US6086935A - Method for the reduction of microbial level in cereal and legume products - Google Patents
Method for the reduction of microbial level in cereal and legume products Download PDFInfo
- Publication number
- US6086935A US6086935A US09/081,380 US8138098A US6086935A US 6086935 A US6086935 A US 6086935A US 8138098 A US8138098 A US 8138098A US 6086935 A US6086935 A US 6086935A
- Authority
- US
- United States
- Prior art keywords
- food product
- steam
- conduit
- particulate food
- particulate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B9/00—Preservation of edible seeds, e.g. cereals
- A23B9/02—Preserving by heating
- A23B9/025—Preserving by heating with use of gases
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B9/00—Preservation of edible seeds, e.g. cereals
- A23B9/02—Preserving by heating
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Cereal-Derived Products (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
- Beans For Foods Or Fodder (AREA)
Abstract
A particulate food product is indirectly heated to at least about 170° after steam is directly injected onto the particulate food product to provide a moist environment and surface moisture on the particulate food product. The indirect heating is continued for a time and temperature to reduce the microbial contamination of the particulate cereal and/or legume products by an amount of at least log 2 without the loss of the functional properties.
Description
The present invention generally relates to a method to reduce the microbial level in particulate food products such as cereal products and legume products. More particularly, steam is directly injected onto the particulate food product to provide a moist environment and surface moisture on the particulate food product. After the particulate food has a surface moisture content it is indirectly heated for a time and temperature sufficient to reduce the microbial contamination of the particulate cereal and/or legume products without the loss of the functional properties of the food product.
There is considerable commercial interest in reducing the microbial content of cereal grains, flours and grits made therefrom as well as legumes and uncooked particulate products made from legumes. Lower initial microbial count would prolong shelf life and generally provide a more wholesome food. Almost any foods can certainly be sterilized through heat treatment. That is part of a cooking process. What is important, however, to this invention and to any discussion of reducing the microbial count of foods prior to use, is to reduce the microbial count prior to cooking without substantially adversely affecting the performance characteristics of the food being treated. Moreover, it is important that the process to reduce microbial count of the particulate food be continuous and not require increased pressure or pressurized vessels.
The invention provides a continuous process or method of reducing the microbial level in a particulate food product. In one aspect, the invention provides a method for reducing the microbial level in (1) a cereal product which has been milled into a flour, (2) a full particulate cereal grain such a kernels of corn, wheat, barley, malt and grains of rice, or (3) broken cereal particulates such as grits, broken corn kernels and broken rice grains. In another aspect, the invention provides a method for reducing the microbial level in legumes such as soy beans, grits and flours as well as and peas (outside the pods) or peanuts.
The method of the invention is unique in that it is continuous, does not require increased pressures with sealed containers and indirectly heats the particulate food product shortly after and/or during the injection of steam directly onto the food product to increase the moisture level of the surface of the food particles. Care should be taken not to expose the food particulates to moisture prior to its indirect heating because the moisture will hydrate the particulate food below the surface of the food particles and then the steam and indirect heat will tend to cook the food product and reduce its functionality. Care also should be taken to inject substantially just steam and not steam with oxygen or some other inert gas because oxygen or another gas will tend to reduce the moisture level of the surface of the particles. It is this surface moisture coupled with indirect heating, however, which is important to reducing the microbial content of the food product without substantially adversely affecting the functionality of the food product. The method of the invention will reduce the microbial count of the particulate food by at least log 2, and in an important aspect by at least log 4. Indeed in many cases, the invention permits the reduction of a microbial count to levels which are currently undetectable. Moreover, the method of the invention is practiced without the necessity of pressurizing the heating vessel to pressures substantially above one atmosphere or atmospheric conditions.
The method includes continuously conveying the particulate food product through an elongated conduit without pressurizing the conduit. As the particulate product goes through the conduit, it has steam directly injected onto it and is indirectly heated. The important function of the steam is to provide an amount of surface moisture on the food particles which with the indirect heat will kill bacteria on the food. Just indirect heat without steam will not provide a sufficiently lethal atmosphere for the bacteria without having too much heat, such that the functionality of the food will be adversely affected. Conversely, just using steam to provide heat will merely "steam cook" the food. The heat source for the indirect heat coupled with the steam injection should have a temperature which is effective for indirectly heating the particulate food product to a temperature of at least about 170° F. The heat source should not heat the food through substantial direct contact with the food particles, but indirectly heat the particulate food such as by convection from the heat source to the particles. In an important aspect the conduit should have a heat source which is a jacket which substantially surrounds the conduit throughout its length where the jacket is heated such as by steam, oil, electrically or any other suitable means for heating. In another important aspect, the indirect heat source should have a temperature of from about 212° F. to about 370° F. The temperature of the heat source and time of exposure of the particulate food product to the heat source is a function of the sensitivity of the food to heating such that it does not lose any substantial functionality. The combination of the temperature of the heat source, steam injection, surface moisture and time of exposure of the particulate food to the indirect heat source, however, should be effective to heat the particulate food to at least 170° F. and reduce the microbial count the particulate food product being conveyed through the conduit by at least about log 2 when the particulate food is mixed and has steam injected to it as described below.
As the particulate food product is being conveyed through the elongated conduit and just after the injection of the steam or during the injection of steam into the particulate food product, the food product is indirectly heated. The steam injection is to raise the moisture level of the surface of the food particulates as they are conveyed through the conduit and being exposed to indirect heat. The steam is injected into the conduit in an amount which is effective for providing an atmosphere in the conduit with a relative humidity of at least about 80%. In an important aspect the steam is provided in an amount where the atmosphere in the conduit has a relative humidity of from about 80 to about 100%. The steam should have a temperature of at least 212° F., and in an important aspect, it is superheated to a temperature of from about 230° F. to about 330° F. The temperature of the steam should not exceed 370° F. because the steam may then reduce the functionality of the food product. Generally, if more than 5 weight percent of the starch in the particulate product is gelatinized, the functional properties of the product likely will be adversely affected. In the case of malt, not more than 5 percent of the enzyme activity should be adversely affected after the process of the invention. In the case of soy beans or products made therefrom, the protein dispersibility index should not be reduced more than about 5%. In the case of soybeans, the invention also may be used to deactivate some enzymes.
While the particulate food product is (1) being conveyed through the conduit, (2) is being directly exposed to steam and (3) is being exposed to the indirect heat, the particulate food product is mixed at a rate to insure that as many particles as possible are (a) heated to 170° F. and (b) have their surface moisture increased such that after exit from the conduit the microbial count of the particulate food product is reduced by at least log 2 without substantially affecting the functionality of the food product. In the invention, it is important that the food product not be substantially hydrated below its surface such that it will be "cooked" and have its functionality impaired. The indirect heat, the steam, the surface moisture on the particles and the time of exposure of the particulate food to the indirect heat and steam are all related such that they are effective to reduce the microbial content of the particulate food at least about log 2, and in an important aspect about log 4.
FIG. 1 is a schematic diagram of an apparatus which may be used to practice the invention.
FIG. 2 is a side view of the apparatus of FIG. 1.
The to-be-treated product is fed into a elongated heating device 4 which is shown in FIG. 1. The particulate food product is fed into the heating device from hopper 6 through feed aperture 8 into channel 10. The particulate product is conveyed down channel 10 in the y direction. Channel 10 is surrounded by a steam jacket 12 through which steam is circulated. A hollow rod 14 extends longitudinally down the center of the channel. A plurality of paddles 16 are mounted on the rod 14 down its longitudinal length. The rod 14 is rotated and the paddles are angled such that as the rod rotates the paddles mix the particulate food product and push the product down channel 10. The paddles have openings 18 which from channels which extend through the paddles to the hollow center of rod 14. These openings are to transmit steam going through the rod and paddles so that the steam may be injected into the particulate food product being transmitted down channel 10. As the rod rotates the paddles push product down the conduit to exit aperture 20 through which treated particulate food product drops. The openings in the paddles may be opened or closed to control steam injection into the product being transmitted down the channel. In one aspect of the invention, some of the openings in the paddles towards the feed input end of the channel are open to transmit steam from the hollow rotating rod 14 into the particulate food product. Steam can be supplied through the rod and as such through the paddles into the to-be-treated particulate product. The amount of steam injected is effective for providing a moist environment having a relative humidity of at least 80% and also heats the product. Additional indirect heating of the particulate food is done by using indirect heat from the jacket of the device. Just enough steam is injected to provide moisture on the surface of the to be treated particles. With the moisture and heat from the steam and the indirect heat from the heat jacket heat source of the device, the conditions are sufficient to kill micro-organisms at the surface of the particulate food without substantially reducing the functionality of the food. The higher moisture content, the heat and the time of exposure of the food to the heat must be limited to prevent that the functional properties of the to-be-treated product is negatively influenced. A device which can be used to treat the particulate food as described herein is available as a Solidaire Model SJCS 8-4 from the Hosokawa Bepex Corporation, 333 N.E. Taft Street, Minneapolis, Minn. 55413.
The rotating paddles as vehicles for injecting steam, assure that the steam is uniformly distributed over the surfaces of the food product particles, but not into the particulate food. By choosing a specific length for the device, the indirect heating time of the product can be varied. It is important that the steam is injected at about the beginning of indirect heating in the device and that the rest of the time that the product is exposed to the indirect heat is used to kill the micro-organisms present and thereafter dry the product. It is important that there is sufficient mixing of the particulate product during the treatment that the surfaces of the food product are moist and achieve a temperature of at least about 170° F. The particulate product should not be exposed to indirect heating for more than about 3 minutes before cooking might take place and an adverse affect to the product. In an important aspect of the invention the product is not exposed to indirect heating for more than about 90 seconds, with about 60 seconds as a maximum being preferred.
The product after the steam and heat treatment can be cooled and dried (if necessary) using conventional techniques. Thereafter the product is packaged and may be packaged under aseptic conditions to keep the product from being recontaminated with micro-organisms.
Cereals, such as barley, malted barley, wheat, rye, rice can be treated but also a processed product from them, such as grits, meal, flour, brokens. In the conduit system described above with a conduit length of about seven feet, rice brokens and rice flour were heated to 180° F. for 54 to 60 seconds and conveyed through the conduit at a rate of from 200 to 1500 pounds of particulate food per hour with two paddles injecting steam. In this treatment, a reduction of the micro-organism count of at least about log 2 was obtained. In the conduit systems described above, with a conduit length of about seven feet, malt was heated to about 180° F. for 15 seconds at a rate of about 960 pounds per hour with three paddles open (rotating at 400 rpm). In this malt treatment, a reduction of the micro-organism count of at least about log 4 was obtained.
After the treatment, the product can be used as such for food applications or further processed, such as milling, breaking, sifting to obtain a specific granulation. The heat treatment as claimed above will provide a food-safe product related to microbial contaminations.
The following examples illustrate methods for carrying out the invention and should be understood to be illustrative of, but not limiting upon, the scope of the invention which is defined in the appended claims.
Treatment of Malt
A Solidaire Model SJCS 8-4 is used to treat malt at a rate of 960 pounds per hour using three paddles open for the injection of steam into the malt as it was being put into the conduit. The paddles were rotated at 400 rpm. with the time of exposure of the particulate food in the conduit varying from 10 to 15 seconds. Three runs were made where run 1 provided an exit product temperature of 194° F., had a jacket temperature of 222° F. and a steam temperature of 301° F., run 2 provided an exit product temperature of 194° F., had a jacket temperate of 280° F. and a steam temperature of 268° F., and run 3 provided an exit product temperature of 206° F., had a jacket temperate of 280° F. and a steam temperature of 275° F. The conditions for the three runs, the control and the reduction in microbial count are summarized in the Table I below.
TABLE I
______________________________________
3 Control Samples of Food Malt
Log Log
TPC/gr. coliform MPN/gr.
______________________________________
A 6.4 5.5
B 6.2 5.56
C 6.25 5.38
______________________________________
3 Treatments Food Malt
Exit Est. Jacket Steam
Log Log Product Retention
Temp. Temp.
TPC/gr. coli Temp. (° F.)
Time (sec)
(° F.)
(° F.)
______________________________________
1 4.4 3.38 194 50.15 222 301
2 4.17 2.81 194 50.15 280 268
3 4.22 2.87 206 50.15 280 285
______________________________________
Treatment of Rice Brokens
A Solidaire Model SJCS 8-4 is used to treat rice brokens at a rate shown below using one or two paddles open for the injection of steam into the rice brokens as it was being put into the conduit. The paddles were rotated with the time of exposure of the particulate food in the conduit as shown in Table II below.
TABLE II
______________________________________
Temperature ° F.
Prod. Direct
Approx.
TPC/g Colif/g Exit Jacket
Steam Retention
Sample Log Log Temp. Temp. Temp. Time
______________________________________
1 1.45 0.7 216 347 228 54 sec
2 1.82
0.7 208
347
54 sec
3 1.48
0.7 207.5
350
54 sec
4 1.86
0.7 206.2
350
54 sec
5 1.68
0.7 207
346
54 sec
6 1.71
0.7 206.5
346
220
54 sec
Control
5.19 4.05
Control
4.92 3.55
2
Control
4.44 2.95
3
Control
4.99 4.29
4
Control
5.58 4.27
5
______________________________________
Treatment of Rice Flour
A Solidaire Model SJCS 8-4 is used to treat rice flour under the conditions described in Table III below.
TABLE III
______________________________________
Time 11.35
12.00 12.20
12.30 12.45
1.00 blanc
______________________________________
Lb./Hr. 1160
1160 1160
1160
1160
1160
# Paddles 3
3 3
3
3
open to
steam
RPM Rotor 600
600 600
600
600
600
Steam Jacket
254 254 254
254
254
254
Temp (° F.)
Direct Steam
250 270 265
264
264
263
Temp. (° F.)
PSI 244
24
24
24
24
H20 Cooking
11.62
13 13.9
13.5
12.27
H20 Cooling
11.31
12.28 12.6
12.45
11.63
10.92
# Code 1 2 3
Prod. Temp.
185 192
195
192
190
St. Dama 5.1 3.9
4.6
RVA 35%
1 Minute 347 322 337 328
10 Minute 312 305 312 272
12.5 Minute
275 294 290 260
______________________________________
Time 1.30 1.55 2.15
2.25
2.40
2.55
blanc 2
______________________________________
Lb./Hr. 1160
1160 1160
1160
1160
1160
# Paddles 3
3 3
3
3
open to
steam
RPM Rotor 600
600 600
600
600
600
Steam Jacket
254 254 254
254
254
254
Direct Steam
250 250 250
250
250
250
PSI 2424
24
22
22
22
H20 Cooking
13.7
13.7 14.5
12.35
13.1
H20 Cooling
12.4
12.4 12.9
12.6
9.92
# Code 4 5 7
Prod. Temp.
195
199 199
199
200
208
St. Dam. 3.6
3.9 5.1
3.08
RVA 35%
1 Minute 328
327
321
376
10 Minute 306
301
302
302 312
12.5 Minute
282
293 292
290 294
______________________________________
Time 3.30 3.45
4.10 pm
4.25
4.30
blanc
______________________________________
Lb./Hr. 116060
1160
1740-
2000
2000
1800
# Paddles Open
3 3
3
3
3
3
to Steam
RPM Rotor 600
600
600
600
600
Steam Jacket
254
254
254
254
254
254
Temp. ° F.
Direct Steam
256
256
256
261
270
Temp. ° F.
PSI 20.5 20
22
24
H20 Cooking
13.25
12.77
12.38
12.69
H20 Cooling
12.6 12.46
11.63
11.4 11.39
# Code 9 8
10
11
12
13
Prod. Temp.
200.3
203.5
205.5
187.7
175
182
St. Dam. 5.7 4.2
RVA 35%
5 Minute 276
311
350
350
339
10 Min. 2590
288
302
279
285
12.5 Min 253
282
291
295
265
______________________________________
TPC
Sample TPC (log geom log geom
(3/9/98) (cfu/g) cfu/g) mean Coliform
cfu/g
mean
______________________________________
Control A-a
6.7E + 04
4.83
4.84
4.4E + 03
3.64
3.70
Control A-b
7.2E + 04
4.86
5.8E + 03
3.76
Control B-a
5.5E + 04
4.74
4.76
6.9E + 03
3.84
3.83
Control B-b
6.0E + 04
4.78
6.5E + 03
3.81
Control C-a
3.1E + 04
4.49
4.62
5.1E + 03
3.71
3.75
Control C-b
5.SE + 04
4.74
6.2E + 03
3.79
Control D-a
3.2E + 04
4.51
4.40
1.6E + 03
3.20
3.40
Control D-b
2.0E + 04
4.30
3.9E + 03
3.59
Control E-a
1.7E + 04
4.23
4.19
1.3E + 03
3.11
3.21
Control E-b
1.4E + 04
4.15
2.0E + 03
3.30
Flour 1Aa
2.5E + 02
2.40
2.06
5.0E + 00
0.70
0.70
Flour 1Ab
2.0E + 02
2.30
5.0E + 00
0.70
Flour lBa
6.0E + 01
1.78
5.0E + 00
0.70
Flour lBb
6.0E + 01
1.78
5.0E + 00
0.70
Flour 2Aa
3.1E + 02
2.49
2.16
5.0E + 00
0.70
0.70
Flour 2Ab
2.5E + 02
2.40
S.0E + 00
0.70
Flour 2Ba
9.0E + 01
1.95
5.0E + 00
0.70
Flour 2Bb
6.0E + 01
1.78
5.0E + 00
0.70
3Aa 1.95 01
2.07
5.0E + 00
0.70
0.70
3Ab 2.11 02
5.0E + 00
0.70
3Ba 2.18 02
5.0E + 00
0.70
3Bb 2.04 02
5.0E + 00
0.70
4Aa 1.7001
1.70
5.0E + 00
0.70
0.70
4Ab 1.7801
5.0E + 00
0.70
4Ba 1.4801
5.0E + 00
0.70
4Bb 1.85 01
0.7000
5Aa 2.15 02
1.90
5.0E + 00
0.70
0.70
5Ab 1.90 01
5.0E + 00
0.70
5Ba 1.85 01
0.70 00
5Bb 1.70 01
0.70 00
6Aa 1.85 01
1.90
5.0E + 00
0.70
0.70
6Ab 1.60 01
5.0E + 00
0.70
6Ba 2.00 02
5.0E + 00
0.70
6Bb 2.15 02
5.0E + 00
0.70
7Aa 1.85 01
1.75
5.0E + 00
0.70
0.70
7Ab 2.30 02
5.0E + 00
0.70
7Ba 1.85 01
0.70+ 00
7Bb 1.00 01
5.0E + 00
0.70
8Aa 1.95 01
1.89
5.0E + 00
0.70
0.70
8Ab 2.00 02
5.0E + 00
0.70
8Ba 1.90 01
5.0E + 00
0.70
8Bb 1.70 01
5.0E + 00
0.70
9Aa 2.00 02
1.96
5.0E + 00
0.70
0.70
9Ab 1.70 01
5.0E + 00
0.70
9Ba 2.04 02
5.0E + 00
0.70
9Bb 2.11 02
5.0E + 00
0.70
10Aa 9.0E + 01
1.95
2.44
5.0E + 00
0.70
0.70
10Ab 1.2E + 02
2.08
5.0E + 00
0.70
10Ba 7.4E + 02
2.87
5.0E + 00
0.70
10Bb 7.3E + 02
2.86
5.0E + 00
0.70
11Aa 1.5E + 03
3.18
2.97
1.0E + 01
1.00
0.85
11Ab 1.8E + 03
3.26
1.0E + 01
1.00
11Ba 5.0E + 02
2.70
5.0E + 00
0.70
11Bb 5.8E + 02
2.76
5.0E + 00
0.70
12Aa 5.7E + 03
3.76
3.57
1.2E + 02
2.08
1.77
12Ab 5.4E + 03
3.73
3.0E + 01
1.48
12Ba 2.6E + 03
3.41
8.0E + 01
1.90
12Bb 2.4E + 03
3.38
4.0E + 01
1.60
13Aa 1.0E + 03
3.00
3.44
2.0E + 01
1.30
1.96
13Ab 1.1E + 03
3.04
5.0E + 01
1.70
13Ba 7.6E + 03
3.88
2.8 + 02
2.45
13Bb 7.0E + 03
3.85
2.4E + 02
2.38
______________________________________
Numerous modifications and variations in practice of the invention are expected to occur to those skilled in the art upon consideration of the foregoing detailed description of the invention. Consequently, such modifications and variations are intended to be included within the scope of the following claims.
Claims (22)
1. A continuous process for reducing the microbial level in a particulate cereal or legume food product, the process comprising:
conveying the particulate food product through a conduit, the conduit having a temperature which is effective for indirectly heating the particulate food product to a temperature of at least about 170° F., the particulate food product being conveyed through the conduit at a rate which is effective for heating the particulate food product to a temperature of at least about 170° F. as the particulate food product exits the conduit;
injecting steam into the particulate food product as it is being conveyed through the conduit to provide a moisture content on the surface of the particles of food product, the steam being injected in an amount which is effective for providing an atmosphere in the conduit with a relative humidity of at least about 80%;
mixing the particulate food product as it is being exposed to the indirect heat, while the particulate food product is being conveyed through the conduit and while the steam is being injected into the particulate food product, the mixing being at a rate which is effective to increase the temperature of substantially of all of the particulate food product to at least 170° F. and the mixing being at a rate which is effective to increase the surface moisture of the particles of food,
the indirect heat, the steam, the surface moisture on the particles and the particles having a time of exposure to the indirect heat and steam all of which are effective to reduce the microbial content of the particulate food at least about log 2, but not substantially adversely affect the functionality of the food.
2. The process as recited in claim 1 wherein the conduit has an indirect heat source which has a temperature of from about 212° F. to about 370° F.
3. The process as recited in claim 1 wherein the steam has a temperature of from about 212° F. to about 370° F.
4. The process as recited in claim 1 wherein the steam is injected into the conduit in an amount which is effective to provide a relative humidity of from about 80% to about 100%.
5. The process as recited in claim 1 wherein the conduit has an indirect heat source which has a temperature of from about 212° F. to about 370° F., the steam has a temperature of from about 212° F. to about 370° F., and the steam is injected into the conduit in an amount which is effective to provide a relative humidity of from about 80% to about 100%.
6. The process as recited in claim 1 wherein the indirect heating and the steam is injected into the conduit while maintaining the pressure in the conduit substantially at or below atmospheric conditions.
7. The process as recited in claim 5 wherein the indirect heating and the steam is injected into the conduit while maintaining the pressure in the conduit substantially at or below atmospheric conditions.
8. The process as recited in claim 1 wherein the steam injected into the conduit is substantially pure steam.
9. The process as recited in claim 5 wherein the steam injected into the conduit is substantially pure steam.
10. The process as recited in claim 1 wherein the steam is injected prior to or during the indirect heating of the particulate food product.
11. The process as recited in claim 5 wherein the steam is injected prior to or during the indirect heating of the particulate food product.
12. The process as recited in claim 1 wherein not more than 5 weight percent of starch in the food product is gelatinized during the process.
13. The process as recited in claim 5 wherein not more than 5 weight percent of starch in the food product is gelatinized during the process.
14. The process as recited in claim 1 wherein the particulate food product is selected from the group consisting of a cereal grain, broken cereal grains, a milled cereal product and mixtures thereof.
15. The process as recited in claim 5 wherein the particulate food product is selected from the group consisting of a cereal grain, broken cereal grains, a milled cereal product and mixtures thereof.
16. The process as recited in claim 4 wherein the particulate food product is selected from the group consisting of rice, broken rice grains, rice flour and mixtures thereof.
17. The process as recited in claim 13 wherein the particulate food product is selected from the group consisting of rice, broken rice grains, rice flour and mixtures thereof.
18. The process as recited in claim 14 wherein the particulate food product is malt and enzyme activity of the malt is not reduced more than about 5%.
19. The process as recited in claim 14 wherein the particulate food product is indirectly heated for not more than about 90 seconds.
20. The process as recited in claim 5 wherein the particulate food product is aseptically packaged.
21. The process as recited in claim 1 wherein the particulate food product is selected from the group consisting of soybeans and soy flour and a protein dispersibility index of the particulate food product is not reduced more than about 5%.
22. A continuous process for reducing the microbial level in a particulate cereal or legume food product, the process comprising:
conveying the particulate food product through a conduit, the conduit having a temperature which is effective for indirectly heating the particulate food product to a temperature of at least about 170° F., the particulate food product being conveyed through the conduit at a rate which is effective for heating the particulate food product to a temperature of at least about 170° F. as the particulate food product exits the conduit;
injecting steam into the particulate food product in an amount effective for raising the surface moisture content of the particulate food just prior to or during indirect heating, the steam being injected in an amount which is effective for providing an atmosphere in the conduit with a relative humidity of at least about 80% to about 100% without increasing pressure in the conduit substantially above atmospheric conditions;
mixing the particulate food product as it is being exposed to the indirect heat, while the particulate food product is being conveyed through the conduit and while the steam is being injected into the particulate food product, the mixing being at a rate which is effective to increase the temperature of substantially of all of the particulate food product to at least 170° F. and the mixing being at a rate which is effective to increase the surface moisture of the particles of food,
the indirect heat, the steam, the surface moisture on the particles and the particles having a time of exposure to the indirect heat and steam all of which are effective to reduce the microbial content of the particulate food at least about log 2.
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/081,380 US6086935A (en) | 1998-05-19 | 1998-05-19 | Method for the reduction of microbial level in cereal and legume products |
| CA002332354A CA2332354C (en) | 1998-05-19 | 1999-05-14 | Method for sterilising cereal and leguminous products |
| DE69926499T DE69926499T2 (en) | 1998-05-19 | 1999-05-14 | STERILIZATION PROCESS FOR CEREAL AND LEGUMINO PRODUCTS |
| PCT/US1999/010748 WO1999059418A1 (en) | 1998-05-19 | 1999-05-14 | Method for sterilising cereal and leguminous products |
| AU40802/99A AU4080299A (en) | 1998-05-19 | 1999-05-14 | Method for sterilising cereal and leguminous products |
| EP99924256A EP1079694B1 (en) | 1998-05-19 | 1999-05-14 | Method for sterlising cereal and legumous products |
| AT99924256T ATE300872T1 (en) | 1998-05-19 | 1999-05-14 | STERILIZATION PROCESS FOR GRAIN AND LEGUMINOSE PRODUCTS |
| US09/736,961 US6613371B2 (en) | 1997-07-23 | 2000-12-14 | Method for malting seeds |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/081,380 US6086935A (en) | 1998-05-19 | 1998-05-19 | Method for the reduction of microbial level in cereal and legume products |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US46189099A Continuation-In-Part | 1997-07-23 | 1999-12-15 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US6086935A true US6086935A (en) | 2000-07-11 |
Family
ID=22163784
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US09/081,380 Expired - Fee Related US6086935A (en) | 1997-07-23 | 1998-05-19 | Method for the reduction of microbial level in cereal and legume products |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US6086935A (en) |
| EP (1) | EP1079694B1 (en) |
| AT (1) | ATE300872T1 (en) |
| AU (1) | AU4080299A (en) |
| CA (1) | CA2332354C (en) |
| DE (1) | DE69926499T2 (en) |
| WO (1) | WO1999059418A1 (en) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2001047364A1 (en) * | 1999-12-15 | 2001-07-05 | Cargill Incorporated | Method for malting seeds |
| US6449872B1 (en) | 1998-11-02 | 2002-09-17 | Lp-Tutkimuskeskus Oy | Method and apparatus for treating cereal kernels, treated cereal kernels and their use |
| US6613371B2 (en) | 1997-07-23 | 2003-09-02 | Cargill, Incorporated | Method for malting seeds |
| US6616957B1 (en) | 2000-11-28 | 2003-09-09 | Kraft Foods Holdings, Inc. | Method of stabilizing graham flour, and cracker produced from said flour |
| US20050217504A1 (en) * | 2004-02-19 | 2005-10-06 | Walker Paul N | Gas treatment apparatus |
| WO2006021680A1 (en) | 2004-08-13 | 2006-03-02 | Moulins Soufflet Sa | Method for decontaminating berries |
| US20070292583A1 (en) * | 2006-06-16 | 2007-12-20 | Haynes Lynn C | Production of stabilized whole grain wheat flour and products thereof |
| US20080131582A1 (en) * | 2006-12-05 | 2008-06-05 | Jan Karwowski | Production of whole grain hot cereal products |
| US20080152781A1 (en) * | 2004-05-11 | 2008-06-26 | Dreese Patrick C | Wheat Materials and Related Methods |
| US20080286435A1 (en) * | 2007-05-17 | 2008-11-20 | Satake Corporation | Grain or legume having increased content of functional component and a manufacturing method thereof |
| US20150104549A1 (en) * | 2013-10-14 | 2015-04-16 | Roberto Leopoldo CASTRO GENERA | Process for deep thermal treatment of corn, for high-yield production of whole nixtamal (boiled corn) and reactor for obtaining the necessary conditions for the process |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102005035926A1 (en) * | 2005-07-28 | 2007-02-01 | Franz Zentis Gmbh & Co. Kg | Method and device for sterilization of porous particles, comprise use of heated nitrogen gas |
| BR112012017460A2 (en) | 2010-01-20 | 2015-09-01 | Conagra Foods Food Ingredients Company | Microbial reduction in a processing stream of a milled product |
| CN102971756B (en) | 2010-06-15 | 2016-11-09 | 艾丹米尔斯粮食有限责任公司 | The transportation dispatching of low microorganism bulk products |
| FR3009928B1 (en) * | 2013-09-03 | 2017-03-03 | Jean-Louis Benoit | PROCESS FOR PRETREATING CEREALS, IN PARTICULAR RICE |
Citations (42)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US31513A (en) * | 1861-02-19 | haasz | ||
| US198192A (en) * | 1877-12-18 | Improvement in processes and apparatus for disintegrating cereals | ||
| US1010202A (en) * | 1908-07-02 | 1911-11-28 | Simon Ltd Henry | Art of milling and conditioning flour from wheat. |
| US1574210A (en) * | 1924-10-29 | 1926-02-23 | Horace R Spaulding | Method and apparatus for steaming grain and the like |
| US2704257A (en) * | 1952-10-01 | 1955-03-15 | Process Millers Inc | Method of producing corn tortilla flour |
| US3035918A (en) * | 1959-06-01 | 1962-05-22 | Battalle Dev Corp | Process for treating food |
| US3159494A (en) * | 1962-12-31 | 1964-12-01 | Procter & Gamble | Treatment of flour to reduce microbiological contamination |
| US3159493A (en) * | 1962-12-31 | 1964-12-01 | Procter & Gamble | Method of sterilizing flour with minimum physicochemical change |
| US3194664A (en) * | 1960-05-19 | 1965-07-13 | Frito Company | Method for continuously producing nixtamal |
| US3212904A (en) * | 1963-02-04 | 1965-10-19 | Quaker Oats Co | Process for preparing a precooked corn flour |
| US3368902A (en) * | 1967-03-22 | 1968-02-13 | Isadore A. Berg | Corn chip |
| US3404986A (en) * | 1966-07-18 | 1968-10-08 | Krause Milling Co | Process for manufacturing corn flour |
| US3554772A (en) * | 1967-01-30 | 1971-01-12 | Borden Inc | Method of pasteurizing flour |
| US3653915A (en) * | 1970-06-08 | 1972-04-04 | Manuel Jesus Rubio | Tortilla and process using mono-or diglyceride |
| US3655385A (en) * | 1970-06-08 | 1972-04-11 | Roberto Gonzalez Barrera | Tortilla and process using edible hydrophilic gum |
| US3859452A (en) * | 1972-07-03 | 1975-01-07 | Fausto Celorio Mendoza | Method for obtaining nixtamalized flours |
| US4255459A (en) * | 1978-02-10 | 1981-03-10 | Glen Donald H G | Blanching, pasteurizing and sterilizing process and apparatus suitable therefor |
| US4329371A (en) * | 1976-10-04 | 1982-05-11 | Seven-H Corporation | Method of processing grain |
| GB2139872A (en) * | 1981-03-19 | 1984-11-21 | Weert Meelfab | Processing seeds and cocoa beans |
| US4543263A (en) * | 1983-06-07 | 1985-09-24 | Campbell Soup Company | Heating and cooling foods at high pressure in a continuous sterilization system |
| US4547383A (en) * | 1983-06-07 | 1985-10-15 | Campbell Soup Company | Continuous food sterilization system with hydrostatic sealed treatment chamber |
| US4555409A (en) * | 1984-04-09 | 1985-11-26 | Hart Edwin R | Cereal processing |
| US4594260A (en) * | 1984-09-21 | 1986-06-10 | Imit, A.C. | Process for producing nixtamalized corn flour |
| EP0196464A2 (en) * | 1985-02-28 | 1986-10-08 | Kikkoman Corporation | Method of processing by heating a powdery and/or granular substance, and apparatus therefor |
| WO1986005956A1 (en) * | 1985-04-11 | 1986-10-23 | Scanflavour A/S | A process for sterilising spices |
| EP0269257A2 (en) * | 1986-10-30 | 1988-06-01 | McCORMICK & COMPANY, INC. | Apparatus & process for sterilization of spices and leafy herbs |
| US4770891A (en) * | 1986-01-20 | 1988-09-13 | Willard Miles J | Method for preparing sheeted fried snack products |
| US4844937A (en) * | 1987-04-13 | 1989-07-04 | J. R. Scott Milling Company | Method for making puffable food products from corn and products produced therefrom |
| US4882188A (en) * | 1985-02-22 | 1989-11-21 | Nakamura & Partners | Process for preparing heat treated granular solid food |
| US4985269A (en) * | 1990-06-12 | 1991-01-15 | Borden, Inc. | Continuous extrusion for tortilla chip production |
| US4996063A (en) * | 1989-06-30 | 1991-02-26 | The United States Of America, As Represented By The Secretary Of Agriculture | Method for making a soluble dietary fiber composition from oats |
| US5176931A (en) * | 1992-03-13 | 1993-01-05 | Wenger Manufacturing, Inc. | Preparation of masa flour |
| US5225224A (en) * | 1992-07-15 | 1993-07-06 | Vannortwick H Christian | Process for forming corn grit food products |
| US5296253A (en) * | 1992-05-28 | 1994-03-22 | Texas A&M University | Intermediate moisture legume and cereal food product and method of producing |
| US5532013A (en) * | 1993-10-21 | 1996-07-02 | Centro De Investigacion Y De Estudios Avanzados Del I.P.N. | Method for the preparation of instant fresh corn dough or masa |
| US5558886A (en) * | 1993-10-21 | 1996-09-24 | Centro De Investigacion Y De Estudios Avanzados Del I.P.N. | Extrusion apparatus for the preparation of instant fresh corn dough or masa |
| US5558898A (en) * | 1994-09-20 | 1996-09-24 | Wenger Manufacturing Inc. | Continuous method of producing masa flour |
| US5589214A (en) * | 1989-01-27 | 1996-12-31 | Alfa-Laval Food Engineering Ab | Process for heat treatment of particulate materials such as food |
| US5637342A (en) * | 1995-06-07 | 1997-06-10 | Schreiber Foods, Inc. | Method for cooking bacon |
| US5652010A (en) * | 1984-12-14 | 1997-07-29 | Nabisco, Inc. | Production of masa corn-based products |
| US5681600A (en) * | 1995-12-18 | 1997-10-28 | Abbott Laboratories | Stabilization of liquid nutritional products and method of making |
| US5700505A (en) * | 1995-12-28 | 1997-12-23 | Mei Research, Inc. | Method of improving head rice yield |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE207724C (en) * | ||||
| US1750508A (en) * | 1928-06-23 | 1930-03-11 | Gen Mill Equipment Company | Method for conditioning grain |
| GB543720A (en) * | 1940-10-31 | 1942-03-10 | Simon Ltd Henry | Improvements relating to the heat treatment of wheat |
| US2801176A (en) * | 1953-09-10 | 1957-07-30 | Ataullah K Ozai-Durrani | Preparing ready-to-eat cereal foods |
| EP0094448B1 (en) * | 1982-05-19 | 1986-06-25 | Kikkoman Corporation | Method and apparatus for heat-treating powdered, granular and like materials |
| DE3344214A1 (en) * | 1983-12-07 | 1985-06-20 | Müller's Mühle Schneekoppe AG, 4650 Gelsenkirchen | Apparatus for the thermal flow treatment of linseed grain |
| GB2221830B (en) * | 1988-07-28 | 1992-08-26 | Daniel Henry Dudek | Means and method for sterilizing spices and like substances |
| AU3188693A (en) * | 1992-02-07 | 1993-08-12 | Mccormick & Company, Inc. | Method and apparatus for continuous sterilization and drying of spices and leafy herbs |
-
1998
- 1998-05-19 US US09/081,380 patent/US6086935A/en not_active Expired - Fee Related
-
1999
- 1999-05-14 EP EP99924256A patent/EP1079694B1/en not_active Expired - Lifetime
- 1999-05-14 WO PCT/US1999/010748 patent/WO1999059418A1/en active IP Right Grant
- 1999-05-14 CA CA002332354A patent/CA2332354C/en not_active Expired - Fee Related
- 1999-05-14 AT AT99924256T patent/ATE300872T1/en not_active IP Right Cessation
- 1999-05-14 AU AU40802/99A patent/AU4080299A/en not_active Abandoned
- 1999-05-14 DE DE69926499T patent/DE69926499T2/en not_active Expired - Fee Related
Patent Citations (44)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US198192A (en) * | 1877-12-18 | Improvement in processes and apparatus for disintegrating cereals | ||
| US31513A (en) * | 1861-02-19 | haasz | ||
| US1010202A (en) * | 1908-07-02 | 1911-11-28 | Simon Ltd Henry | Art of milling and conditioning flour from wheat. |
| US1574210A (en) * | 1924-10-29 | 1926-02-23 | Horace R Spaulding | Method and apparatus for steaming grain and the like |
| US2704257A (en) * | 1952-10-01 | 1955-03-15 | Process Millers Inc | Method of producing corn tortilla flour |
| US3035918A (en) * | 1959-06-01 | 1962-05-22 | Battalle Dev Corp | Process for treating food |
| US3194664A (en) * | 1960-05-19 | 1965-07-13 | Frito Company | Method for continuously producing nixtamal |
| US3159494A (en) * | 1962-12-31 | 1964-12-01 | Procter & Gamble | Treatment of flour to reduce microbiological contamination |
| US3159493A (en) * | 1962-12-31 | 1964-12-01 | Procter & Gamble | Method of sterilizing flour with minimum physicochemical change |
| US3212904A (en) * | 1963-02-04 | 1965-10-19 | Quaker Oats Co | Process for preparing a precooked corn flour |
| US3404986A (en) * | 1966-07-18 | 1968-10-08 | Krause Milling Co | Process for manufacturing corn flour |
| US3554772A (en) * | 1967-01-30 | 1971-01-12 | Borden Inc | Method of pasteurizing flour |
| US3368902A (en) * | 1967-03-22 | 1968-02-13 | Isadore A. Berg | Corn chip |
| US3653915A (en) * | 1970-06-08 | 1972-04-04 | Manuel Jesus Rubio | Tortilla and process using mono-or diglyceride |
| US3655385A (en) * | 1970-06-08 | 1972-04-11 | Roberto Gonzalez Barrera | Tortilla and process using edible hydrophilic gum |
| US3859452A (en) * | 1972-07-03 | 1975-01-07 | Fausto Celorio Mendoza | Method for obtaining nixtamalized flours |
| US4329371A (en) * | 1976-10-04 | 1982-05-11 | Seven-H Corporation | Method of processing grain |
| US4255459A (en) * | 1978-02-10 | 1981-03-10 | Glen Donald H G | Blanching, pasteurizing and sterilizing process and apparatus suitable therefor |
| USRE31513E (en) | 1978-02-10 | 1984-01-31 | Blanching, pasteurizing and sterilizing process and apparatus suitable therefor | |
| GB2139872A (en) * | 1981-03-19 | 1984-11-21 | Weert Meelfab | Processing seeds and cocoa beans |
| US4543263A (en) * | 1983-06-07 | 1985-09-24 | Campbell Soup Company | Heating and cooling foods at high pressure in a continuous sterilization system |
| US4547383A (en) * | 1983-06-07 | 1985-10-15 | Campbell Soup Company | Continuous food sterilization system with hydrostatic sealed treatment chamber |
| US4555409A (en) * | 1984-04-09 | 1985-11-26 | Hart Edwin R | Cereal processing |
| US4594260A (en) * | 1984-09-21 | 1986-06-10 | Imit, A.C. | Process for producing nixtamalized corn flour |
| US5652010A (en) * | 1984-12-14 | 1997-07-29 | Nabisco, Inc. | Production of masa corn-based products |
| US4882188A (en) * | 1985-02-22 | 1989-11-21 | Nakamura & Partners | Process for preparing heat treated granular solid food |
| EP0196464A2 (en) * | 1985-02-28 | 1986-10-08 | Kikkoman Corporation | Method of processing by heating a powdery and/or granular substance, and apparatus therefor |
| WO1986005956A1 (en) * | 1985-04-11 | 1986-10-23 | Scanflavour A/S | A process for sterilising spices |
| US4770891A (en) * | 1986-01-20 | 1988-09-13 | Willard Miles J | Method for preparing sheeted fried snack products |
| EP0269257A2 (en) * | 1986-10-30 | 1988-06-01 | McCORMICK & COMPANY, INC. | Apparatus & process for sterilization of spices and leafy herbs |
| US4844933A (en) * | 1986-10-30 | 1989-07-04 | Mccormick & Company, Inc. | Process for sterilization of spices and leafy herbs |
| US4844937A (en) * | 1987-04-13 | 1989-07-04 | J. R. Scott Milling Company | Method for making puffable food products from corn and products produced therefrom |
| US5589214A (en) * | 1989-01-27 | 1996-12-31 | Alfa-Laval Food Engineering Ab | Process for heat treatment of particulate materials such as food |
| US4996063A (en) * | 1989-06-30 | 1991-02-26 | The United States Of America, As Represented By The Secretary Of Agriculture | Method for making a soluble dietary fiber composition from oats |
| US4985269A (en) * | 1990-06-12 | 1991-01-15 | Borden, Inc. | Continuous extrusion for tortilla chip production |
| US5176931A (en) * | 1992-03-13 | 1993-01-05 | Wenger Manufacturing, Inc. | Preparation of masa flour |
| US5296253A (en) * | 1992-05-28 | 1994-03-22 | Texas A&M University | Intermediate moisture legume and cereal food product and method of producing |
| US5225224A (en) * | 1992-07-15 | 1993-07-06 | Vannortwick H Christian | Process for forming corn grit food products |
| US5532013A (en) * | 1993-10-21 | 1996-07-02 | Centro De Investigacion Y De Estudios Avanzados Del I.P.N. | Method for the preparation of instant fresh corn dough or masa |
| US5558886A (en) * | 1993-10-21 | 1996-09-24 | Centro De Investigacion Y De Estudios Avanzados Del I.P.N. | Extrusion apparatus for the preparation of instant fresh corn dough or masa |
| US5558898A (en) * | 1994-09-20 | 1996-09-24 | Wenger Manufacturing Inc. | Continuous method of producing masa flour |
| US5637342A (en) * | 1995-06-07 | 1997-06-10 | Schreiber Foods, Inc. | Method for cooking bacon |
| US5681600A (en) * | 1995-12-18 | 1997-10-28 | Abbott Laboratories | Stabilization of liquid nutritional products and method of making |
| US5700505A (en) * | 1995-12-28 | 1997-12-23 | Mei Research, Inc. | Method of improving head rice yield |
Non-Patent Citations (10)
| Title |
|---|
| Akao et al., "Sterilization of Powdery Food by Superheated Steam," Eng. and Food, vol. 2, 1993, 595-600. |
| Akao et al., Sterilization of Powdery Food by Superheated Steam, Eng. and Food , vol. 2, 1993, 595 600. * |
| Baquir, "Sanitation of Cereal Grains," Dissertation Abstracts, Dec. 1977, vol. 38, No. 6. |
| Baquir, Sanitation of Cereal Grains, Dissertation Abstracts , Dec. 1977, vol. 38, No. 6. * |
| Casolari, "About Basic Parameters of Food Sterilization Technology," Food MicroBiology, 1994, 11. 75-84. |
| Casolari, About Basic Parameters of Food Sterilization Technology, Food MicroBiology , 1994, 11. 75 84. * |
| Lawrence et al., "Fluidized Heating Process for Microbial Destruction in Wheat Flour," Chemical Eng. Progress Symp Series, No. 86, vol. 64, pp. 77-84. |
| Lawrence et al., Fluidized Heating Process for Microbial Destruction in Wheat Flour, Chemical Eng. Progress Symp Series , No. 86, vol. 64, pp. 77 84. * |
| Martinez et al., "Caracteristicas quimicas y usos de harina instantanea de maiz II.", Archivos Latinoamericanos de Nutricion 1993, 43, 316-320. |
| Martinez et al., Caracteristicas quimicas y usos de harina instantanea de maiz II. , Archivos Latinoamericanos de Nutricion 1993, 43, 316 320. * |
Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6613371B2 (en) | 1997-07-23 | 2003-09-02 | Cargill, Incorporated | Method for malting seeds |
| US6449872B1 (en) | 1998-11-02 | 2002-09-17 | Lp-Tutkimuskeskus Oy | Method and apparatus for treating cereal kernels, treated cereal kernels and their use |
| WO2001047364A1 (en) * | 1999-12-15 | 2001-07-05 | Cargill Incorporated | Method for malting seeds |
| US6616957B1 (en) | 2000-11-28 | 2003-09-09 | Kraft Foods Holdings, Inc. | Method of stabilizing graham flour, and cracker produced from said flour |
| US20050217504A1 (en) * | 2004-02-19 | 2005-10-06 | Walker Paul N | Gas treatment apparatus |
| US8313708B2 (en) | 2004-02-19 | 2012-11-20 | The Penn State Research Foundation | Gas treatment apparatus |
| US20080152781A1 (en) * | 2004-05-11 | 2008-06-26 | Dreese Patrick C | Wheat Materials and Related Methods |
| WO2006021680A1 (en) | 2004-08-13 | 2006-03-02 | Moulins Soufflet Sa | Method for decontaminating berries |
| US20070292583A1 (en) * | 2006-06-16 | 2007-12-20 | Haynes Lynn C | Production of stabilized whole grain wheat flour and products thereof |
| US8133527B2 (en) | 2006-06-16 | 2012-03-13 | Kraft Foods Global Brands Llc | Production of stabilized whole grain wheat flour and products thereof |
| US8173193B2 (en) | 2006-06-16 | 2012-05-08 | Kraft Foods Global Brands Llc | Production of stabilized whole grain flour and products thereof |
| US8455037B2 (en) | 2006-06-16 | 2013-06-04 | Kraft Food Global Brands Llc | Production of stabilized whole grain flour and products thereof |
| US8455036B2 (en) | 2006-06-16 | 2013-06-04 | Kraft Foods Global Brands Llc | Production of stabilized whole grain wheat flour and products thereof |
| US20080131582A1 (en) * | 2006-12-05 | 2008-06-05 | Jan Karwowski | Production of whole grain hot cereal products |
| US20080286435A1 (en) * | 2007-05-17 | 2008-11-20 | Satake Corporation | Grain or legume having increased content of functional component and a manufacturing method thereof |
| US20110151086A1 (en) * | 2007-05-17 | 2011-06-23 | Satake Corporation | Grain or legume having increased content of functional component and a manufacturing method thereof |
| US8399037B2 (en) | 2007-05-17 | 2013-03-19 | Satake Corporation | Grain or legume having increased content of functional component and a manufacturing method thereof |
| US20150104549A1 (en) * | 2013-10-14 | 2015-04-16 | Roberto Leopoldo CASTRO GENERA | Process for deep thermal treatment of corn, for high-yield production of whole nixtamal (boiled corn) and reactor for obtaining the necessary conditions for the process |
Also Published As
| Publication number | Publication date |
|---|---|
| CA2332354A1 (en) | 1999-11-25 |
| DE69926499D1 (en) | 2005-09-08 |
| EP1079694B1 (en) | 2005-08-03 |
| AU4080299A (en) | 1999-12-06 |
| DE69926499T2 (en) | 2006-06-14 |
| WO1999059418A1 (en) | 1999-11-25 |
| EP1079694A1 (en) | 2001-03-07 |
| ATE300872T1 (en) | 2005-08-15 |
| CA2332354C (en) | 2007-07-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US6086935A (en) | Method for the reduction of microbial level in cereal and legume products | |
| US9055764B2 (en) | System and method for the continuous treatment of solids at non-atmospheric pressure | |
| Kumitch et al. | Effect of fermentation time on the nutritional properties of pea protein‐enriched flour fermented by Aspergillus oryzae and Aspergillus niger | |
| KR960011518B1 (en) | High fiber flaked cereal | |
| US4903414A (en) | High pressure conditioning system | |
| Kwok et al. | Heat inactivation of trypsin inhibitors in soymilk at ultra‐high temperatures | |
| CN101959425A (en) | Detoxification of feed products | |
| Deepa et al. | Effect of high-temperature short-time ‘micronization’of grains on product quality and cooking characteristics | |
| CA2309968C (en) | Predigested seed food composition | |
| Correia et al. | Protein profile and malt activity during sorghum germination | |
| US6613371B2 (en) | Method for malting seeds | |
| AU781475B2 (en) | Method for malting seeds | |
| WO2001054519A1 (en) | Microwave radiation for heat treatment of grain | |
| Peisker | Feed processing-impacts on nutritive value and hygienic status in broiler feeds. | |
| WO1993025616A1 (en) | Encapsulated starch for ruminant feed | |
| Arrage et al. | Protein quality of whole wheat as affected by drum-drying and single-screw extrusion | |
| Warchalewski et al. | Influence of microwave heating on biological activities and electrophoretic pattern of albumin fraction of wheat grain | |
| NL2035033B1 (en) | Method for inhibiting bitter taste of tartary buckwheat seeds and its application | |
| Mulimani et al. | Effect of heat treatments on alpha-amylase inhibitor activity in sorghum (Sorghum bicolour L.) | |
| EP0103604A1 (en) | Improved rapid cooking foodstuffs | |
| JPS6411274B2 (en) | ||
| Shad et al. | Novel Radiant Heating Approaches to Dry Corn Kernels and Inactivate Harmful Microbes | |
| JPH0515324A (en) | Method for improving flavor of grains | |
| GB2116415A (en) | Improved rapid cooking foodstuffs | |
| Nierle | Views on the Amino Acid Composition of Grain and the Influence of Processing |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| AS | Assignment |
Owner name: CARGILL, INCORPORATED, MINNESOTA Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:TINERI, ROBERT M.;REEL/FRAME:009539/0650 Effective date: 19981007 Owner name: CARGILL, INCORPORATED, MINNESOTA Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:FISCHER, PHILLIP L.;REEL/FRAME:009537/0632 Effective date: 19981008 Owner name: CARGILL, INCORPORATED, MINNESOTA Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNOR:DELRUE, RITA M.;REEL/FRAME:009537/0616 Effective date: 19981008 |
|
| FEPP | Fee payment procedure |
Free format text: PAYOR NUMBER ASSIGNED (ORIGINAL EVENT CODE: ASPN); ENTITY STATUS OF PATENT OWNER: LARGE ENTITY |
|
| FPAY | Fee payment |
Year of fee payment: 4 |
|
| FPAY | Fee payment |
Year of fee payment: 8 |
|
| REMI | Maintenance fee reminder mailed | ||
| REMI | Maintenance fee reminder mailed | ||
| LAPS | Lapse for failure to pay maintenance fees | ||
| STCH | Information on status: patent discontinuation |
Free format text: PATENT EXPIRED DUE TO NONPAYMENT OF MAINTENANCE FEES UNDER 37 CFR 1.362 |
|
| FP | Lapsed due to failure to pay maintenance fee |
Effective date: 20120711 |