US3738884A - Method for producing non-woven fibrous products - Google Patents

Method for producing non-woven fibrous products Download PDF

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US3738884A
US3738884A US00059823A US3738884DA US3738884A US 3738884 A US3738884 A US 3738884A US 00059823 A US00059823 A US 00059823A US 3738884D A US3738884D A US 3738884DA US 3738884 A US3738884 A US 3738884A
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rolls
fabric
filament
filamentary material
gap
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US00059823A
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J Soehngen
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Suez WTS Solutions USA Inc
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Celanese Corp
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    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H3/00Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
    • D04H3/02Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of forming fleeces or layers, e.g. reorientation of yarns or filaments
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H11/00Non-woven pile fabrics
    • D04H11/08Non-woven pile fabrics formed by creation of a pile on at least one surface of a non-woven fabric without addition of pile-forming material, e.g. by needling, by differential shrinking
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H3/00Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
    • D04H3/08Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating
    • D04H3/16Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between thermoplastic filaments produced in association with filament formation, e.g. immediately following extrusion
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T156/00Adhesive bonding and miscellaneous chemical manufacture
    • Y10T156/10Methods of surface bonding and/or assembly therefor
    • Y10T156/1052Methods of surface bonding and/or assembly therefor with cutting, punching, tearing or severing
    • Y10T156/1059Splitting sheet lamina in plane intermediate of faces

Definitions

  • This invention relates to non-woven fibrous products and to processes and apparatus for producing such products.
  • the invention is concerned particularly with the provision of non-woven fibrous products of substantial bulk.
  • the present invention also is concerned with the collection of spray-spun filamentary material in the form of fibrous bodies.
  • the invention envisions the formation at a single collection station of non-woven fabrics in which different arrangements of the filamentary material exist at different zones across the thickness direction to give the fabrics distinctive properties.
  • Another object of the invention is to provide non- Woven pile-like fabrics characterized by the presence of a backing layer and integrally formed fibrous components protruding upwardly from the backing layer.
  • the invention may be used in connection with the production of products from any of the various materials that may be melted and extruded through an orifice to 3,738,884 Patented June 12, 1973 form a filament.
  • suitable types of fiber-forming materials are polyolefins, polyamides, polyesters, cellulose acetate, polyvinyl acetate, poly(methyl methacrylate) styrene copolymers, and glass.
  • a substantially continuous filament of thermoplastic polymeric material is formed by the spray spinning techniques disclosed in the aforesaid patent application of Wagner et al. and collected by means of opposed spaced-apart, contrarotating rolls disposed in the path of the material issuing from the extrusion orifice.
  • the gap between the two rolls is substantial, and only portions of the spray-gun filamentary material are deposited directly upon the roll surfaces.
  • the remainder of the filamentary material crosses back and forth randomly between the layers of material deposited on the roll surfaces to form a bridging structure connecting the layers together.
  • j i 1 Some bonding together of the filament sections ordinarily is desirable.
  • the rolls may be located close enough to the spray spinning nozzle to receive the filamentary material while surface portions of the filament sections are sufficiently tacky to permit a degree of self bonding at crossover points.
  • the collected filamentary material is removed from the collection zone in the form of a non-woven fabric having surface layers in which the fiber components are generally parallel to the fabric surfaces and having an interior core in which the fiber components extend at angles to the surfaces.
  • the relative thicknesses of the different fabric zones may be regulated by suitable adjustment of such factors as the gap between the rolls, the spacing of the rolls from the spray spinning nozzle and the speed of rotation of the rolls.
  • fibrous subassemblies contributing significantly to the overall fabric properties may be formed during the collection of the spray spun filamentary material.
  • the collector rolls are traversed laterally back and forth in front of the spinning nozzle in such a manner as to produce during each traverse a generally U-shaped sheet the ends of which are adjacent the roll surfaces and the central portion of which bridges the gap between the rolls.
  • the successively collected U-shaped sheet-like units are combined into a non-woven fabric in which overlapping and contacting end portions of a number of the U-shaped sheets are consolidated as surface layers or skins and in which the central bridging portions of adjacent sheets are spaced apart from each other to provide a resilient core formed integrally with the surface layers.
  • a plurality of spray spinning nozzles are arranged to project filamentary material toward the gap between the opposed collection surfaces of a single collector unit.
  • the spray patterns from adjacent nozzles overlap in the collection zone so that a unitary product will be formed even though the filamentary material issues from different sources.
  • Set-ups of this type are particularly desirable in producing fabrics having zones of different characteristics across the width thereof and in producing wide fabrics without the sheet-like subassemblies which sometimes are formed when a traverse motion is employed.
  • the invention also contemplates the production of pilelike non-woven fabrics.
  • the fibrous body removed from the collection zone through the gap between the opposed collector surfaces may be severed or slit lengthwise at a level between the surface layers deposited on the collector surfaces to provide two fabrics in each of which the surface layer serves as a backing and the attached portion of the bridging structure projects upwardly from the backing.
  • the nature of the upstanding material or pile will depend of course upon the conditions maintained during collection of the spray spun fiber, and a variety of effects can be achieved.
  • the upstanding material on the surface of the fabric may be thin sheet-like subassemblies forming transversely extending leaves.
  • This particular effect is achieved by slitting an assembly collected on a set-up having a traverse motion, and operating as described above to produce a series of thin, generally U-shaped, sheet-like subassemblies as the spray pattern moves laterally back and forth across the collector surfaces.
  • FIG. 1 is a schematic elevational view depicting one form of apparatus setup that may be used in practicing the invention. 7
  • FIG. 2 is a face view of the collector roll assembly shown in FIG. 1;
  • FIG. 3 is a top view of an apparatus setup similar to that illustrated in FIG. 1 but having a plurality of spray spinning nozzles associated with a single collector unit;
  • FIG. 4 is an elevational view depicting another form of collector structure and also illustrating the formation of pile-like non-woven fabrics in accordance with the invention
  • FIG. 5 is a schematic top view of another embodiment of the invention in which the collector unit is traversed bodily back and forth in front of the spray spinning means;
  • FIG. 6 is a diagrammatic view of the fibrous sub-assemblies produced during traverse motions of the collector unit of the apparatus of FIG. 5;
  • FIG. 7 is a photograph showing in longitudinal cross section the non-woven fabric produced through use in accordance with the invention of the apparatus of FIG. 5.
  • Spray spinning nozzle means are indicated schematically at 2 in FIG. 1.
  • Preferred nozzle structures are disclosed in the aforesaid patent application of Wagner et al. and for detailed information on these structures reference should be made to such application. It will be sufficient to point out here that the preferred spray spinning nozzle is provided with an orifice through which the molten fiber-forming material is extruded and is also provided with a plurality of gas passages disposed about the axis of the extrusion orifice.
  • the gas passages are inclined to direct heated gas, such as steam, along paths the axes of which converge toward but do not intersect the projected axis of the extrusion orifice.
  • the high velocity gas streams issuing from the gas passages attenuate the filament extruded through the extrusion orifice and project the filament away from the nozzle in a random swirling pattern.
  • the collector unit depicted in FIG. 1 includes a pair of opposed, spaced-apart rolls 4 and 6 mounted for rotation in a suitable frame and having smooth surfaces.
  • the rolls 4 and 6 are spaced a predetermined distance from the nozzle 2, and the gap between the rolls is in substantial alignment with the central axis of the nozzle 2.
  • the filament 8 is projected in a generally longitudinal direction from the nozzle 2, but increments thereof deviate randomly from the extrusion orifice axis due to the high filament velocity and the effects of the gas issuing from the nozzle.
  • the overall result is a spray pattern that 4 is generally conical in outline as indicated schematically at 9 in FIGS. 1 and 2.
  • the diameter of the spray pattern 9 should be greater than the gap between the surfaces of the collection rolls 4 and 6.
  • the extent to which the freshly-spun filamentary material hardens prior to collection also is affected by the spacing between the nozzle 2 and the collection unit. Ordinarily, it is desirable that collection takes place while the surfaces of the filamentary material are still sufiiciently tacky to effect self-bonding as between filament sections at crossover points. If other factors be held constant, the degree of self-bonding may be varied by changing the distance from the nozzle 2 to the collection rolls 4 and 6. Control over the degree of self-bonding achieved may also be exercised by regulation of the extrusion temperature at the nozzle 2 and/or by heating or cooling the surfaces of the collection rolls 4 and 6.
  • suitable binders and/or plasticizers may be employed.
  • compositions compatible with the fiber-forming material may be added to the melt supplied to the extrusion orifice, or spraying techniques may be used to apply suitable compositions to the filamentary material either in the zone of collection thereof or at a subsequent stage of the process.
  • the collection rolls 4 and 6 are rotated in the directions indicated by the arrows in FIG. 1, the collected filamentary material is removed from the collection zone through the gap between the rolls in the form of a nonwoven fabric product 10.
  • Any suitable drive means may be employed for rotating the rolls 4 and 6.
  • the drive means has been shown as including a motor 11, gear means 12 coupling the motor 11 to the shaft of roll 6, and gears 13 coupling together the rolls 4 and 6 for rotation at the same speed but in opposite directions.
  • the non-woven fabric 10 has a distinctive structure.
  • This structure includes upper and lower surface layers 14 spaced apart by an integrally formed core 15.
  • the surface layers 14 are made up of the fiber deposited upon the smooth surfaces of the collector rolls 4 and 6, and in these layers the predominant orientation of the filamentary material is parallel to the surface of the product 10.
  • the fiber components here are those that were collected as bridging units extending across the gap between the collector rolls 4 and 6, and their predominant orientation is at an angle to the faces of the product 10.
  • the density characteristics of the zones 14 and 15 also are different. In the surface layers 14 the filamentary components are packed closely together.
  • the bridging portion 15, however, is in the form of a network havimx substantial open spaces between fibrous componer
  • the thickness of the fabric 10 is determined by the spacing between the collector rolls 4 and 6. Normally it will be found desirable to mount the rolls so as to permit ad ustment of their relative positions, so that fabrics of different thicknesses may be produced.
  • the gap between the opposed surfaces of the rolls 4 and 6 should be in the range of from about one-eighth inch to about four inches in thickness, and more preferably within the range from about one-half inch to about two inches.
  • FIG. 3 Such an embodiment of the invention is illustrated in FIG. 3.
  • This embodiment includes a plurality of spray nozzles 16 disposed in alignment with the gap between a single pair of opposed collector rolls 18.
  • the rolls are mounted in a frame 20.
  • a motor 22 on the frame drives a belt 24, which passes over a pulley on the end of the shaft for the lower roll 18, and the shaft for the upper roll 18 is connected with the lower roll by a cross belt 26.
  • the rolls 18 rotate in opposite directions when the motor 22 is operating.
  • the positional relationships between the several nozzles 16. are such that the spray patterns 30 from adjacent nozzles overlap in the collection zone.
  • a wide non-woven fabric 32 is produced during operation of the equipment.
  • This fabric 32 is similar to the fabric described above in connection with FIG. I inthe sense that it is made up of surface layers connected together by bridging fiber components. In the widthwise direction the fabric 32 may be substantially uniform from zone to zone across the fabric or it may be characterized by zones that are different from one another.
  • Transverse uniformity is achieved when the overlap between the spray patterns from adjacent ones of the nozzles 16 is sufiicient to assure delivery of substantially the same amount of filamentary material to all portions of the collector zone.
  • the overlap between adjacent spray patterns from the nozzles 16 may be such as to cause the delivery of filamentary material to one portion of the collector to be greater than the delivery of filamentary material to another portion thereof.
  • Still other effects may be achieved in the embodiment of FIG. 3 by supplying fiber-forming materials having different characteristics to various ones of the several nozzles 16, and/or by using nozzles having extrusion orifices of different sizes or different rates of delivery.
  • the spray patterns of several nozzles 16 may overlap to the extent of intermingling filaments during formation of the mat or fabric. Different materials may be sprayed simultaneously from the nozzles to produce a fabric having a uniform dispersion of filaments of different materials.
  • the nozzles may be arranged along an axis perpendicular to the width dimension of the gap between the collector rolls, or any other suitable arrangement of nozzles may be used.
  • a non-woven fabric 32 may be produced that is characterized by the presence of longitudinally extending portions or stripes having different visual or structural properties.
  • the fabrics be provided with a defined flex-zone susceptible of being bent more readily than other portions of the fabric.
  • Such a zone can be formed by spray spinning from one of the nozzles 16 filamentary material of significantly smaller average denier than the filamentary material issuing from the other nozzles 16.
  • collector units in the embodiment described above have been shown as including opposed rolls having smooth surfaces, it will be understood that the invention is not limited to this particular form.
  • Suitable collector surfaces may be provided by endless belts, webs or the like, and the collector surfaces may be rough or provided with protruding portions or embossed patterns.
  • laminated products may be formed by collecting the filamentary material directly upon sheets or webs passed over one or both of the collector rolls and causing the filamentary material to adhere to such sheets or webs, as by heating or bonding treatments.
  • an endless belt 34 is mounted over rolls 36 and 38 and over an idler roll 40 which supports the intermediate portion of the belt 34.
  • An opposing belt 42 is mounted between the rolls 44 and 46 and passes over an idler roll 48.
  • Presser rolls 49 are mounted adjacent the idler rolls 40 and 48 in 6 position to bear against and guide the exterior surfaces of the belts 34 and 42.
  • a spray spinning nozzle 50 corresponding to the nozzle 2 in FIG. 1 is positioned opposite the gap between the belts 34 and 42 in the zone of the rolls 36 and 44. Collection of the filamentary material issuing from the nozzle 50 takes place in much the same manner as in FIG. 1. Portions of the filamentary material are deposited directly upon the surfaces of the belts 34 and 42 and other portions bridge back and forth across the gap. As the rolls rotate in the directions indicated by the arrows, the collected material is removed from the collection zone in the form of a non-woven fabric structure.
  • the fiber contacting flights of the belts 34 and 42 are substantially parallel. These surfaces maintain the newly formed non-woven fabric to the dimension of the gap and serve to minimize the mechanical loads imposed on the material.
  • the non-woven fabric product delivered by the belts 34 and 42 in the zone of the idler rolls 40 and 48 is similar to the product 10 produced as described in connection with FIG. 1, and this product may be used as such if desired.
  • FIG. 4 illustrates an additional operation that may be carried out in forming other novel products in accordance with the invention.
  • Severing means 52 is disposed between the belts 34 and 42 just beyond the idler rolls 40 and 48. This severing means 52 may be in the form of a stationary cutter blade, a reciprocating saw or blade, a band saw, or other suitable fiber severing device.
  • the level of the severing means 52 is such that it contacts the fiber components bridging the vertical space between the surface layers of the fibrous body being advanced by the belts 34 and 42.
  • the severance of these bridging components across the entire width of the body yields two separate fabrics 54. These move with the diverging flights of the belts 34 and 42 in the zone between the idler rolls 40 and 48 and the back rolls 38 and 46, and they are individually guided away by suitable means 55 for separate collection.
  • Each of the non-woven fabrics S4 is pile-like in character.
  • the surface layer of the filamentary material deposited on one of the belts of the collector constitutes a firm backing structure 56, and the severed portion 57 of the bridging fiber components extends from the backing in flexible pile-like configurations.
  • These non-woven pile; like fabrics may be produced economically and they are suitable for use in many of the environments where conventional pile fabrics have been employed heretofore.
  • a belt-type collector unit In producing these pile-like fabrics it is not essential that a belt-type collector unit be employed. Apparatus having roll-type collector units as shown in FIGS. 1-3 can be used for the production of pile fabrics by disposing suitable severing means downstream of the gap between the rolls. Generally, however, it will be found preferable to utilize a belt-type collector, because belts such as those shown at 34 and 42 in FIG. 4 provide relatively large surface areas for frictionally advancing the fibrous assembly against the severing means 52.
  • FIG. 5 illustrates schematically an apparatus setup in which relative lateral movement is effected as between spray spinning nozzle means and a collector unit.
  • a pair of opposed collector rolls 58 are disposed in front of spray spinning means 60, with the spray pattern 62 from the nozzle 60 intersecting the gap between the rolls 58.
  • the rolls 58 are mounted for rotation in a frame 64, and the frame 64 is carried by rails 66.
  • the rolls 58 are relatively long, as compared with the diameter of the spray pattern 62 at the collection zone.
  • the frame 64 is shifted back and forth along the rails 66 to position different portions of the roll surfaces in the path of the filamentary material issuing from the nozzle means 60.
  • the traversing motion of the rolls 58 may be accomplished through the use of any suitable drive means.
  • the drive means has been illustrated as including a link 68 pivotally connected at one of its ends to a pin 70 projecting from a belt 72 and at its other end to a bracket 74 on the frame 64.
  • the belt 72 is disposed beneath the level of the frame 64 and is trained about rolls 76 and 78.
  • the roll 78 is driven from a motor 80 through suitable coupling means such as a belt 82.
  • the roll 78 is rotated to move the belt 72 through an endless path.
  • the frame 64 traverses back and forth along the rails 66 in front of the nozzle 60.
  • a substantial degree of bonding at crossover points between contacting filament sections be achieved in the collection zone. This normally presents no difficulty because it usually is feasible to regulate the extrusion temperature and/or the spacing between the nozzle 60 and the collector rolls 58 so that the filamentary material reaches the collection zone while surface portions thereof are still sufficiently tacky to permit self-bonding at crossover points.
  • a suitable binder or plasticizer composition may be sprayed into the collection zone along with the filamentary material if desired.
  • each of the subassemblies is generally U-shaped in configuration, as suggested in FIG. 6, and within each sheet the filament is randomly arrayed in the sense that, if the U-shaped subassembly were flattened into a plane, incremental portions of the filament would be found extending in substantially all directions within that plane.
  • the U-shaped subassemblies 84 formed on successive traverses of the collector units are not entirely separate from each other. At the end of one traversing motion and the beginning of the next traversing motion, only a single body of filamentary material is collected, so that successive ones of the subassemblies 84 actually are united at the lateral margins of the fabric. This effect ordinarily is a desirable one, but in those instances where a high degree of widthwise product uniformity is required, the lateral margins of the fabric may be trimmed off.
  • the upper and lower end portions 86 of adjacent U- shaped subassemblies overlap substantially. These are interentangled somewhat and are packed together to form the surface layers at the top and bottom of the product collected. Portions of at least three and preferably five or more of the subassemblies 84 should be present at any given vertical cross section through one of the surface layers. In these surface layers, the fiber components are generally parallel to the faces of the fabric.
  • the mid-portions 88 of adjacent ones of the U-shaped subassemblies 84 are spaced apart from each other. This effect is indicated in FIG. 6 and in the photograph designated FIG. 7. The amount of the spacing is subject to variation, depending upon the characteristics desired in the products produced. Control over the spacing between the mid-portions 88 of successive U-shaped subassemblies 84 may be effected by suitable regulation of the surface speeds of the collector rolls 58 in relation to the rate of traverse of the rolls along the rails 66.
  • the mid-portions 88 of the subassemblies extend at angles to the faces of the non-woven fabrics.
  • the non-Woven fabric as a whole exhibits different fiber orientations in different zones across the thickness of the fabric. That is to say, the predominant orientation of the fiber components in the surface layers is parallel to the faces of the fabric, while the predominant fiber orientation in the middle of the fabric is at an angle to the fabric faces. This angle varies, of course, from 90 on down as one follows a U-shaped 8 subassembly from its mid-point toward a surface layer of the fabric.
  • Fabrics of the type illustrated in FIG. 7 may be used as such or they may be subjected to further treatments. Particularly interesting results may be obtained, for example, by slitting a fabric of this type through the midportions 88 of the U-shaped subassemblies. This slitting action may be carried out as described above in connection with FIG. 4.
  • Each of the two fabrics resulting from the slitting operation is characterized by a base or backing structure having a plurality of leaf-like assemblies of fiber components protruding therefrom.
  • the leaf-like bodies may be flexed independently of each other in a manner somewhat analogous to that of the pile of pile fabrics of a more conventional nature. However, the transverse continuity of the leaves gives these fabrics structural properties not heretofore attainable.
  • EXAMPLE Polypropylene pellets (Hercules Pro-fax 6423) were fed to a Modern Plastics Machinery extruder (1" x 24") having three zones maintained at 205 C., 275 C. and 335 C., respectively, and extruded through a nozzle having a circular orifice of 0.028 inch diameter at a material temperature of about 332 C.
  • the nozzle included three 0.082 inch ports disposed annularly about the orifice, directing streams of steam along paths the axes of which converged toward but did not intersect the extended axis of the extrusion orifice, the closest point to convergence lying about 1 inch from the orifice.
  • the steam had a line pressure of 16 p.s.i.g. and a temperature of 410 C.
  • the ports were spaced about apart and the axes were arranged to provide an opening of about inch in diameter therebetween at the point of closest convergence, through which the extrudate passed.
  • the extrudate was thereupon attenuated and whipped about with little or no breakage, and taken up While still at least tacky and capable of self-bonding at a point 8 /2 inches from the die orifice on a pair of rolls of 4 inch diameter, counterrotating at about 0.11 r.p.m. and providing a /2 inch nip therebetween through which the material passed in a band of about 3 inches width.
  • the resulting fabric had the firmness, deformability and resilience qualities required of carpet underlayments.
  • a suitable carpet underlay may be provided as 4 x 8 foot sheets or as a continuous matting of e.g., 9 feet width rolled about 4 to 6" cores, by utilizing a multiplicity of spray nozzles or traversing the take-up surface.
  • the underlayment may also be sprayed directly onto a carpet backing with a suitable binder or may even constitute the secondary backing itself.
  • the carpet backing comprises a similar synthetic polymer such as polypropylene as in the woven form described in US. Pat. 3,110,905.
  • the products of this invention are suitable for many other uses. Since the bulky structures are produced directly from an extrusion operation, they are relatively inexpensive. Furthermore, the structures produced in accordance with this invention do not necessarily contain any adhesive and therefore may be more resistant to solvent action than conventional non-woven fabrics.
  • unsevered fabric may be used for insulation, ceiling tile, air filters and other articles.
  • the pile-like structures produced from the severed fabric may be used for low cost floor covering, in clothing apparel, and other articles.
  • a method of making non-woven fabrics comprising extruding melted thermoplastic material to form a substantially continuous filament, projecting said filament in a longitudinal direction and in a random swirling pattern toward a gap between an opposed pair of spaced-apart moving collecting surfaces; and collecting the filamentary material in a zone extending across the path of the projected filament and partially occupied by convergent portions of the pair of moving collection surfaces so oriented with respect to each other as to leave a gap therebetween, the filamentary material being collected in the form of spaced-apart first and second surface layers respectively adjacent said collection surfaces and bridging portions between said layers, with the substantially continuous filament passing randomly through said surface layers and bridging portions.
  • thermoplastic, substantially continuous filament in a longitudinal direction spaced laterally from but generally parallel to said first-mentioned filament and in a random turbulent pattern overlapping a portion of said first-mentioned filament.
  • a process for making a non-woven fabric comprising spray spinning thermoplastic filamentary material toward a gap between an opposed pair of spaced apart collectors,
  • a process for making non-woven fabrics comprising extruding melted thermoplastic material through an orifice to form a substantially continuous filament stream, directing a plurality of high velocity gas streams generally longitudinally of said filament stream, to attenuate the filament stream and causing a swirling movement of said filament stream about the axis of said orifice,

Abstract

ING SURFACES DISPOSED IN THE PATH OF THE MATERIAL ISSUING FROM THE EXTRUSION ORIFICE.

A METHOD OF MAKING NON-WOVEN FABRICS COMPRISING SPRAY SPINNING A SUBSTANTIALLY CONTINUOUS FILAMENT OF THERMOPLASTIC POLYMERIC MATERIAL AND COLLECTING THIS MATERIAL BY MEANS OF OPPOSED SPACED-APART MOVING COLLECT-

Description

Jim'e 12, 1973 .1. w. SOEHNGEM METHOD FOR PRODUCING NON-WOVEN FIBROUS PRODUCTS 3 Sheets-Sheet 1 Original Filed Sept. 21. 1966 June 12, 1973 J. w. SOEHNGEN 3,738,
METHOD FOR PRODUCING NON-WOVEN FIBROUS PRODUCTS Original Filed Sept. 21, 1966 3 Sheefs-Sheet 2 June 12, 1973 J. w. SCEHNGEN 3,738,334
METHOD FOR PRODUCING NON-WOVEN FIBROUS PRODUCTS Original Filed Sept. 21, 1966 3 Sheefis-Sheet 5 United States Paten .0"
US. Cl. 156-167 11 Claims ABSTRACT OF THE DISCLOSURE A method of making non-woven fabrics comprising spray spinning a substantially continuous filament of thermoplastic polymeric material and collecting this material by means of opposed spaced-apart moving collecting surfaces disposed in the path of the material issuing from the extrusion orifice.
This application is a divisional of US. application Ser. No. 580,994, filed Sept. 21, 1966, now US. Pat. 3,607,588.
This invention relates to non-woven fibrous products and to processes and apparatus for producing such products. The invention is concerned particularly with the provision of non-woven fibrous products of substantial bulk.
Various proposals have been advanced heretofore for the formation of such fibrous products as mats and the like directly from molten fiber-forming material. In general, the fiber-forming material is extruded through orifices to form fiber and the fiber is collected on moving belts or the like in mat form. Examples of such proposals are disclosed in US. Pats. 2,206,058; 2,382,290; and 3,810,- 426. The density of the fibrous bodies collected by these techniques, and the orientation patterns of the fiber therein, do not vary much from zone to zone across the thickness direction of the mat.
More recently improved spray-spinning processes and apparatus have been developed which permit the formation of substantially continuous filaments at high production rates and without the concurrent formation of quantities of shot and such other undesirable physical forms as very short fiber elements. In this connection reference is made to the patent application of Wagner et al. US. application Ser. No. 581,075, filed Sept. 21, .1966, now abandoned, which is being filed concurrently herewith under the title Method and Apparatus for Producing Fibrous Structures and which is owned by applicants assignee.
The present invention also is concerned with the collection of spray-spun filamentary material in the form of fibrous bodies. However, the invention envisions the formation at a single collection station of non-woven fabrics in which different arrangements of the filamentary material exist at different zones across the thickness direction to give the fabrics distinctive properties.
More particularly, it is an object of this invention to provide novel non-woven fibrous structures having spacedapart surface layers of substantial density and having an integrally formed core made up of fibrous components bridging the space between the surface layers.
Another object of the invention is to provide non- Woven pile-like fabrics characterized by the presence of a backing layer and integrally formed fibrous components protruding upwardly from the backing layer.
Other objects of the invention include the provision of novel processes and apparatus for producing these fabrics economically and reliably.
The invention may be used in connection with the production of products from any of the various materials that may be melted and extruded through an orifice to 3,738,884 Patented June 12, 1973 form a filament. Examples of suitable types of fiber-forming materials are polyolefins, polyamides, polyesters, cellulose acetate, polyvinyl acetate, poly(methyl methacrylate) styrene copolymers, and glass.
In accordance with a preferred embodiment of the invention, a substantially continuous filament of thermoplastic polymeric material is formed by the spray spinning techniques disclosed in the aforesaid patent application of Wagner et al. and collected by means of opposed spaced-apart, contrarotating rolls disposed in the path of the material issuing from the extrusion orifice. The gap between the two rolls is substantial, and only portions of the spray-gun filamentary material are deposited directly upon the roll surfaces. The remainder of the filamentary material crosses back and forth randomly between the layers of material deposited on the roll surfaces to form a bridging structure connecting the layers together. j i 1 Some bonding together of the filament sections ordinarily is desirable. For example, the rolls may be located close enough to the spray spinning nozzle to receive the filamentary material while surface portions of the filament sections are sufficiently tacky to permit a degree of self bonding at crossover points.
.As the rolls rotate, the collected filamentary material is removed from the collection zone in the form of a non-woven fabric having surface layers in which the fiber components are generally parallel to the fabric surfaces and having an interior core in which the fiber components extend at angles to the surfaces. The relative thicknesses of the different fabric zones may be regulated by suitable adjustment of such factors as the gap between the rolls, the spacing of the rolls from the spray spinning nozzle and the speed of rotation of the rolls. In producing the high bulk products of this invention, it ordinarily is desirable that the individual surface layers have a thickness no greater than one-third of thickness of the product. More preferably, each of the surface layers should have a thickness less than one-sixth of the total fabricthickness, leaving over half of the fabric thickness to be taken up by the bridging structure constituting the interior core.
In accordance with another aspect of the invention, fibrous subassemblies contributing significantly to the overall fabric properties may be formed during the collection of the spray spun filamentary material. In one embodiment for example, the collector rolls are traversed laterally back and forth in front of the spinning nozzle in such a manner as to produce during each traverse a generally U-shaped sheet the ends of which are adjacent the roll surfaces and the central portion of which bridges the gap between the rolls. As the traversing continues, the successively collected U-shaped sheet-like units are combined into a non-woven fabric in which overlapping and contacting end portions of a number of the U-shaped sheets are consolidated as surface layers or skins and in which the central bridging portions of adjacent sheets are spaced apart from each other to provide a resilient core formed integrally with the surface layers.
In another embodiment, a plurality of spray spinning nozzles are arranged to project filamentary material toward the gap between the opposed collection surfaces of a single collector unit. The spray patterns from adjacent nozzles overlap in the collection zone so that a unitary product will be formed even though the filamentary material issues from different sources. Set-ups of this type are particularly desirable in producing fabrics having zones of different characteristics across the width thereof and in producing wide fabrics without the sheet-like subassemblies which sometimes are formed when a traverse motion is employed.
The invention also contemplates the production of pilelike non-woven fabrics. The fibrous body removed from the collection zone through the gap between the opposed collector surfaces may be severed or slit lengthwise at a level between the surface layers deposited on the collector surfaces to provide two fabrics in each of which the surface layer serves as a backing and the attached portion of the bridging structure projects upwardly from the backing. The nature of the upstanding material or pile will depend of course upon the conditions maintained during collection of the spray spun fiber, and a variety of effects can be achieved. For example, the upstanding material on the surface of the fabric may be thin sheet-like subassemblies forming transversely extending leaves. This particular effect is achieved by slitting an assembly collected on a set-up having a traverse motion, and operating as described above to produce a series of thin, generally U-shaped, sheet-like subassemblies as the spray pattern moves laterally back and forth across the collector surfaces.
A more complete understanding of these and other features of the invention will be gained from a consideration of the following description of certain embodiments illustrated in the accompanying drawings, in which:
FIG. 1 is a schematic elevational view depicting one form of apparatus setup that may be used in practicing the invention; 7
FIG. 2 is a face view of the collector roll assembly shown in FIG. 1;
FIG. 3 is a top view of an apparatus setup similar to that illustrated in FIG. 1 but having a plurality of spray spinning nozzles associated with a single collector unit;
FIG. 4 is an elevational view depicting another form of collector structure and also illustrating the formation of pile-like non-woven fabrics in accordance with the invention;
FIG. 5 is a schematic top view of another embodiment of the invention in which the collector unit is traversed bodily back and forth in front of the spray spinning means;
FIG. 6 is a diagrammatic view of the fibrous sub-assemblies produced during traverse motions of the collector unit of the apparatus of FIG. 5; and
FIG. 7 is a photograph showing in longitudinal cross section the non-woven fabric produced through use in accordance with the invention of the apparatus of FIG. 5.
Spray spinning nozzle means are indicated schematically at 2 in FIG. 1. Preferred nozzle structures are disclosed in the aforesaid patent application of Wagner et al. and for detailed information on these structures reference should be made to such application. It will be sufficient to point out here that the preferred spray spinning nozzle is provided with an orifice through which the molten fiber-forming material is extruded and is also provided with a plurality of gas passages disposed about the axis of the extrusion orifice. The gas passages are inclined to direct heated gas, such as steam, along paths the axes of which converge toward but do not intersect the projected axis of the extrusion orifice. The high velocity gas streams issuing from the gas passages attenuate the filament extruded through the extrusion orifice and project the filament away from the nozzle in a random swirling pattern.
The collector unit depicted in FIG. 1 includes a pair of opposed, spaced-apart rolls 4 and 6 mounted for rotation in a suitable frame and having smooth surfaces. The rolls 4 and 6 are spaced a predetermined distance from the nozzle 2, and the gap between the rolls is in substantial alignment with the central axis of the nozzle 2.
The filament 8 is projected in a generally longitudinal direction from the nozzle 2, but increments thereof deviate randomly from the extrusion orifice axis due to the high filament velocity and the effects of the gas issuing from the nozzle. The overall result is a spray pattern that 4 is generally conical in outline as indicated schematically at 9 in FIGS. 1 and 2.
In establishing the proper spacial relationship between the nozzle 2 and the collector unit, consideration should be given to the shape and size of the spray pattern 9 in the collection zone. As indicated in FIG. 2, the diameter of the spray pattern 9 should be greater than the gap between the surfaces of the collection rolls 4 and 6. When this relationship exists, portions of the projected filamentary material will be deposited directly upon the surfaces of the rolls 4 and 6 and other portions will be swirled about randomly to bridge the gap between the rolls.
The extent to which the freshly-spun filamentary material hardens prior to collection also is affected by the spacing between the nozzle 2 and the collection unit. Ordinarily, it is desirable that collection takes place while the surfaces of the filamentary material are still sufiiciently tacky to effect self-bonding as between filament sections at crossover points. If other factors be held constant, the degree of self-bonding may be varied by changing the distance from the nozzle 2 to the collection rolls 4 and 6. Control over the degree of self-bonding achieved may also be exercised by regulation of the extrusion temperature at the nozzle 2 and/or by heating or cooling the surfaces of the collection rolls 4 and 6.
In instances where supplemental fiber-to-fiber bonding may be desired, suitable binders and/or plasticizers may be employed. For example, compositions compatible with the fiber-forming material may be added to the melt supplied to the extrusion orifice, or spraying techniques may be used to apply suitable compositions to the filamentary material either in the zone of collection thereof or at a subsequent stage of the process.
As the collection rolls 4 and 6 are rotated in the directions indicated by the arrows in FIG. 1, the collected filamentary material is removed from the collection zone through the gap between the rolls in the form of a nonwoven fabric product 10. Any suitable drive means may be employed for rotating the rolls 4 and 6. In FIG. 2 the drive means has been shown as including a motor 11, gear means 12 coupling the motor 11 to the shaft of roll 6, and gears 13 coupling together the rolls 4 and 6 for rotation at the same speed but in opposite directions.
The non-woven fabric 10 has a distinctive structure. This structure includes upper and lower surface layers 14 spaced apart by an integrally formed core 15. The surface layers 14 are made up of the fiber deposited upon the smooth surfaces of the collector rolls 4 and 6, and in these layers the predominant orientation of the filamentary material is parallel to the surface of the product 10. However, a significantly different orientation exists in the core 15. The fiber components here are those that were collected as bridging units extending across the gap between the collector rolls 4 and 6, and their predominant orientation is at an angle to the faces of the product 10.
The density characteristics of the zones 14 and 15 also are different. In the surface layers 14 the filamentary components are packed closely together. The bridging portion 15, however, is in the form of a network havimx substantial open spaces between fibrous componer The thickness of the fabric 10 is determined by the spacing between the collector rolls 4 and 6. Normally it will be found desirable to mount the rolls so as to permit ad ustment of their relative positions, so that fabrics of different thicknesses may be produced. The gap between the opposed surfaces of the rolls 4 and 6 should be in the range of from about one-eighth inch to about four inches in thickness, and more preferably within the range from about one-half inch to about two inches.
Although a single spray spinning nozzle is indicated in FIG. 1, the use of a plurality of such nozzles is preferable in some instances. Such an embodiment of the invention is illustrated in FIG. 3. This embodiment includes a plurality of spray nozzles 16 disposed in alignment with the gap between a single pair of opposed collector rolls 18. The rolls are mounted in a frame 20. A motor 22 on the frame drives a belt 24, which passes over a pulley on the end of the shaft for the lower roll 18, and the shaft for the upper roll 18 is connected with the lower roll by a cross belt 26. Thus, the rolls 18 rotate in opposite directions when the motor 22 is operating.
The positional relationships between the several nozzles 16. are such that the spray patterns 30 from adjacent nozzles overlap in the collection zone. With this arrangement, a wide non-woven fabric 32 is produced during operation of the equipment. This fabric 32 is similar to the fabric described above in connection with FIG. I inthe sense that it is made up of surface layers connected together by bridging fiber components. In the widthwise direction the fabric 32 may be substantially uniform from zone to zone across the fabric or it may be characterized by zones that are different from one another.
Transverse uniformity is achieved when the overlap between the spray patterns from adjacent ones of the nozzles 16 is sufiicient to assure delivery of substantially the same amount of filamentary material to all portions of the collector zone. On the other hand, Where density variations in the transverse direction are desired, the overlap between adjacent spray patterns from the nozzles 16 may be such as to cause the delivery of filamentary material to one portion of the collector to be greater than the delivery of filamentary material to another portion thereof.
Still other effects may be achieved in the embodiment of FIG. 3 by supplying fiber-forming materials having different characteristics to various ones of the several nozzles 16, and/or by using nozzles having extrusion orifices of different sizes or different rates of delivery. The spray patterns of several nozzles 16 may overlap to the extent of intermingling filaments during formation of the mat or fabric. Different materials may be sprayed simultaneously from the nozzles to produce a fabric having a uniform dispersion of filaments of different materials. The nozzles may be arranged along an axis perpendicular to the width dimension of the gap between the collector rolls, or any other suitable arrangement of nozzles may be used. By arranging a plurality of nozzles, side by side along an axis parallel to the width of the gap, a non-woven fabric 32 may be produced that is characterized by the presence of longitudinally extending portions or stripes having different visual or structural properties. For example, in some applications for the high bulk non-woven fabrics of this invention it is desirable that the fabrics be provided with a defined flex-zone susceptible of being bent more readily than other portions of the fabric. Such a zone can be formed by spray spinning from one of the nozzles 16 filamentary material of significantly smaller average denier than the filamentary material issuing from the other nozzles 16.
Although the collector units in the embodiment described above have been shown as including opposed rolls having smooth surfaces, it will be understood that the invention is not limited to this particular form. Suitable collector surfaces may be provided by endless belts, webs or the like, and the collector surfaces may be rough or provided with protruding portions or embossed patterns. Also, laminated products may be formed by collecting the filamentary material directly upon sheets or webs passed over one or both of the collector rolls and causing the filamentary material to adhere to such sheets or webs, as by heating or bonding treatments.
In the embodiment illustrated in FIG. 4, an endless belt 34 is mounted over rolls 36 and 38 and over an idler roll 40 which supports the intermediate portion of the belt 34. An opposing belt 42 is mounted between the rolls 44 and 46 and passes over an idler roll 48. Presser rolls 49 are mounted adjacent the idler rolls 40 and 48 in 6 position to bear against and guide the exterior surfaces of the belts 34 and 42.
A spray spinning nozzle 50 corresponding to the nozzle 2 in FIG. 1 is positioned opposite the gap between the belts 34 and 42 in the zone of the rolls 36 and 44. Collection of the filamentary material issuing from the nozzle 50 takes place in much the same manner as in FIG. 1. Portions of the filamentary material are deposited directly upon the surfaces of the belts 34 and 42 and other portions bridge back and forth across the gap. As the rolls rotate in the directions indicated by the arrows, the collected material is removed from the collection zone in the form of a non-woven fabric structure.
In the area between the front rolls 36 and 44 and the idler rolls 40 and 48, the fiber contacting flights of the belts 34 and 42 are substantially parallel. These surfaces maintain the newly formed non-woven fabric to the dimension of the gap and serve to minimize the mechanical loads imposed on the material.
The non-woven fabric product delivered by the belts 34 and 42 in the zone of the idler rolls 40 and 48 is similar to the product 10 produced as described in connection with FIG. 1, and this product may be used as such if desired. However, FIG. 4 illustrates an additional operation that may be carried out in forming other novel products in accordance with the invention. Severing means 52 is disposed between the belts 34 and 42 just beyond the idler rolls 40 and 48. This severing means 52 may be in the form of a stationary cutter blade, a reciprocating saw or blade, a band saw, or other suitable fiber severing device.
The level of the severing means 52 is such that it contacts the fiber components bridging the vertical space between the surface layers of the fibrous body being advanced by the belts 34 and 42. The severance of these bridging components across the entire width of the body yields two separate fabrics 54. These move with the diverging flights of the belts 34 and 42 in the zone between the idler rolls 40 and 48 and the back rolls 38 and 46, and they are individually guided away by suitable means 55 for separate collection.
Each of the non-woven fabrics S4 is pile-like in character. The surface layer of the filamentary material deposited on one of the belts of the collector constitutes a firm backing structure 56, and the severed portion 57 of the bridging fiber components extends from the backing in flexible pile-like configurations. These non-woven pile; like fabrics may be produced economically and they are suitable for use in many of the environments where conventional pile fabrics have been employed heretofore.
In producing these pile-like fabrics it is not essential that a belt-type collector unit be employed. Apparatus having roll-type collector units as shown in FIGS. 1-3 can be used for the production of pile fabrics by disposing suitable severing means downstream of the gap between the rolls. Generally, however, it will be found preferable to utilize a belt-type collector, because belts such as those shown at 34 and 42 in FIG. 4 provide relatively large surface areas for frictionally advancing the fibrous assembly against the severing means 52.
Still other aspects of the invention are illustrated in connection with FIGS. 5-7 of the drawings. FIG. 5 illustrates schematically an apparatus setup in which relative lateral movement is effected as between spray spinning nozzle means and a collector unit.
A pair of opposed collector rolls 58 are disposed in front of spray spinning means 60, with the spray pattern 62 from the nozzle 60 intersecting the gap between the rolls 58. The rolls 58 are mounted for rotation in a frame 64, and the frame 64 is carried by rails 66. The rolls 58 are relatively long, as compared with the diameter of the spray pattern 62 at the collection zone. However, the frame 64 is shifted back and forth along the rails 66 to position different portions of the roll surfaces in the path of the filamentary material issuing from the nozzle means 60.
The traversing motion of the rolls 58 may be accomplished through the use of any suitable drive means. In FIG. the drive means has been illustrated as including a link 68 pivotally connected at one of its ends to a pin 70 projecting from a belt 72 and at its other end to a bracket 74 on the frame 64. The belt 72 is disposed beneath the level of the frame 64 and is trained about rolls 76 and 78. The roll 78 is driven from a motor 80 through suitable coupling means such as a belt 82. Upon operation of the motor 80, the roll 78 is rotated to move the belt 72 through an endless path. As the pin 70 moves along the belt path, the frame 64 traverses back and forth along the rails 66 in front of the nozzle 60.
In this embodiment, it is preferred that a substantial degree of bonding at crossover points between contacting filament sections be achieved in the collection zone. This normally presents no difficulty because it usually is feasible to regulate the extrusion temperature and/or the spacing between the nozzle 60 and the collector rolls 58 so that the filamentary material reaches the collection zone while surface portions thereof are still sufficiently tacky to permit self-bonding at crossover points. However, a suitable binder or plasticizer composition may be sprayed into the collection zone along with the filamentary material if desired.
As the zone of intersection between the spray pattern 62 from the nozzle 60 and the collection rolls 58 shifts back and forth across the width of the collection unit, a series of thin sheetlike fibrous subassemblies 84 are formed. Each of the subassemblies is generally U-shaped in configuration, as suggested in FIG. 6, and within each sheet the filament is randomly arrayed in the sense that, if the U-shaped subassembly were flattened into a plane, incremental portions of the filament would be found extending in substantially all directions within that plane.
Of course, the U-shaped subassemblies 84 formed on successive traverses of the collector units are not entirely separate from each other. At the end of one traversing motion and the beginning of the next traversing motion, only a single body of filamentary material is collected, so that successive ones of the subassemblies 84 actually are united at the lateral margins of the fabric. This effect ordinarily is a desirable one, but in those instances where a high degree of widthwise product uniformity is required, the lateral margins of the fabric may be trimmed off.
The upper and lower end portions 86 of adjacent U- shaped subassemblies overlap substantially. These are interentangled somewhat and are packed together to form the surface layers at the top and bottom of the product collected. Portions of at least three and preferably five or more of the subassemblies 84 should be present at any given vertical cross section through one of the surface layers. In these surface layers, the fiber components are generally parallel to the faces of the fabric.
The mid-portions 88 of adjacent ones of the U-shaped subassemblies 84 are spaced apart from each other. This effect is indicated in FIG. 6 and in the photograph designated FIG. 7. The amount of the spacing is subject to variation, depending upon the characteristics desired in the products produced. Control over the spacing between the mid-portions 88 of successive U-shaped subassemblies 84 may be effected by suitable regulation of the surface speeds of the collector rolls 58 in relation to the rate of traverse of the rolls along the rails 66.
The mid-portions 88 of the subassemblies extend at angles to the faces of the non-woven fabrics. Thus, although the fiber components are randomly arrayed within the individual subassemblies 84, the non-Woven fabric as a whole exhibits different fiber orientations in different zones across the thickness of the fabric. That is to say, the predominant orientation of the fiber components in the surface layers is parallel to the faces of the fabric, while the predominant fiber orientation in the middle of the fabric is at an angle to the fabric faces. This angle varies, of course, from 90 on down as one follows a U-shaped 8 subassembly from its mid-point toward a surface layer of the fabric.
Fabrics of the type illustrated in FIG. 7 may be used as such or they may be subjected to further treatments. Particularly interesting results may be obtained, for example, by slitting a fabric of this type through the midportions 88 of the U-shaped subassemblies. This slitting action may be carried out as described above in connection with FIG. 4.
Each of the two fabrics resulting from the slitting operation is characterized by a base or backing structure having a plurality of leaf-like assemblies of fiber components protruding therefrom. The leaf-like bodies may be flexed independently of each other in a manner somewhat analogous to that of the pile of pile fabrics of a more conventional nature. However, the transverse continuity of the leaves gives these fabrics structural properties not heretofore attainable.
An example will serve to further illustrate the invention. This example outlines conditions used in the production of a non-woven fabric adapted to be employed as a pad under a carpet.
EXAMPLE Polypropylene pellets (Hercules Pro-fax 6423) were fed to a Modern Plastics Machinery extruder (1" x 24") having three zones maintained at 205 C., 275 C. and 335 C., respectively, and extruded through a nozzle having a circular orifice of 0.028 inch diameter at a material temperature of about 332 C. The nozzle included three 0.082 inch ports disposed annularly about the orifice, directing streams of steam along paths the axes of which converged toward but did not intersect the extended axis of the extrusion orifice, the closest point to convergence lying about 1 inch from the orifice. The steam had a line pressure of 16 p.s.i.g. and a temperature of 410 C.
The ports were spaced about apart and the axes were arranged to provide an opening of about inch in diameter therebetween at the point of closest convergence, through which the extrudate passed. The extrudate was thereupon attenuated and whipped about with little or no breakage, and taken up While still at least tacky and capable of self-bonding at a point 8 /2 inches from the die orifice on a pair of rolls of 4 inch diameter, counterrotating at about 0.11 r.p.m. and providing a /2 inch nip therebetween through which the material passed in a band of about 3 inches width.
About 1 lb./hr. of material was extruded and taken up as about a 25 oz./yd. batting containing principally endless continuous filament ranging in diameter from about 15 to about 55 microns with the changes in diameter having a relatively long period on the order of several inches. The average diameter was about 24 microns, indicating some preponderance of the lower diameters.
The resulting fabric had the firmness, deformability and resilience qualities required of carpet underlayments.
Of course, in normal production operations it is desirable to produce carpet padding material in wide strips. A suitable carpet underlay may be provided as 4 x 8 foot sheets or as a continuous matting of e.g., 9 feet width rolled about 4 to 6" cores, by utilizing a multiplicity of spray nozzles or traversing the take-up surface. The underlayment may also be sprayed directly onto a carpet backing with a suitable binder or may even constitute the secondary backing itself. Such an embodiment is particularly desirable where the carpet backing comprises a similar synthetic polymer such as polypropylene as in the woven form described in US. Pat. 3,110,905.
The products of this invention are suitable for many other uses. Since the bulky structures are produced directly from an extrusion operation, they are relatively inexpensive. Furthermore, the structures produced in accordance with this invention do not necessarily contain any adhesive and therefore may be more resistant to solvent action than conventional non-woven fabrics. The
unsevered fabric may be used for insulation, ceiling tile, air filters and other articles. The pile-like structures produced from the severed fabric may be used for low cost floor covering, in clothing apparel, and other articles.
While this invention has been illustrated and described in several embodiments, it is recognized that variations and changes may be made therein without departing from the invention as set forth in the claims.
What is claimed is:
1. A method of making non-woven fabrics comprising extruding melted thermoplastic material to form a substantially continuous filament, projecting said filament in a longitudinal direction and in a random swirling pattern toward a gap between an opposed pair of spaced-apart moving collecting surfaces; and collecting the filamentary material in a zone extending across the path of the projected filament and partially occupied by convergent portions of the pair of moving collection surfaces so oriented with respect to each other as to leave a gap therebetween, the filamentary material being collected in the form of spaced-apart first and second surface layers respectively adjacent said collection surfaces and bridging portions between said layers, with the substantially continuous filament passing randomly through said surface layers and bridging portions.
2. The process according to claim 1 including moving said collection surfaces toward said gap at a uniform rate.
3. The process according to claim 1 including projecting a second thermoplastic, substantially continuous filament in a longitudinal direction spaced laterally from but generally parallel to said first-mentioned filament and in a random turbulent pattern overlapping a portion of said first-mentioned filament.
4. The process according to claim 3 wherein said secnd filament has different characteristics from those of said first-mentioned filament.
5. The process according to claim 2 including reciprocally displacing said filament pattern laterally along said gap whereby a fabric having a greater width than said pattern is produced.
6. The process according to claim 5 wherein said displacing is accomplished by reciprocating said collection surfaces laterally relative to said filament pattern along said gap.
7. A process for making a non-woven fabric comprising spray spinning thermoplastic filamentary material toward a gap between an opposed pair of spaced apart collectors,
depositing on one of said collectors a first layer of closely packed filamentary material having a thickness no greater than one-third the width of the gap between the collectors,
depositing on the other of said collectors a second layer of closely packed filamentary material having a 10 thickness no greater than one-third the width of the gap between the collectors, and
collecting the remaining filamentary material between said first and second layers in the form of a core in which the filamentary material is less closely packed than in said first and second layers.
8. The process according to claim 5 wherein said filamentary material in said first and second layers is deposited generally parallel to the surfaces of the respective layers, and said filamentary material between said layers is generally inclined relative to the surfaces of said layers.
9. The process according to claim 7 wherein said filamentary material contacts said surfaces in a pattern extending across said gap, and including reciprocally displacing said pattern later-ally along said gap to produce a fabric having a width greater than said pattern.
10. A process for making non-woven fabrics comprising extruding melted thermoplastic material through an orifice to form a substantially continuous filament stream, directing a plurality of high velocity gas streams generally longitudinally of said filament stream, to attenuate the filament stream and causing a swirling movement of said filament stream about the axis of said orifice,
collecting said filament stream on a pair of surfaces defining a gap therebetween, said filament stream being deposited on said surfaces in the form of surface layers joined together by continuous filament portions between said layers, and
advancing said surfaces in a direction away from said orifice to draw filament portions collected on said surfaces through said gap while maintaining said gap at a greater thickness than the combined thickness of said surface layers whereby a continuous fabric is formed having a center portion with a lower density of filament portions than in said layers.
11. The process according to claim 10 including severing said fabric between said surface layers, and separating said severed mats to form a non-woven fabric having randomly oriented upstanding filament portions on one side.
References Cited UNITED STATES PATENTS 3,509,009 4/1970 Hartmann 156-l8l 3,505,155 4/1970 Balch et al. 156--181 3,423,266 1/ 1969 Davies et a1. 156181 3,314,840 4/ 1967 Lloyd et al. 156167 3,511,742 5/1970 Rasmussen 161-409 3,010,508 11/1961 Wilson et al. 156-254 DANIEL J. FRITSCH, Primary Examiner US. Cl. X.R.
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US3860370A (en) * 1972-06-16 1975-01-14 Continentale Linoleum Union Be Apparatus for the manufacture of fibers
US4128678A (en) * 1977-04-12 1978-12-05 Fiberglas Canada Limited Heat insulating material and method of and apparatus for the manufacture thereof
US4135903A (en) * 1975-08-20 1979-01-23 Nippon Sheet Glass Co., Ltd. Method for producing fibers from heat-softening materials
US4212692A (en) * 1977-05-06 1980-07-15 Akzona Incorporated Matting article with process and apparatus for its production
US4247270A (en) * 1979-01-29 1981-01-27 Iwka-Industrie-Werke-Karlsruhe Augsburg Ag Apparatus for the continued manufacture of staple fibers from thermoplastic materials
US4267002A (en) * 1979-03-05 1981-05-12 Eastman Kodak Company Melt blowing process
DE3041088A1 (en) * 1979-11-01 1981-05-14 Toa Nenryo Kogyo K.K., Tokyo LEATHERETTE
DE3041089A1 (en) * 1979-11-01 1981-05-21 Toa Nenryo Kogyo K.K., Tokyo NONWOVEN FABRIC
US4375446A (en) * 1978-05-01 1983-03-01 Toa Nenryo Kogyo Kabushiki Kaisha Process for the production of a nonwoven fabric
US4440700A (en) * 1981-04-28 1984-04-03 Polymer Processing Research Institute Ltd. Process for collecting centrifugally ejected filaments
US4995928A (en) * 1988-10-31 1991-02-26 Sabee Reinhardt N Method and apparatus for forming and transporting elastic ribbons
US5145727A (en) * 1990-11-26 1992-09-08 Kimberly-Clark Corporation Multilayer nonwoven composite structure
US5149576A (en) * 1990-11-26 1992-09-22 Kimberly-Clark Corporation Multilayer nonwoven laminiferous structure
US5230851A (en) * 1989-01-31 1993-07-27 The Procter & Gamble Company Process of manufacturing a refastenable mechanical fastening system
WO2000066824A1 (en) * 1999-04-30 2000-11-09 Kimberly-Clark Worldwide, Inc. Controlled loft and density nonwoven webs and method for producing
US6372076B1 (en) 1999-09-28 2002-04-16 L&P Property Management Company Convoluted multi-layer pad and process
GB2387180A (en) * 1999-04-30 2003-10-08 Kimberly Clark Co A lofted non-woven material with z orientated fibres
US20040097155A1 (en) * 2002-11-15 2004-05-20 3M Innovative Properties Company Fibrous nonwoven web
DE102012018481A1 (en) * 2012-09-19 2014-03-20 Sandler Ag insulation
US10961644B2 (en) 2014-01-29 2021-03-30 Biax-Fiberfilm Corporation High loft, nonwoven web exhibiting excellent recovery

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3860370A (en) * 1972-06-16 1975-01-14 Continentale Linoleum Union Be Apparatus for the manufacture of fibers
US4135903A (en) * 1975-08-20 1979-01-23 Nippon Sheet Glass Co., Ltd. Method for producing fibers from heat-softening materials
US4128678A (en) * 1977-04-12 1978-12-05 Fiberglas Canada Limited Heat insulating material and method of and apparatus for the manufacture thereof
US4212692A (en) * 1977-05-06 1980-07-15 Akzona Incorporated Matting article with process and apparatus for its production
US4375446A (en) * 1978-05-01 1983-03-01 Toa Nenryo Kogyo Kabushiki Kaisha Process for the production of a nonwoven fabric
US4247270A (en) * 1979-01-29 1981-01-27 Iwka-Industrie-Werke-Karlsruhe Augsburg Ag Apparatus for the continued manufacture of staple fibers from thermoplastic materials
US4267002A (en) * 1979-03-05 1981-05-12 Eastman Kodak Company Melt blowing process
DE3041088A1 (en) * 1979-11-01 1981-05-14 Toa Nenryo Kogyo K.K., Tokyo LEATHERETTE
DE3041089A1 (en) * 1979-11-01 1981-05-21 Toa Nenryo Kogyo K.K., Tokyo NONWOVEN FABRIC
US4440700A (en) * 1981-04-28 1984-04-03 Polymer Processing Research Institute Ltd. Process for collecting centrifugally ejected filaments
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