Ultrafine Particles in Reverse Micelles by Hydrolisys of Titanium Tetrabutoxide", IND. ENG. CHEM. RES., vol. 32, 1993, pages 3014 - 3019, XP002442200 *
ZHIXIANG LU, SOFIAN M. KANAN AND CARL P. TRIPP: "Synthesis of high surface area monoclinic WO3 particles using organic ligands and emulsion based methods", J. MATER. CHEM., vol. 12, 25 February 2002 (2002-02-25), pages 983 - 989, XP002442199 *

Also Published As

Publication number Publication date
US20070059544A1 (en) 2007-03-15
JP5368094B2 (en) 2013-12-18
WO2007030254A2 (en) 2007-03-15
JP2009508001A (en) 2009-02-26
US8173166B2 (en) 2012-05-08

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