WO2003008664A3 - Method of making a passivated surface - Google Patents

Method of making a passivated surface Download PDF

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Publication number
WO2003008664A3
WO2003008664A3 PCT/IB2002/002770 IB0202770W WO03008664A3 WO 2003008664 A3 WO2003008664 A3 WO 2003008664A3 IB 0202770 W IB0202770 W IB 0202770W WO 03008664 A3 WO03008664 A3 WO 03008664A3
Authority
WO
WIPO (PCT)
Prior art keywords
metal surface
concentration
reactive gas
gas
exposing
Prior art date
Application number
PCT/IB2002/002770
Other languages
French (fr)
Other versions
WO2003008664A2 (en
Inventor
Tracey Jacksier
Robert Benesch
Original Assignee
Air Liquide
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=26854161&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=WO2003008664(A3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority claimed from US10/157,466 external-priority patent/US20030017359A1/en
Application filed by Air Liquide filed Critical Air Liquide
Priority to AT02745713T priority Critical patent/ATE500350T1/en
Priority to JP2003514975A priority patent/JP2004536227A/en
Priority to KR10-2003-7016559A priority patent/KR20040030684A/en
Priority to CA2448697A priority patent/CA2448697C/en
Priority to DE60239339T priority patent/DE60239339D1/en
Priority to AU2002317422A priority patent/AU2002317422A1/en
Priority to EP02745713A priority patent/EP1412551B1/en
Publication of WO2003008664A2 publication Critical patent/WO2003008664A2/en
Publication of WO2003008664A3 publication Critical patent/WO2003008664A3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/22—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
    • C23C16/30—Deposition of compounds, mixtures or solid solutions, e.g. borides, carbides, nitrides
    • C23C16/40—Oxides
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/04—Coating on selected surface areas, e.g. using masks
    • C23C16/045—Coating cavities or hollow spaces, e.g. interior of tubes; Infiltration of porous substrates
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C1/00—Pressure vessels, e.g. gas cylinder, gas tank, replaceable cartridge
    • F17C1/10—Pressure vessels, e.g. gas cylinder, gas tank, replaceable cartridge with provision for protection against corrosion, e.g. due to gaseous acid
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C3/00—Vessels not under pressure
    • F17C3/12—Vessels not under pressure with provision for protection against corrosion, e.g. due to gaseous acid
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/10—Composition for standardization, calibration, simulation, stabilization, preparation or preservation; processes of use in preparation for chemical testing
    • Y10T436/100833—Simulative of a gaseous composition
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/15—Inorganic acid or base [e.g., hcl, sulfuric acid, etc. ]
    • Y10T436/156666—Sulfur containing
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/18—Sulfur containing
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/18—Sulfur containing
    • Y10T436/182—Organic or sulfhydryl containing [e.g., mercaptan, hydrogen, sulfide, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/18—Sulfur containing
    • Y10T436/182—Organic or sulfhydryl containing [e.g., mercaptan, hydrogen, sulfide, etc.]
    • Y10T436/184—Only hydrogen sulfide
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/18—Sulfur containing
    • Y10T436/186—Sulfur dioxide
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/18—Sulfur containing
    • Y10T436/188—Total or elemental sulfur

Abstract

Methods of passivating a metal surface are described, the methods comprising the step of i) exposing the metal surface ti a silicon-containing passivation material; ii) evacuating the metal surface, iii) exposing the treated surface to a gas composition having a concentration of reactive gas that is greater than an intended reactive gas concentration of gas to be transported by the metal surface; iv) evacuating the metal surface to remove substantially all of the gas composition to enable maintenance of an increased shelf-life, low concentration reactive gas at an intended concentration; and v) exposing the metal surface to the reactive gas at the intended reactive gas concentration. Manufactured products, high stability fluids, and methods of making same are also described.
PCT/IB2002/002770 2001-07-17 2002-07-15 Method of making a passivated surface WO2003008664A2 (en)

Priority Applications (7)

Application Number Priority Date Filing Date Title
AT02745713T ATE500350T1 (en) 2001-07-17 2002-07-15 METHOD FOR PRODUCING A PASSIVATED SURFACE
JP2003514975A JP2004536227A (en) 2001-07-17 2002-07-15 Stability-enhancing gas with low concentration, product containing the same, and method for producing the same
KR10-2003-7016559A KR20040030684A (en) 2001-07-17 2002-07-15 Increased stability low concentration gases, products comprising same, and methods of making same
CA2448697A CA2448697C (en) 2001-07-17 2002-07-15 Method of making a passivated surface
DE60239339T DE60239339D1 (en) 2001-07-17 2002-07-15 METHOD FOR PRODUCING A PASSIVATED SURFACE
AU2002317422A AU2002317422A1 (en) 2001-07-17 2002-07-15 Method of making a passivated surface
EP02745713A EP1412551B1 (en) 2001-07-17 2002-07-15 Method of making a passivated surface

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US30601401P 2001-07-17 2001-07-17
US60/306,014 2001-07-17
US10/157,466 US20030017359A1 (en) 2001-07-17 2002-05-29 Increased stability low concentration gases, products comprising same, and methods of making same
US10/157,466 2002-05-29

Publications (2)

Publication Number Publication Date
WO2003008664A2 WO2003008664A2 (en) 2003-01-30
WO2003008664A3 true WO2003008664A3 (en) 2003-06-05

Family

ID=26854161

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/IB2002/002770 WO2003008664A2 (en) 2001-07-17 2002-07-15 Method of making a passivated surface

Country Status (10)

Country Link
US (3) US7794841B2 (en)
EP (1) EP1412551B1 (en)
JP (1) JP2004536227A (en)
KR (1) KR20040030684A (en)
CN (1) CN1223701C (en)
AT (1) ATE500350T1 (en)
AU (1) AU2002317422A1 (en)
CA (1) CA2448697C (en)
DE (1) DE60239339D1 (en)
WO (1) WO2003008664A2 (en)

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CN101724446B (en) * 2008-10-29 2012-11-21 中国石油化工股份有限公司 Operation method of metal-contained petroleum fraction storage tank
US9381082B2 (en) 2011-04-22 2016-07-05 Edwards Lifesciences Corporation Devices, systems and methods for accurate positioning of a prosthetic valve
CN102258837A (en) * 2011-06-22 2011-11-30 华南理工大学 Passivating agent as well as preparation method and application thereof
US8993336B1 (en) 2012-05-04 2015-03-31 Air Liquide America Specialty Gases Llc Sulfur calibration and analytical reference gas for part per billion concentration sulfur measurements
SG11201408075QA (en) * 2012-06-15 2015-01-29 Praxair Technology Inc Cylinder preparation for maintaining stability of stored materials
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CN105387337B (en) * 2014-09-09 2018-10-16 中国石油天然气股份有限公司 A kind of aluminium alloy gas cylinder and its processing method
JP6845235B2 (en) * 2016-06-22 2021-03-17 昭和電工株式会社 Hydrogen sulfide mixture and its manufacturing method and filling container
US20190242524A1 (en) * 2018-02-05 2019-08-08 Sharpsville Container Corporation High pressure cylinder
JP7117000B2 (en) * 2018-11-01 2022-08-12 国立研究開発法人物質・材料研究機構 Method for manufacturing container, method for manufacturing hydrogen sulfide container, and method for filling hydrogen sulfide
US11920732B2 (en) 2019-08-23 2024-03-05 Airgas, Inc. Use of stable isotopes of CO2 to validate cylinder preparation
CN113840941A (en) * 2019-12-17 2021-12-24 昭和电工株式会社 Method for manufacturing passivation film

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WO2003008664A2 (en) 2003-01-30
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EP1412551A2 (en) 2004-04-28
DE60239339D1 (en) 2011-04-14
CN1223701C (en) 2005-10-19
JP2004536227A (en) 2004-12-02
US7794841B2 (en) 2010-09-14
AU2002317422A1 (en) 2003-03-03
US20110100088A1 (en) 2011-05-05
US20050271544A1 (en) 2005-12-08
US20090120158A1 (en) 2009-05-14
US7837806B2 (en) 2010-11-23
ATE500350T1 (en) 2011-03-15
CA2448697C (en) 2012-09-25
EP1412551B1 (en) 2011-03-02
US8288161B2 (en) 2012-10-16

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