US4415729A - Recovering granular poly(arylene sulfide) particles from a poly(arylene sulfide) reaction mixture - Google Patents
Recovering granular poly(arylene sulfide) particles from a poly(arylene sulfide) reaction mixture Download PDFInfo
- Publication number
- US4415729A US4415729A US06/385,223 US38522382A US4415729A US 4415729 A US4415729 A US 4415729A US 38522382 A US38522382 A US 38522382A US 4415729 A US4415729 A US 4415729A
- Authority
- US
- United States
- Prior art keywords
- poly
- arylene sulfide
- organic solvent
- polar organic
- sulfide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
- C08G75/02—Polythioethers
- C08G75/0204—Polyarylenethioethers
- C08G75/025—Preparatory processes
- C08G75/0259—Preparatory processes metal hydrogensulfides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
- C08G75/02—Polythioethers
- C08G75/0204—Polyarylenethioethers
- C08G75/0209—Polyarylenethioethers derived from monomers containing one aromatic ring
- C08G75/0213—Polyarylenethioethers derived from monomers containing one aromatic ring containing elements other than carbon, hydrogen or sulfur
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
- C08G75/02—Polythioethers
- C08G75/0204—Polyarylenethioethers
- C08G75/0231—Polyarylenethioethers containing chain-terminating or chain-branching agents
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
- C08G75/02—Polythioethers
- C08G75/0204—Polyarylenethioethers
- C08G75/025—Preparatory processes
- C08G75/0254—Preparatory processes using metal sulfides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
- C08G75/02—Polythioethers
- C08G75/0204—Polyarylenethioethers
- C08G75/0277—Post-polymerisation treatment
- C08G75/0281—Recovery or purification
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
Abstract
Description
TABLE I ______________________________________ Run 1 Run 2 (Control) (Invention) ______________________________________ % greater than 0.1 mm 64.0 99.9 % greater than 0.2 mm 44.0 97.4 % greater than 0.4 mm 19.0 58.0 % greater than 0.7 mm 4.5 6.0 % greater than 2.0 mm 0 0 ______________________________________
TABLE II ______________________________________ Run 1 Run 3 (Control) (Invention) ______________________________________ Melt Flow after 1 hour 1098 1017 Melt Flow after 2 hours 450 423 Melt Flow after 4hours 137 103 Melt Flow after 6 hours 45 11 ______________________________________
TABLE III ______________________________________ Run 4Run 5 Run 6 Run (Invention) (Invention) (Invention) ______________________________________ Added 1 lb H.sub.2 O/lb PPS 0 0.20 0.25 Total Moles 0.30 0.66 0.75 H.sub.2 O/Mole NMP.sup.a % greater than 0.1 mm 99.8 -- -- % greater than 0.2 mm 97.8 -- -- % greater than 0.4 mm 73.0 98.5 99.0 % greater than 0.7 mm 22.0 92.5 83.0 % greater than 2.0 mm 0 16 10 ______________________________________ .sup.a includes residual water liberated during the polymerization
TABLE IV ______________________________________Run 7 Run 8Run 9 Run 10 (Con- (Inven- (Inven- (Inven- trol) tion) tion) tion) ______________________________________ Added lb H.sub.2 O/lb PPS 0.sup.a 0 0.12 0.20 Total Moles H.sub.2 O/Mole NMP.sup.b 0 0.30 0.516 0.661 % greater than 0.1 mm 10 -- -- -- % greater than 0.2mm 5 99.6 99.9 99.8 % greater than 0.4 mm 3.2 86 99.8 99.0 % greater than 0.7 mm 2.0 37 96.5 89.0 % greater than 2.0 mm 0 0 42 40 ______________________________________ .sup.a about 0.17 lb of H.sub.2 O per lb of PPS was vented from the reactor .sup.b includes residual water liberated during the polymerization.
TABLE V ______________________________________ Recovery Number of Discs Run Method Recipe Cracked Uncracked ______________________________________ 11 (Control) Blender Flash A 8 8 12 (Invention)Water Quench A 5 11 13 (Invention) Water Quench A 0 16 14 (Contol) Blender Flash B 12 4 15 (Control) Blender Flash B 4 12 16 (Invention) Water Quench B 0 16 17 (Invention) Water Quench B 0 16 ______________________________________
Claims (25)
Priority Applications (7)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US06/385,223 US4415729A (en) | 1982-06-04 | 1982-06-04 | Recovering granular poly(arylene sulfide) particles from a poly(arylene sulfide) reaction mixture |
CA000426301A CA1228448A (en) | 1982-06-04 | 1983-04-20 | Recovering granular poly(arylene sulfide) particles from a poly(arylene sulfide) reaction mixture |
AT83105506T ATE26989T1 (en) | 1982-06-04 | 1983-06-03 | RECOVERY OF POLY(ARYLENE SULPHIDE) GRANULES FROM A POLY(ARYLENE SULPHIDE) REACTION MIXTURE. |
EP83105506A EP0096384B2 (en) | 1982-06-04 | 1983-06-03 | Recovering granular poly(arylene sulfide) particles from a poly (arylene sulfide) reaction mixture |
DE8383105506T DE3371349D1 (en) | 1982-06-04 | 1983-06-03 | Recovering granular poly(arylene sulfide) particles from a poly (arylene sulfide) reaction mixture |
ES522953A ES8500301A1 (en) | 1982-06-04 | 1983-06-03 | Recovering granular poly(arylene sulfide) particles from a poly (arylene sulfide) reaction mixture. |
JP58099271A JPS591536A (en) | 1982-06-04 | 1983-06-03 | Recovery of granular poly(arylene sulfide) |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US06/385,223 US4415729A (en) | 1982-06-04 | 1982-06-04 | Recovering granular poly(arylene sulfide) particles from a poly(arylene sulfide) reaction mixture |
Publications (1)
Publication Number | Publication Date |
---|---|
US4415729A true US4415729A (en) | 1983-11-15 |
Family
ID=23520538
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US06/385,223 Expired - Lifetime US4415729A (en) | 1982-06-04 | 1982-06-04 | Recovering granular poly(arylene sulfide) particles from a poly(arylene sulfide) reaction mixture |
Country Status (7)
Country | Link |
---|---|
US (1) | US4415729A (en) |
EP (1) | EP0096384B2 (en) |
JP (1) | JPS591536A (en) |
AT (1) | ATE26989T1 (en) |
CA (1) | CA1228448A (en) |
DE (1) | DE3371349D1 (en) |
ES (1) | ES8500301A1 (en) |
Cited By (63)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4524200A (en) * | 1982-09-27 | 1985-06-18 | Phillips Petroleum Company | Granular poly(arylene sulfide) recovery using evaporation |
EP0202537A2 (en) * | 1985-05-08 | 1986-11-26 | Kureha Kagaku Kogyo Kabushiki Kaisha | Process for treating a polymer slurry |
US4645826A (en) * | 1984-06-20 | 1987-02-24 | Kureha Kagaku Kogyo Kabushiki Kaisha | Process for production of high to ultra-high molecular weight linear polyarylenesulfides |
US4703081A (en) * | 1986-04-08 | 1987-10-27 | Phillips Petroleum Company | Poly(arylene sulfide) resin ternary blends |
US4711796A (en) * | 1985-01-31 | 1987-12-08 | Phillips Petroleum Company | Poly(arylene sulfide) coating compositions |
US4716212A (en) * | 1986-09-05 | 1987-12-29 | Phillips Petroleum Company | Preparation of a high molecular weight poly(arylene sulfide ketone) |
US4730034A (en) * | 1987-01-23 | 1988-03-08 | Phillips Petroleum Company | Recovering poly(arylene sulfide) oligomers from a poly(arylene sulfide) reaction mixture |
US4748231A (en) * | 1986-11-21 | 1988-05-31 | Phillips Petroleum Company | Reprecipitation of poly(arylene sulfide) to increase molecular weight thereof |
EP0271253A2 (en) * | 1986-11-25 | 1988-06-15 | Tosoh Corporation | Process for recovering a polyarylene sulfide |
US4786711A (en) * | 1987-01-23 | 1988-11-22 | Phillips Petroleum Company | P-phenylene sulfide polymer preparation with dehydrated mixture of alkali metal hydroxide and excess alkali metal bisulfide |
US4794164A (en) * | 1986-08-13 | 1988-12-27 | Kureha Kagaku Kogyo Kabushiki Kaisha | Process for producing a polyarylene sulfide of excellent handling property and a polyarylene sulfide produced by the process thereof |
US4812552A (en) * | 1987-04-15 | 1989-03-14 | Phillips Petroleum Company | Process for preparing poly(arylene sulfide ketone) with water addition |
EP0311040A1 (en) * | 1987-10-05 | 1989-04-12 | Phillips Petroleum Company | Method to recover poly(arylene sulfide)s with vaporized liquids |
US4883552A (en) * | 1986-12-05 | 1989-11-28 | Phillips Petroleum Company | Pultrusion process and apparatus |
US4931516A (en) * | 1986-08-04 | 1990-06-05 | Kureha Kagaku Kogyo Kabushiki Kaisha | Process for producing polyarylene sulfide in titanium vessel with addition of water |
US4963651A (en) * | 1987-10-05 | 1990-10-16 | Phillips Petroleum Company | Method to recover poly(arylene sulfide)s with vaporized liquids |
USRE33545E (en) * | 1986-09-05 | 1991-02-26 | Phillips Petroleum Company | Preparation of a high molecular weight poly(arylene sulfide ketone) |
EP0417448A1 (en) * | 1989-07-31 | 1991-03-20 | Phillips Petroleum Company | Process for the preparation of poly(arylene sulfide) |
US5003042A (en) * | 1989-12-29 | 1991-03-26 | Phillips Petroleum Company | Preparation of poly(arylene sulfide ketone) and poly(arylene sulfide diketone) resins having improved filterability |
US5013822A (en) * | 1989-12-07 | 1991-05-07 | Phillips Petroleum Company | Process for preparing poly(arylene sulfide sulfone) with in-situ preparation of alkali metal carboxylate |
US5023315A (en) * | 1990-04-18 | 1991-06-11 | Phillips Peteroleum Company | Process for preparing arylene sulfide polymers |
US5037954A (en) * | 1989-05-08 | 1991-08-06 | Phillips Petroleum Company | Method to recover liquified poly(arylene sulfide) with separation agent |
US5045629A (en) * | 1987-10-05 | 1991-09-03 | Phillips Petroleum Company | Method to recover particulate poly(arylene) sulfides with vaporized separation agent |
US5045628A (en) * | 1989-12-29 | 1991-09-03 | Phillips Petroleum Company | Production and recovery of poly(arylene sulfide ketone) and poly(arylene sulfide diketone) resins |
US5053487A (en) * | 1989-10-04 | 1991-10-01 | Phillips Petroleum Company | Method to recover high molecular weight poly(arylene sulfide) by reprecipitation |
US5071949A (en) * | 1986-04-02 | 1991-12-10 | Tohpren Co., Ltd. | Process for preparation of polyphenylene-sulfide resins in the absence of specific polymerization assistants |
US5089597A (en) * | 1988-04-28 | 1992-02-18 | Phillips Petroleum Company | Method to recover granular poly(arylene sulfide ketone) and poly(arylene sulfide diketone) |
US5091509A (en) * | 1989-12-29 | 1992-02-25 | Phillips Petroleum Company | Recovery of poly(arylene sulfide ketone) and poly(arylene sulfide diketone) resins |
US5098992A (en) * | 1989-10-04 | 1992-03-24 | Phillips Petroleum Company | Method to recover high molecular weight poly(arylene sulfide) by reprecipitation |
US5115093A (en) * | 1990-11-23 | 1992-05-19 | Phillips Petroleum Company | Process for preparing arylene sulfide polymers in the presence of functionalized olefin |
US5126431A (en) * | 1989-12-29 | 1992-06-30 | Phillips Petroleum Company | Production and recovery of poly(arylene sulfide ketone) and poly(arylene sulfide diketone) resins |
EP0492572A2 (en) * | 1990-12-24 | 1992-07-01 | Phillips Petroleum Company | Distillation plus ion exchange processing of a brine stream |
US5128445A (en) * | 1990-06-14 | 1992-07-07 | Phillips Petroleum Company | Method to recover poly(arylene sulfide) polymers with water-polar organic compound |
US5149749A (en) * | 1990-05-31 | 1992-09-22 | Phillips Petroleum Company | Poly(phenylene sulfide) composition and articles having improved thermal stability at high temperatures |
US5159056A (en) * | 1990-12-11 | 1992-10-27 | Phillips Petroleum Company | Preparation of arylene sulfide polymer in the presence of titanium dioxide |
US5171831A (en) * | 1990-12-03 | 1992-12-15 | Phillips Petroleum Company | Producing high molecular weight poly(arylene sulfide) polymers by adding second polar solvent prior to termination of polymerization |
US5175243A (en) * | 1990-11-14 | 1992-12-29 | Phillips Petroleum Company | Process for preparing arylene sulfide polymers with halo benzene containing deactivating group |
US5210128A (en) * | 1991-07-24 | 1993-05-11 | Phillips Petroleum Company | Poly(arylene sulfide) compositions, composites, and methods of production |
US5239050A (en) * | 1991-05-13 | 1993-08-24 | Phillips Petroleum Company | Process for preparing arylene sulfide polymer with addition of aqueous alkali metal carboxylate prior to termination of polymerization |
US5266680A (en) * | 1989-07-31 | 1993-11-30 | Phillips Petroleum Company | Process for the preparation of poly(arylene sulfide) compositions |
US5360890A (en) * | 1991-08-14 | 1994-11-01 | Tosoh Corporation | Refining of polyarylene sulfides |
US5475081A (en) * | 1992-11-12 | 1995-12-12 | Tonen Chemical Corporation | Process for controlling a particle size of polyarylene sulfide and polyarylene sulfide thus produced |
WO2000032644A1 (en) * | 1998-12-02 | 2000-06-08 | Phillips Petroleum Company | Processes for the recovery of poly(arylene sulfide) |
US6281326B1 (en) | 1991-06-24 | 2001-08-28 | Phillips Petroleum Company | Process for preparing poly(arylene sulfide) polymers using waste material |
US6331608B1 (en) | 1999-09-13 | 2001-12-18 | Phillips Petroleum Company | Process for producing poly(arylene sulfide) |
US6369191B1 (en) | 1992-11-12 | 2002-04-09 | Dainippon Ink And Chemicals, Incorporated | Process for controlling a particle size of polyarylene sulfide and polyarylene sulfide thus produced |
EP1226184A1 (en) * | 1999-09-13 | 2002-07-31 | Phillips Petroleum Company | Methanol extraction of polar organic compounds and modifier compounds from poly(arylene sulfide) polymer and oligomer streams |
EP1375541A1 (en) * | 2001-03-12 | 2004-01-02 | Idemitsu Petrochemical Co., Ltd. | Process for producing polyarylene sulfide |
US20060189786A1 (en) * | 2005-02-22 | 2006-08-24 | Chevron Phillips Chemical Company, Lp | Inferred water analysis in polyphenylene sulfide production |
WO2015197857A1 (en) * | 2014-06-27 | 2015-12-30 | Solvay Sa | A process for production of poly(arylene sulfide) |
US9809681B2 (en) | 2015-02-19 | 2017-11-07 | Ticona Llc | Method for forming a low viscosity polyarylene sulfide |
US9815942B2 (en) | 2015-03-25 | 2017-11-14 | Ticona Llc | Technique for forming a high melt viscosity polyarylene sulfide |
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Families Citing this family (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6140323A (en) * | 1984-07-31 | 1986-02-26 | Dainippon Ink & Chem Inc | Production of arylene sulfide polymer |
JPS6176528A (en) * | 1984-09-25 | 1986-04-19 | Dainippon Ink & Chem Inc | Production of arylene sulfide polymer having high molecular weight |
JPS6176529A (en) * | 1984-09-21 | 1986-04-19 | Toyo Soda Mfg Co Ltd | Granular polyarylene sulfide and its production |
JPH0613609B2 (en) * | 1984-10-05 | 1994-02-23 | 大日本インキ化学工業株式会社 | A method of making Allen Sulfide polymer |
JPS61111329A (en) * | 1984-11-05 | 1986-05-29 | Dainippon Ink & Chem Inc | Production of arylene sulfide polymer |
DE3535455A1 (en) * | 1985-10-04 | 1987-04-09 | Bayer Ag | METHOD FOR ISOLATING POLYARYL SULFIDES |
JPS62148567A (en) * | 1985-12-23 | 1987-07-02 | Toyo Soda Mfg Co Ltd | Polyphenylene sulfide resin composition |
JPS62151462A (en) * | 1985-12-26 | 1987-07-06 | Toyo Soda Mfg Co Ltd | Polyphenylene sulfide resin composition |
JPH0768350B2 (en) * | 1986-12-24 | 1995-07-26 | 東ソー株式会社 | Method for producing polyarylene sulfide |
DE3728703A1 (en) * | 1987-08-28 | 1989-03-09 | Bayer Ag | PREPARATION OF POLYARYLENEULFIDES OF HIGH PURITY |
EP0339621A3 (en) * | 1988-04-28 | 1991-05-22 | Phillips Petroleum Company | Method to recover granular poly(arylene sulfide ketone) and poly(arylene sulfide diketone) by a liquid quench process |
JP2722577B2 (en) * | 1988-12-16 | 1998-03-04 | 東レ株式会社 | Method for producing porous particulate polyarylene sulfide resin |
JPH0672185B2 (en) * | 1989-07-17 | 1994-09-14 | 出光石油化学株式会社 | Method for producing polyarylene sulfide |
NL9001526A (en) * | 1990-07-05 | 1992-02-03 | Akzo Nv | PROCESS FOR PREPARING POLYARYLENE SULFIDE WITH LOW ALKALINE METAL CONTENT |
CA2043664A1 (en) * | 1990-10-22 | 1992-04-23 | Afif M. Nesheiwat | Poly(arylene sulfide/sulfone) processing properties improvement method |
US5334701A (en) * | 1992-10-23 | 1994-08-02 | Phillips Petroleum Company | Process for the removal of lower molecular weight fractions of poly(arylene sulfide) polymers |
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JP5125993B2 (en) * | 2008-10-31 | 2013-01-23 | 東レ株式会社 | Method for producing polyarylene sulfide resin |
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EP2821427B1 (en) | 2012-02-29 | 2018-12-12 | Toray Industries, Inc. | Method for producing polyarylene sulfide, cyclic polyarylene sulfide pellet and method for producing same |
WO2015047719A1 (en) * | 2013-09-25 | 2015-04-02 | Ticona Llc | Method of polyarylene sulfide crystallization |
CN107636045B (en) * | 2015-06-12 | 2020-02-18 | 株式会社吴羽 | Process for producing polyarylene sulfide in pellet form, and polyarylene sulfide in pellet form |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3687907A (en) * | 1970-11-09 | 1972-08-29 | Phillips Petroleum Co | Recovery of solvent in arylene sulfide polymer production |
US3697487A (en) * | 1971-05-05 | 1972-10-10 | Phillips Petroleum Co | Recovery of diluent in arylene sulfide polymer production |
US3839302A (en) * | 1973-10-01 | 1974-10-01 | Phillips Petroleum Co | Treatment of poly(arylene sulfide) reaction product |
US3919177A (en) * | 1973-11-19 | 1975-11-11 | Phillips Petroleum Co | P-phenylene sulfide polymers |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3308211A (en) * | 1962-06-27 | 1967-03-07 | Baker Perkins Inc | Process for producing plastic granules |
US3457242A (en) * | 1966-08-22 | 1969-07-22 | Phillips Petroleum Co | Arylene sulfide polymer recovery |
US3707528A (en) * | 1971-01-12 | 1972-12-26 | Phillips Petroleum Co | Recovery of poly(arylene sulfide) reaction slurry constituents |
US3956060A (en) * | 1971-12-30 | 1976-05-11 | Phillips Petroleum Company | Removal of reaction diluent from poly(arylene sulfide) reaction slurry |
JPS5212240A (en) * | 1975-07-18 | 1977-01-29 | Matsushita Electric Ind Co Ltd | Process for preparing transparent coating compounds |
US4116947A (en) * | 1977-04-29 | 1978-09-26 | Phillips Petroleum Company | Branched arylene sulfide polymer production |
JPS6043855B2 (en) * | 1977-09-26 | 1985-09-30 | 三菱瓦斯化学株式会社 | Method for isolating solid polyarylene esters from organic solutions |
JPS5450593A (en) * | 1977-09-29 | 1979-04-20 | Mitsubishi Gas Chem Co Inc | Isolation of solid polyarylene ester |
JPS5845425B2 (en) * | 1978-09-05 | 1983-10-08 | 三菱化学株式会社 | Method for producing naphthostyrills |
JPS5540738A (en) * | 1978-09-19 | 1980-03-22 | Toray Ind Inc | Preparation of poly-p-phenylene sulfide |
US4254207A (en) * | 1979-12-26 | 1981-03-03 | Hercules Incorporated | Process for producing spherical particles or crystalline polymers |
CA1230197A (en) * | 1983-12-07 | 1987-12-08 | Lacey E. Scoggins | Method for the crystallization of poly(arylene sulfide) |
-
1982
- 1982-06-04 US US06/385,223 patent/US4415729A/en not_active Expired - Lifetime
-
1983
- 1983-04-20 CA CA000426301A patent/CA1228448A/en not_active Expired
- 1983-06-03 DE DE8383105506T patent/DE3371349D1/en not_active Expired
- 1983-06-03 JP JP58099271A patent/JPS591536A/en active Granted
- 1983-06-03 EP EP83105506A patent/EP0096384B2/en not_active Expired - Lifetime
- 1983-06-03 ES ES522953A patent/ES8500301A1/en not_active Expired
- 1983-06-03 AT AT83105506T patent/ATE26989T1/en not_active IP Right Cessation
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3687907A (en) * | 1970-11-09 | 1972-08-29 | Phillips Petroleum Co | Recovery of solvent in arylene sulfide polymer production |
US3697487A (en) * | 1971-05-05 | 1972-10-10 | Phillips Petroleum Co | Recovery of diluent in arylene sulfide polymer production |
US3839302A (en) * | 1973-10-01 | 1974-10-01 | Phillips Petroleum Co | Treatment of poly(arylene sulfide) reaction product |
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Also Published As
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ATE26989T1 (en) | 1987-05-15 |
EP0096384A3 (en) | 1984-10-17 |
EP0096384A2 (en) | 1983-12-21 |
EP0096384B2 (en) | 1996-01-31 |
DE3371349D1 (en) | 1987-06-11 |
ES522953A0 (en) | 1984-10-01 |
ES8500301A1 (en) | 1984-10-01 |
EP0096384B1 (en) | 1987-05-06 |
JPS591536A (en) | 1984-01-06 |
JPH0125493B2 (en) | 1989-05-18 |
CA1228448A (en) | 1987-10-20 |
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