WO1997003154A3 - Process for making granular detergent component - Google Patents

Process for making granular detergent component Download PDF

Info

Publication number
WO1997003154A3
WO1997003154A3 PCT/US1996/011274 US9611274W WO9703154A3 WO 1997003154 A3 WO1997003154 A3 WO 1997003154A3 US 9611274 W US9611274 W US 9611274W WO 9703154 A3 WO9703154 A3 WO 9703154A3
Authority
WO
WIPO (PCT)
Prior art keywords
granular detergent
detergent component
hcl
powder
weight
Prior art date
Application number
PCT/US1996/011274
Other languages
French (fr)
Other versions
WO1997003154A2 (en
Inventor
Mark William Ridyard
David William York
Original Assignee
Procter & Gamble
Mark William Ridyard
David William York
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Procter & Gamble, Mark William Ridyard, David William York filed Critical Procter & Gamble
Priority to BR9609732A priority Critical patent/BR9609732A/en
Priority to US08/983,543 priority patent/US5962397A/en
Publication of WO1997003154A2 publication Critical patent/WO1997003154A2/en
Publication of WO1997003154A3 publication Critical patent/WO1997003154A3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/046—Salts
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/62—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions
    • C11D11/0082—Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions
    • C11D11/02—Preparation in the form of powder by spray drying
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/042—Acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/10—Carbonates ; Bicarbonates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/126—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in solid compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/128—Aluminium silicates, e.g. zeolites
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2086—Hydroxy carboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3757—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
    • C11D3/3761—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions in solid compositions

Abstract

The invention relates to a process for the preparation of a granular detergent component comprising the steps of: (i) forming the granular detergent component by drying an aqueous solution of a cationic surfactant to form a powder; (ii) optionally, densifying the powder; wherein the granular detergent component further comprises an acid, the granular detergent component having a reserve acidity of at least 1.0 g HCl/100g, preferably at least 3.0 g HCl/100g, and more preferably at least 8.0 g HCl/100g. The invention also relates to granular detergent components having a bulk density of at least 500 g/l comprising: at least 20 % by weight of cationic surfacatant (preferably choline ester), and from 1 % to 60 % by weight of an acid, and optionally, up to 79 % by weight of a detergent powder wherein the granular detergent component has a reserve acidity of at least 1.0 g HCl/100 g.
PCT/US1996/011274 1995-07-10 1996-07-03 Process for making granular detergent component WO1997003154A2 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
BR9609732A BR9609732A (en) 1995-07-10 1996-07-03 Process for the preparation of granular detergent component
US08/983,543 US5962397A (en) 1995-07-10 1996-07-03 Process for making granular detergent component

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP95304794A EP0753571A1 (en) 1995-07-10 1995-07-10 Process for making granular detergent composition
EP95304794.1 1995-07-10

Publications (2)

Publication Number Publication Date
WO1997003154A2 WO1997003154A2 (en) 1997-01-30
WO1997003154A3 true WO1997003154A3 (en) 1997-02-20

Family

ID=8221247

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US1996/011274 WO1997003154A2 (en) 1995-07-10 1996-07-03 Process for making granular detergent component

Country Status (5)

Country Link
EP (1) EP0753571A1 (en)
AR (1) AR002800A1 (en)
BR (1) BR9609732A (en)
CA (1) CA2226568A1 (en)
WO (1) WO1997003154A2 (en)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2315763A (en) * 1996-07-31 1998-02-11 Procter & Gamble Preparation of an agglomerated detergent composition comprising a surfactant a an acid source
DE19721885A1 (en) † 1997-05-26 1998-12-03 Henkel Kgaa Process for the production of granules containing cationic surfactants
US6627596B1 (en) * 1999-02-01 2003-09-30 The Procter & Gamble Company Cationic particle and a process for making thereof
GB0009029D0 (en) 2000-04-12 2000-05-31 Unilever Plc Laundry wash compositions
GB0009877D0 (en) * 2000-04-20 2000-06-07 Unilever Plc Granular detergent component and process for its preparation
GB0207484D0 (en) 2002-03-28 2002-05-08 Unilever Plc Solid fabric conditioning compositions
DE102008015110A1 (en) * 2008-03-19 2009-09-24 Henkel Ag & Co. Kgaa Spray-dried detergents or cleaning products
CA3075147C (en) 2009-04-30 2022-06-21 Zeltiq Aesthetics, Inc. Device, system and method of removing heat from subcutaneous lipid-rich cells
US20110166370A1 (en) 2010-01-12 2011-07-07 Charles Winston Saunders Scattered Branched-Chain Fatty Acids And Biological Production Thereof
GB201008825D0 (en) 2010-05-26 2010-07-14 Bripco Bvba Data centre cooling system
EP2678410B1 (en) 2011-02-17 2017-09-13 The Procter and Gamble Company Composiitons comprising mixtures of c10-c13 alkylphenyl sulfonates
CA2827658A1 (en) 2011-02-17 2012-08-23 The Procter & Gamble Company Bio-based linear alkylphenyl sulfonates
US8790670B2 (en) * 2012-12-28 2014-07-29 The Dial Corporation Detergent compositions dispersed in personal care products comprising a sorbent carrier

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4203851A (en) * 1978-06-16 1980-05-20 Colgate-Palmolive Company Fabric softening compositions and methods for manufacture thereof
US4228044A (en) * 1978-06-26 1980-10-14 The Procter & Gamble Company Laundry detergent compositions having enhanced particulate soil removal and antiredeposition performance
US4321157A (en) * 1979-11-03 1982-03-23 The Procter & Gamble Company Granular laundry compositions
US4715979A (en) * 1985-10-09 1987-12-29 The Procter & Gamble Company Granular detergent compositions having improved solubility
US5259964A (en) * 1991-12-18 1993-11-09 Colgate-Palmolive Co. Free-flowing powder fabric softening composition and process for its manufacture

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3128287A (en) 1963-01-31 1964-04-07 Pfizer & Co C 2,2'-oxodisuccinic acid, derivatives thereof, and process for preparing
US3308067A (en) 1963-04-01 1967-03-07 Procter & Gamble Polyelectrolyte builders and detergent compositions
US3635830A (en) 1968-05-24 1972-01-18 Lever Brothers Ltd Detergent compositions containing oxydisuccing acid salts as builders
US3723322A (en) 1969-02-25 1973-03-27 Procter & Gamble Detergent compositions containing carboxylated polysaccharide builders
CA992423A (en) 1972-04-28 1976-07-06 The Procter And Gamble Company Crystallization seed-containing detergent composition
US3835163A (en) 1973-08-02 1974-09-10 Monsanto Co Tetrahydrofuran polycarboxylic acids
US3985669A (en) 1974-06-17 1976-10-12 The Procter & Gamble Company Detergent compositions
US4120874A (en) 1977-01-05 1978-10-17 Monsanto Company Diesters of 6-cyano-2,2-tetrahydropyrandicarboxylates
US4102903A (en) 1977-01-05 1978-07-25 Monsanto Company Tetrahydropyran and 1,4-dioxane polycarboxylate compounds, methods for making such compounds and compositions and methods employing same
US4144226A (en) 1977-08-22 1979-03-13 Monsanto Company Polymeric acetal carboxylates
IT7828107A0 (en) * 1977-09-26 1978-09-26 Procter & Gamble ANTISTATIC DETERGENT COMPOSITION WITH SOFTENING EFFECT ON FABRICS AND PROCEDURE FOR PRODUCING THIS COMPOSITION.
DE2848892A1 (en) * 1977-11-16 1979-05-17 Unilever Nv SOFTENING DETERGENT
BE40T1 (en) 1977-11-17 1980-01-11 Procter & Gamble GRANULAR DETERGENT COMPOSITIONS FOR IMPROVED REMOVAL OF OILY FOULS
US4158635A (en) 1977-12-05 1979-06-19 Monsanto Company Detergent formulations containing tetrahydropyran or 1,4-dioxane polycarboxylates and method for using same
DE3413571A1 (en) 1984-04-11 1985-10-24 Hoechst Ag, 6230 Frankfurt USE OF CRYSTALLINE LAYERED SODIUM SILICATES FOR WATER SOFTENING AND METHOD FOR WATER SOFTENING
DE3417649A1 (en) 1984-05-12 1985-11-14 Hoechst Ag, 6230 Frankfurt METHOD FOR PRODUCING CRYSTALLINE SODIUM SILICATES
US4566984A (en) 1984-11-16 1986-01-28 The Procter & Gamble Company Ether polycarboxylates
GB8511303D0 (en) 1985-05-03 1985-06-12 Procter & Gamble Liquid detergent compositions
AU582519B2 (en) 1985-10-09 1989-03-23 Procter & Gamble Company, The Granular detergent compositions having improved solubility
US4663071A (en) 1986-01-30 1987-05-05 The Procter & Gamble Company Ether carboxylate detergent builders and process for their preparation
US4769159A (en) * 1986-02-18 1988-09-06 Ecolab Inc. Institutional softener containing cationic surfactant and organic acid
DE3742043A1 (en) 1987-12-11 1989-06-22 Hoechst Ag METHOD FOR PRODUCING CRYSTALLINE SODIUM LAYER SILICATES
GB9209170D0 (en) * 1992-04-28 1992-06-10 Unilever Plc Rinse conditioner
EP0656935A1 (en) * 1992-08-21 1995-06-14 Colgate-Palmolive Company Rinse cycle fabric softener

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4203851A (en) * 1978-06-16 1980-05-20 Colgate-Palmolive Company Fabric softening compositions and methods for manufacture thereof
US4228044A (en) * 1978-06-26 1980-10-14 The Procter & Gamble Company Laundry detergent compositions having enhanced particulate soil removal and antiredeposition performance
US4321157A (en) * 1979-11-03 1982-03-23 The Procter & Gamble Company Granular laundry compositions
US4715979A (en) * 1985-10-09 1987-12-29 The Procter & Gamble Company Granular detergent compositions having improved solubility
US5259964A (en) * 1991-12-18 1993-11-09 Colgate-Palmolive Co. Free-flowing powder fabric softening composition and process for its manufacture

Also Published As

Publication number Publication date
EP0753571A1 (en) 1997-01-15
BR9609732A (en) 1999-07-06
CA2226568A1 (en) 1997-01-30
AR002800A1 (en) 1998-04-29
WO1997003154A2 (en) 1997-01-30
MX9800338A (en) 1998-07-31

Similar Documents

Publication Publication Date Title
WO1997003154A3 (en) Process for making granular detergent component
HK1005518A1 (en) Method for enhancing the bulk softness of tissue paper and product therefrom
CA2089430A1 (en) Aqueous pharmaceutical suspension for pharmaceutical active
WO2001032663A3 (en) Pyrazolecarboxylic acid tricyclic derivatives, preparation and pharmaceutical compositions containing same
CA2293797A1 (en) Aqueous carrier systems for water-insoluble materials
ZA934266B (en) Stable compositions of gastroprotected omeprazole microgranules and process for the production thereof
HUP9900398A2 (en) Encapsulated bleach particles, process for its producing and detergent containing it
CA2094605A1 (en) Stable liquid detergent compositions containing peroxygen bleach suspended by a hydrophobic silica
HUT77716A (en) Process for producing derivatives of 4a,5,9,10,11,12,-hexahydro-6h-benzofuro[3a,3,2-ef][2]benzazepine ano products
EP0949294A4 (en) Aqueous suspension composition and water-dispersible dry composition
WO2002047492A3 (en) A moisture and oxygen stable composition and a process for obtaining said composition
AU6221298A (en) Process for preparing solid pharmaceutical dosage forms
MX9805945A (en) Process for preparing solid cast detergent products.
EP0791362A3 (en) Disinfecting compositions and processes for disinfecting surfaces
CA2228366A1 (en) French fry formulations comprising starch hydrolyzate products
CA2215553A1 (en) Fat-based confection
NZ512538A (en) Nonaqueous sizing composition for application to glass reinforcing fibers comprising a film former, a coupling agent and a polyamide powder
HUT47793A (en) Herbicide compositions containing 2,6-substituted-pyridine-carboxylic acid derivatives as active components and process for producing the active components
EP0368575A3 (en) Bleach formulation and aqueous detergent compositions
EP0699435A3 (en) Detergent compositions
CA2256559A1 (en) N-bis- or n-tris-[(1,2-dicarboxy-ethoxy)-ethyl]-amine derivatives and preparation and use of the same
CA2226071A1 (en) Pulverulent laundry and cleaning detergents ingredient
EP0400454A3 (en) Stabilized phosphite compositions
MX9704078A (en) Detergent compositions comprising cationic surfactant and process for making the composition.
CA2187516A1 (en) Process for the Manufacture of Free-Flowing Detergent Granules

Legal Events

Date Code Title Description
AK Designated states

Kind code of ref document: A2

Designated state(s): BR CA MX US

AK Designated states

Kind code of ref document: A3

Designated state(s): BR CA MX US

DFPE Request for preliminary examination filed prior to expiration of 19th month from priority date (pct application filed before 20040101)
WWE Wipo information: entry into national phase

Ref document number: PA/a/1998/000338

Country of ref document: MX

ENP Entry into the national phase

Ref document number: 2226568

Country of ref document: CA

Ref country code: CA

Ref document number: 2226568

Kind code of ref document: A

Format of ref document f/p: F

WWE Wipo information: entry into national phase

Ref document number: 08983543

Country of ref document: US