WO2006101666A3 - Pure particle generator - Google Patents

Pure particle generator Download PDF

Info

Publication number
WO2006101666A3
WO2006101666A3 PCT/US2006/006582 US2006006582W WO2006101666A3 WO 2006101666 A3 WO2006101666 A3 WO 2006101666A3 US 2006006582 W US2006006582 W US 2006006582W WO 2006101666 A3 WO2006101666 A3 WO 2006101666A3
Authority
WO
WIPO (PCT)
Prior art keywords
dilution
particles
particle generator
dilution system
generate
Prior art date
Application number
PCT/US2006/006582
Other languages
French (fr)
Other versions
WO2006101666A2 (en
Inventor
Qiang Wei
Original Assignee
Horiba Instr Inc
Qiang Wei
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Horiba Instr Inc, Qiang Wei filed Critical Horiba Instr Inc
Priority to CN2006800081996A priority Critical patent/CN101500734B/en
Priority to EP06736013A priority patent/EP1861216A4/en
Priority to JP2008501895A priority patent/JP2008532761A/en
Priority to KR1020077022111A priority patent/KR101154086B1/en
Publication of WO2006101666A2 publication Critical patent/WO2006101666A2/en
Publication of WO2006101666A3 publication Critical patent/WO2006101666A3/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/02—Making metallic powder or suspensions thereof using physical processes
    • B22F9/06—Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/005—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out at high temperatures in the presence of a molten material

Abstract

A particle generator is able to generate pure particles for solid or liquid materials with melting points over several hundred degrees Celsius. The material is heated to generate the vapor in a small chamber. Heated nitrogen or some inert gas is used as the carry gas to bring the mixture into a dilution system. As the super saturation ratio of the material is large enough and over a critical value, particles are formed in the dilution system by homogenous nucleation, and grown in the same dilution system as well. The different size distributions and concentrations of the particles can be obtained by varying dilution parameters, such as residence time and dilution ratio.
PCT/US2006/006582 2005-03-16 2006-02-22 Pure particle generator WO2006101666A2 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN2006800081996A CN101500734B (en) 2005-03-16 2006-02-22 pure particle generator
EP06736013A EP1861216A4 (en) 2005-03-16 2006-02-22 Pure particle generator
JP2008501895A JP2008532761A (en) 2005-03-16 2006-02-22 Pure particle generator
KR1020077022111A KR101154086B1 (en) 2005-03-16 2006-02-22 Pure particle generator

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US11/081,246 US8079838B2 (en) 2005-03-16 2005-03-16 Pure particle generator
US11/081,246 2005-03-16

Publications (2)

Publication Number Publication Date
WO2006101666A2 WO2006101666A2 (en) 2006-09-28
WO2006101666A3 true WO2006101666A3 (en) 2009-04-16

Family

ID=37009460

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2006/006582 WO2006101666A2 (en) 2005-03-16 2006-02-22 Pure particle generator

Country Status (6)

Country Link
US (1) US8079838B2 (en)
EP (1) EP1861216A4 (en)
JP (1) JP2008532761A (en)
KR (1) KR101154086B1 (en)
CN (1) CN101500734B (en)
WO (1) WO2006101666A2 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0428482D0 (en) 2004-12-30 2005-02-02 Ibm Method and apparatus for managing feedback in a group resource environment
US8783090B2 (en) * 2011-11-28 2014-07-22 Southwest Research Institute Apparatus and methods for determination of total and solid carbon content of engine exhaust
CN103234573B (en) * 2013-04-22 2015-03-18 张家港朗亿机电设备有限公司 Dust environment simulation equipment
CN104849189A (en) * 2015-05-14 2015-08-19 常熟市德虞矿山机电有限公司 Mine tunnel dust environment simulating testing system

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4586367A (en) * 1984-03-19 1986-05-06 Horiba Instruments Incorporated Proportional exhaust sampler and control means
US5058440A (en) * 1990-09-04 1991-10-22 Caterpillar Inc. Gas sampling device and dilution tunnel used therewith
US6331290B1 (en) * 1998-11-27 2001-12-18 Accentus Plc Formation of monodisperse particles

Family Cites Families (54)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2802236A (en) * 1953-07-27 1957-08-13 Phillips Petroleum Co Cooling and handling of petroleum pitches
US3342921A (en) * 1966-03-16 1967-09-19 West Virginia Pulp & Paper Co Process for producing fibrous filler having high wet end retention
NL7004971A (en) * 1969-04-12 1970-10-14
US3709641A (en) * 1970-08-03 1973-01-09 Union Oil Co Apparatus for preparing and extruding a gelatinous material
FR2299932A1 (en) * 1975-02-07 1976-09-03 Anvar VERY FINE DIVIDED LITHIUM AND ITS MANUFACTURING PROCESS
NL180807C (en) * 1975-12-26 1987-05-04 Morishita Jintan Co DEVICE FOR MANUFACTURING SEAMLESS MATERIAL FILLED CAPSULES.
US4264641A (en) * 1977-03-17 1981-04-28 Phrasor Technology Inc. Electrohydrodynamic spraying to produce ultrafine particles
JPS53153537U (en) * 1977-05-10 1978-12-02
JPS56118641A (en) * 1980-02-22 1981-09-17 Nippon Soken Inc Fine particle discharge amount measuring apparatus for vehicle
EP0087798B1 (en) * 1982-03-01 1987-05-06 Toyota Jidosha Kabushiki Kaisha A method and apparatus for making a fine powder compound of a metal and another element
JPH0610281B2 (en) * 1983-05-10 1994-02-09 トヨタ自動車株式会社 Ceramic-metal composite fine powder
US4734451A (en) * 1983-09-01 1988-03-29 Battelle Memorial Institute Supercritical fluid molecular spray thin films and fine powders
US4582731A (en) * 1983-09-01 1986-04-15 Battelle Memorial Institute Supercritical fluid molecular spray film deposition and powder formation
GB8604328D0 (en) * 1986-02-21 1986-03-26 Ici Plc Producing spray of droplets of liquid
US4746466A (en) * 1986-03-03 1988-05-24 Tdk Corporation Ultrasonic atomizing apparatus
US5090258A (en) * 1989-09-29 1992-02-25 Mitsubishi Jidosha Kogyo Kabushiki Kaisha Multiple flow-dividing dilution tunnel system
US5503372A (en) * 1989-11-27 1996-04-02 Martin Marietta Energy Systems, Inc. Nozzle for electric dispersion reactor
US5184501A (en) * 1991-05-03 1993-02-09 Horiba Instruments Incorporated Exhaust sampler and control means
JPH05312695A (en) * 1992-05-04 1993-11-22 Horiba Ltd Particulate collector by means of dilute tunneling
GB9313642D0 (en) * 1993-07-01 1993-08-18 Glaxo Group Ltd Method and apparatus for the formation of particles
US5460701A (en) * 1993-07-27 1995-10-24 Nanophase Technologies Corporation Method of making nanostructured materials
US5525320A (en) * 1994-07-11 1996-06-11 University Of Cincinnati Process for aluminum nitride powder production
US5472749A (en) * 1994-10-27 1995-12-05 Northwestern University Graphite encapsulated nanophase particles produced by a tungsten arc method
US5888926A (en) * 1995-08-28 1999-03-30 University Of Cincinnati Process for forming a sorbent-metal complex by employing a sorbent precursor
US6200819B1 (en) * 1995-09-29 2001-03-13 Horiba Instruments, Inc. Method and apparatus for providing diluent gas to exhaust emission analyzer
US6171433B1 (en) * 1996-07-17 2001-01-09 Iowa State University Research Foundation, Inc. Method of making polymer powders and whiskers as well as particulate products of the method and atomizing apparatus
US6075074A (en) * 1996-07-19 2000-06-13 Morton International, Inc. Continuous processing of powder coating compositions
US5788738A (en) * 1996-09-03 1998-08-04 Nanomaterials Research Corporation Method of producing nanoscale powders by quenching of vapors
US5905000A (en) * 1996-09-03 1999-05-18 Nanomaterials Research Corporation Nanostructured ion conducting solid electrolytes
US6652967B2 (en) * 2001-08-08 2003-11-25 Nanoproducts Corporation Nano-dispersed powders and methods for their manufacture
JP2001505190A (en) * 1996-10-14 2001-04-17 エフ・ホフマン―ラ ロシュ アーゲー Preparation method of fine powder preparation
US6379419B1 (en) * 1998-08-18 2002-04-30 Noranda Inc. Method and transferred arc plasma system for production of fine and ultrafine powders
US6062092A (en) * 1998-09-09 2000-05-16 Engine, Fuel, And Emissions Engineering, Incorporated System for extracting samples from a stream
US6472632B1 (en) * 1999-09-15 2002-10-29 Nanoscale Engineering And Technology Corporation Method and apparatus for direct electrothermal-physical conversion of ceramic into nanopowder
CN100418674C (en) * 2000-02-10 2008-09-17 特乔尼科斯有限公司 Plasma arc reactor for the production of fine powders
EP1282470B1 (en) * 2000-05-16 2008-08-20 Regents Of The University Of Minnesota High mass throughput particle generation using multiple nozzle spraying
US6620351B2 (en) * 2000-05-24 2003-09-16 Auburn University Method of forming nanoparticles and microparticles of controllable size using supercritical fluids with enhanced mass transfer
US6729195B2 (en) * 2001-05-10 2004-05-04 Caterpillar Inc Serial multistage aerosol diluter and control system
EP1414633A4 (en) * 2001-07-10 2005-01-26 Univ Technology Corp Devices and methods for the production of particles
US7404340B2 (en) * 2001-07-10 2008-07-29 Caterpillar Inc. Exhaust gas particulate measuring system
US6615677B2 (en) * 2001-07-10 2003-09-09 Caterpillar Inc Method for controlling dilution air
US7008644B2 (en) * 2002-03-20 2006-03-07 Advanced Inhalation Research, Inc. Method and apparatus for producing dry particles
WO2003086443A1 (en) * 2002-04-11 2003-10-23 Medimmune Vaccines, Inc. Spray freeze dry of compositions for intranasal administration
WO2003087339A2 (en) * 2002-04-11 2003-10-23 Medimmune Vaccines, Inc. Spray freeze dry of compositions for pulmonary administration
US7044009B2 (en) * 2002-05-20 2006-05-16 Caterpillar Inc. Dilution tunnel
US6796165B2 (en) * 2002-11-18 2004-09-28 Southwest Research Institute Apparatus and method for real-time measurement of mass, size and number of solid particles of particulate matter in engine exhaust
US7083748B2 (en) * 2003-02-07 2006-08-01 Ferro Corporation Method and apparatus for continuous particle production using supercritical fluid
WO2005005010A2 (en) * 2003-02-21 2005-01-20 Ferro Corporation Methods and apparatus for producing composite particles using supercritical fluid as plasticizing and extracting agent
WO2005022603A2 (en) * 2003-09-02 2005-03-10 Integral Technologies, Inc. Low cost conductive containers manufactured from conductive loaded resin-based materials
US7160489B2 (en) * 2003-10-10 2007-01-09 The Board Of Trustees Of The University Of Illinois Controlled chemical aerosol flow synthesis of nanometer-sized particles and other nanometer-sized products
US7413690B1 (en) * 2003-10-29 2008-08-19 The University Of Mississippi Process and apparatus for producing spherical pellets using molten solid matrices
US7282167B2 (en) * 2003-12-15 2007-10-16 Quantumsphere, Inc. Method and apparatus for forming nano-particles
US7281440B2 (en) * 2005-04-29 2007-10-16 Caterpillar Inc. Particulate sampling system having flow check device
US7261529B2 (en) * 2005-09-07 2007-08-28 Southwest Research Institute Apparatus for preparing biodegradable microparticle formulations containing pharmaceutically active agents

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4586367A (en) * 1984-03-19 1986-05-06 Horiba Instruments Incorporated Proportional exhaust sampler and control means
US5058440A (en) * 1990-09-04 1991-10-22 Caterpillar Inc. Gas sampling device and dilution tunnel used therewith
US6331290B1 (en) * 1998-11-27 2001-12-18 Accentus Plc Formation of monodisperse particles

Also Published As

Publication number Publication date
KR20080027221A (en) 2008-03-26
EP1861216A2 (en) 2007-12-05
US20060208399A1 (en) 2006-09-21
KR101154086B1 (en) 2012-06-11
EP1861216A4 (en) 2010-10-06
CN101500734B (en) 2011-12-21
CN101500734A (en) 2009-08-05
JP2008532761A (en) 2008-08-21
WO2006101666A2 (en) 2006-09-28
US8079838B2 (en) 2011-12-20

Similar Documents

Publication Publication Date Title
Erlebach et al. Structure evolution of nanoparticulate Fe 2 O 3
Pichot et al. Detonation of nanosized explosive: New mechanistic model for nanodiamond formation
CN107777674B (en) A method of two-dimensional material is prepared using atmospheric plasma
WO2006101666A3 (en) Pure particle generator
WO2009012939A3 (en) Cell with a cavity, structural element and method for the production thereof and use thereof
Amirov et al. Synthesis of carbon nanotubes by high current divergent anode-channel plasma torch
WO2009024976A3 (en) Enriched nanostructure composition
Uner et al. Nonequilibrium plasma aerotaxy of InN nanocrystals and their photonic properties
EP1908791A4 (en) Process for producing aqueous fluoropolymer dispersion
Thongtem et al. Solvothermal synthesis of CdS nanowires templated by polyethylene glycol
JP4961323B2 (en) Carbon nanotubes having a surface coated with a surfactant and method for producing the same
Azmina et al. Preparation of palm oil based carbon nanotubes at various ferrocene concentration
WO2005075663A3 (en) Nanosized composite material containing a biological compound and process for the preparation
Ghanbari et al. The effect of CdS/organic nanostructure as additive on the thermal stability of ABS polymer
Li et al. The preparation and properties of AP-based nano-limit growth energetic materials
Mansurov Complete Scheme for Fullerene, Graphene, and Soot Formation in Flame
Zhang et al. Effects on the surface structure of organic energetic materials using spin coating
Yang et al. Amorphous hollow carbon spheres synthesized using radio frequency plasma-enhanced chemical vapour deposition
Liu et al. Effects of polyvinylpyrrolidone and cetyltrimethylammonium bromide on morphology of lead tungstate particles
Detto et al. Excitonic recombination in superstoichiometric nanocrystalline TiO 2 grown by cluster precursors at room temperature
Netrattana et al. First-principles study of hydrogen adsorption on two-dimensional C2N sheet
Li et al. Control of the size and luminescence of carbon nanodots by adjusting ambient pressure in laser ablation process
Khan et al. Preparation of highly pure CdSe hollow structures: Their PL and hydrogen absorption properties
Zhang et al. HRXRD and Raman study of irradiation effects in InGaN/GaN layers induced by 2.3 áMeV Ne and 5.3 áMeV Kr ions
Yuan et al. Effect of a magnetic field on the energy levels of donor impurities in the ZnO parabolic quantum well

Legal Events

Date Code Title Description
WWE Wipo information: entry into national phase

Ref document number: 200680008199.6

Country of ref document: CN

121 Ep: the epo has been informed by wipo that ep was designated in this application
ENP Entry into the national phase

Ref document number: 2008501895

Country of ref document: JP

Kind code of ref document: A

NENP Non-entry into the national phase

Ref country code: DE

WWE Wipo information: entry into national phase

Ref document number: 2006736013

Country of ref document: EP

WWE Wipo information: entry into national phase

Ref document number: 1020077022111

Country of ref document: KR

WWE Wipo information: entry into national phase

Ref document number: 7870/DELNP/2007

Country of ref document: IN

NENP Non-entry into the national phase

Ref country code: RU