US3701484A - Apparatus and process for suspending solids - Google Patents

Apparatus and process for suspending solids Download PDF

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US3701484A
US3701484A US91276A US3701484DA US3701484A US 3701484 A US3701484 A US 3701484A US 91276 A US91276 A US 91276A US 3701484D A US3701484D A US 3701484DA US 3701484 A US3701484 A US 3701484A
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panels
nozzles
posts
discharge
slurry
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Howard Gleason Donovan
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Johns Manville Corp
Johns Manville
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C19/00Other disintegrating devices or methods
    • B02C19/06Jet mills
    • B02C19/065Jet mills of the opposed-jet type

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  • a size reduction method and apparatus are provided PP N94 91,276 in which a pair of coaxially aligned opposing nozzles impel liquid streams toward one another between a ..241 5 241 39 P of Panels that form a zone that extends 1,1,, h m [58] Field 241/4 5 39 40 rality of posts protrude into the narrow zone.
  • Rafe Cited reducing the diameter of fibers, such as asbestos, UNITED STATES TENT V and reducing the particle size of particulate materials l ts dth lik 2,974,886 3/1961 Nagel ..241/39 e 8 1,046,290 12/ 1912 Granville ..241/40 12 Claims, 5 Drawing Figures P'A'TENTED um 31 m2 2 Sheets-Sheet 1 INVENTOR HOWARD GLEASON DONOVAN F IG. 2
  • Suspension fertilizers employ a variety of conventional suspending agents, such as clay. Recently, it has been discovered that asbestos fibers having a relatively short fiber length are particularly desirable for use as a suspending agent in view of the low cost of such fibers and the stability of the suspensions they produce. These asbestos fibers can be derived from asbestos ore or even the tailings remaining after a majority of the fiber is removed from asbestos ore. v,
  • buoyancy is a measure of the period of time required for settlingout of the suspended solids ingredients of the suspension.
  • buoyancy is related directly to particle size. Accordingly, the mixing means for clay stabilized suspensions should be one which will effectively reduce the particle size of the clay.
  • buoyancy is not related solely to particle size, and is more directly affected by fiber diameter.
  • a suspending agent including asbestos fibers For a suspending agent including asbestos fibers, however, buoyancy is not related solely to particle size, and is more directly affected by fiber diameter.
  • buoyancy For example, for asbestos containing material in which up to about 20 percent by weight of the asbestos fibers normally range in length between about (minus) 14 mesh (McNett standard) down to about 1 micron (equivalent to about 20,000 mesh), buoyancy is not substantially increased by the breaking of the asbestos fibers into shorter lengths. In contrast, buoyancy is substantially increased by further decreasing the average diameter of the fibers.
  • Paper'making is another example of a technical area where it is desirable to reduce the size of particulate matter and open fibers.
  • Various size reduction apparatus. and methods are used to condition the solids present in the slurries that are fed to the commonly used Fourdrinier and cylinder paper making machines.
  • an object of this invention is to provide a process and apparatus that possess improved efficien-' particulate matter, such as clay, in a liquid slurry.
  • the invention provides a method for reducing the size of solid particulate matter in a liquid slurry.
  • Two streams of slurry under a pressure of 500 to 2,000 psi are directed towards each other along a common axis at a high velocity to disintegrate the particles.
  • the merged impacted streams of slurry are then passed at a high velocity through a narrow zone extending radially outwardly from the common axis and into contact with solid posts extending into the zone to further disintegrate the particles.
  • the method of the invention is particularly useful in reducing the average diameter of asbestos fiber.
  • the invention also provides an improvement in apparatus for reducing the size of solid particulate matter in a liquid slurry that is fed to the apparatus under pressure.
  • the apparatus includes a pair of aligned nozzles having a common discharge axis.
  • the nozzles have spaced discharge ends for directing a discharge of slurry toward each other to disintegrate the particulate matter.
  • the improvement comprises the combination of elements described below.
  • a pair of spaced panels extend transversely of the common axis of the nozzles. The panels form a narrow zone which extends radially outwardly from the common axis and is in fluid flow communication with the discharge ends of said nozzles.
  • Frame means are provided for fixing the position of each of the panels with the panels mounted on the frame means.
  • a plurality of posts are connected to at least one of the panels and extend into the narrow zone between the panels. Further disintegration of particulate matter passing outwardly at a high velocity from the discharge nozzles occurs when the particulate matter hits the posts.
  • the posts extending across the narrow zone, are effective to dramatically increase the size reduction capability of the apparatus, with a negligible increase in the power requirements for the increase in size reduction capability that results.
  • the apparatus and method are particularly useful in the opening of asbestos fibers for inclusion in suspension fertilizers, because the diameter of the fibers is efficiently reduced, as is the particle size of other inorganic materials usually present in such fertilizers.
  • the invention also possesses advantages that make its practice useful in manufacturing paper and a variety of other products that have a slurry formed at some stage of their manufacturing process.
  • FIG. 1 is a diagrammatic cross-sectional elevation of a typical embodiment of the apparatus of this invention, and also illustrates a container, a pumping means, and conduits for cycling and recycling a slurry through the apparatus.
  • FIG. 2 is an exploded perspective view of the apparatus of FIG. 1 with only one of the six posts illustrated.
  • FIG. 3 illustrates another embodiment of the invention.
  • FIGS. 4A and 4B illustrate the interior faces of the panels of two additional embodiments of the invention and show the posts in cross-section.
  • the apparatus and process of this invention are particularly useful in manufacturing a suspension fertilizer.
  • the process and apparatus of the invention intimately mix a solids-containing slurry, and further reduce the particle size of the suspending agent, such as clay or asbestos fibers. Further, the apparatus and method are unexpectedly effective in obtaining improved suspensions by reducing the diameter of asbestos fibers.
  • the asbestos fibers present in a composition to be suspended range in length from -l4 mesh (Mc- Nett) down to a composition in which about 20 percent of the fibers are 1 micron or less in length.
  • the asbestos fibers range in length from about 30 mesh to about +400 mesh.
  • Preferred suspension fertilizers are obtained when the asbestos fibers are present from about 1.5 to about 30 percent by weight of the total weight of the slurry with total solids preferably ranging from about 45 to 60 percent by weight of the slurry.
  • a pair of aligned nozzles are provided having a common discharge axis.
  • the discharge ends of the nozzles are spaced close together so that the streams of slurry which they emit blast into each other at a high velocity to disintegrate the particulate matter in the stream.
  • a pair of nozzles generally 10 and 12 are formed by openings 23 in a pair of spaced panels 20 and 22.
  • Nozzles l0 and 12 are coaxially aligned along a common axis 14 and have their discharge ends 16, illustrated in FIG. 2, closely spaced for directing a discharge of slurry towards each other.
  • the pair of spaced panels 20 and 22 extend transversely of the common axis 14. As illustrated in FIG. 2, a threaded nipple 25 is welded to the exterior surface of each of panels 20 and 22 to provide a convenient means for introducing slurry to the nozzles, and to permit mounting the panels within a container 26.
  • Zone 24 is in fluid flow communication with the discharge ends 16 of nozzles 10 and 12 and extends radially outwardly from common axis 14.
  • the streams of slurry are free to flow radially outwardly, but in a narrow constricted flow path so that the slurry retains some of its dynamic energy after the discharged streams of slurry impact upon one another.
  • the apparatus of the invention is mounted within container 26.
  • Container 26 functions as both a slurry collection reservoir and also as a shield to prevent loss of slurry as the slurry is moved outwardly from between panels 20 and 22.
  • a pump means 30 is provided to supply slurry under pressure to each of the nozzles 10 and 12 through supply lines 32 and 34, respectively. The'terminal portions of the supply lines also serve as a means for mounting the apparatus of the invention in container 26.
  • novel apparatus and process of this invention do not require extremely high pump pressures to obtain substantial size reduction and mixing results.
  • high elevated pressures above 2,000 psi, can be used in the process and apparatus of the invention.
  • Frame means are provided for fixing the position of the panels with respect to each other.
  • the frame means also function as posts that are impacted by the slurry.
  • the frame means include a plurality of bolts 38 having a threaded end. Bolts 38 extend through holes 40 and 42 in panels 20 and 22, respectively. A nut 44 is screwed on the threaded end of each bolt to hold the panelspressive force on the panels.
  • the frame means also form the posts that perform an important impact size reduction and mixing function as described
  • a plurality of posts are provided which are each fixed to at least one of the panels. Each post extends into the narrow zone between the panels and further disintegrates particulate matter that strikes the post during passage outwardly through the zone.
  • the posts add significantly to the size reduction capability of a pair of opposed nozzles without causing a large increase in power requirements. Further, the posts are unexpectedly efficient in reducing the diameter of short lengths of inorganic fibers, such as asbestos fibers.
  • the posts comprise bolts 38 and spacing washers 46 which extend across narrow zone 24 between. panels and 22.
  • Spacing washers 46 preferably are formed of a hard abrasion resistant material, such as tungsten carbide. Washers 46 are removable from bolts 38 when the apparatus is disassembled to permit replacement of the washers after they become excessively abraded during use.
  • the cross sectional shape of the posts can be varied and may include, square, triangular, hexagonal, or irregular cross sectional shapes.
  • At least two posts are present in the apparatus of the invention, and the preferred number of posts per pair of nozzles is about 6-12. More than twelve posts can be utilized, if desired. When very large numbers of posts are used, however, the posts may create an undesirably large pressure drop across the narrow zone.
  • FIG. 3 illustrates another embodiment of the invention in which a pair of opposing panels 50 and 52 each have concave adjacent faces and include a plurality of openings 54 which do not extend all the way across the panels and a pair of openings which do extend all the way across the thickness of the panels for the insertion of a plurality of bolts 56.
  • the depth of the openings 54 in the adjacent faces of the panels and the length of posts 58 which are inserted in openings 54 maintain a predetermined amount of spacing between the panels.
  • Panels 50 and 52 include threaded openings (not numbered) and nozzle members 60 and 62 include a male threaded portion which permits screwing the nozzles into position for regulating the distance between opposing nozzles.
  • This threaded construction also provides a fluid-sealing relationship between the outer wall of the nozzles and the threaded openings in panels 50 and 52.
  • the discharge opening of the nozzles, the distance between the opposing nozzles, and the distance between any particular post and the outer diameter of the nozzles must each be sufliciently larger than any particles of the slurry to avoid any significant amount of clogging. On. the other hand, it is necessary that these distances and spacings be small enough to create and preferably maximize the impact of the slurry from one nozzle against the slurry from the opposing nozzle,
  • the diameter of the conduits and the nozzle apertures, the distance between the ends of the nozzles, the distances between the nozzles and adjacent posts, and the distance between any one or more posts range between about one thirty-second inch up to about three-fourths inch for preferred apparatus which are particularly useful in suspending fertilizers containing clay or asbestos suspending agents.
  • the outer diameter of the posts is up to about five-eighths inch and the distance between opposing faces of the panels ranges from about three-eighths inch adjacent the nozzles to about one-sixteenth inch at the edges of the panels.
  • a positive-displacement pumping means is provided for producing a liquid slurry pressure ranging from about 500 psi to about 2,000 ps1.
  • FIGS. 4A and 4B illustrate respectively the interior faces of the panels of two additional embodiments of the invention.
  • Each panel includes a plurality of pairs of opposing nozzles extending from the interior face of the panel.
  • three nozzles 70, 72, and 74 and a plurality of posts 76 extend from each panel 78.
  • EXAMPLES 1-3 In a series of tests, asbestos ore tailings, (-66 mesh and 30 mesh) are processed through an apparatus constructed in accordance with the invention.
  • a pump provides a line pressure of 500 psi for all tests, and the solids content of the aqueous slurry is maintained at 9 percent.
  • the apparatus used for these tests utilizes nozzles tapered from three-eighths inch id at the inlet to one-fourth inch id. at the discharge end, with the discharge ends spaced approximately one-eighth inch apart.
  • the panels are spaced about one-eighth in. apart.
  • Example 1 In the procedure of Example 1, one bolt clad with two inch tungsten carbide washers is positioned with its center line three-fourths inch from the common axis of the nozzles.
  • Example 2 the general procedure of Example I is repeated using an apparatus having three equally spaced bolts with washers and three bolts without washers.
  • the washers are inch tungsten carbide washers and the bolts are positioned about three-fourths inch from the axis of the nozzles.
  • Three V4 inch bolts without washers in addition to the three bolts described above, are positioned three-sixteenths inch from the center line of the nozzles and equally spaced from each other and from the bolts with washers.
  • Example 3 In the procedure of Example 3, six bolts as described above are utilized with the addition of six 20D nails which are positioned approximately one inch from the center line of the nozzles to give a total of 12 posts on which the slurry impinges.
  • the slurry is fed from a container which is located above the nozzle assembly, and the slurry is permitted to pass through the nozzle assembly only once.
  • Table I The results of the tests run in Examples 1-3 are shown in Table I below, and compared with a control run in which the 9% solids content slurry was run through the same apparatus, except that no posts were provided.
  • the slurry is fed from a container located above the nozzle apparatus and the apparatus is suspended in a porous plastic bag. During the pumping of the slurry, the apparatus becomes submerged in the liquid slurry within the bag.
  • the suspending apparatus becomes submerged in the slurry during the processing procedure.
  • results that are better than those shown in Table I can be expected, because placement of the apparatus below the slurry level creates a back pressure from the surrounding slurry liquid.
  • the back pressure reduces the efficiency of the posts because it reduces the intensity of impact of the slurry against the SS.
  • the apparatus and process of this invention can be advantageously practiced at plants manufacturing suspensions, such as fertilizer suspensions, and can also be practiced advantageously at the job site.
  • the apparatus can be compactly constructed and is simple to operate and maintain which permits this wide range of potential usage.
  • a method for reducing the size of solid particulate matter in a liquid slurry comprising: directing two streams of slurry under a pressure of 500 to 2,000 psi towards each other along a common axis at a high velocity to disintegrate the particles; and passing the merged impacted streams of slurry at a high velocity through a narrow zone extending radially outwardly from the common axis and into contact with a plurality of solid posts extending into the zone to further disinpositioned entirely on the same side of a first plane parallel with and passing through said common axis and at unequal distances therefrom, a portion of each of said two posts lying in a second common plane parallel with and passing through said common axis.
  • each of said posts comprising a pin connecting said panels and a plurality of abrasion resistant washers concentrically mounted on said pin with one face of one washer abutting the interior face of one of said panels and one face of another washer abutting the interior face of the other panel.
  • the apparatus of claim 4 including a container surrounding said panels for collecting the slurry passing radially outwardly from between said panels; and a high pressure displacement pump having its inlet connected to the interior of said container and its outlet connected to the inlet end of said nozzles for pumping slurry to said nozzles.
  • the apparatus of claim 4 including a high pressure displacement pump having its discharge outlet connected to the inlet end of said nozzles.
  • a plurality of posts connected to at least one of said panels and extending into the narrow zone between said panels to further disintegrate particulate matter passing outwardly through said zone at a high velocity from the discharge nozzles, at least two of said posts being positioned entirely on the same side of a first plane parallel with and passing through said common axis and at unequal distances therefrom, a portion of each of said two posts lying in a second common plane parallel with and passing through said common axis.

Abstract

A size reduction method and apparatus are provided in which a pair of coaxially aligned opposing nozzles impel liquid streams toward one another between a pair of panels that form a narrow zone that extends radially outwardly from the axis of the nozzles. A plurality of posts protrude into the narrow zone. These posts increase the size reduction capability of the apparatus and are particularly effective in opening (reducing the diameter of) fibers, such as asbestos, and reducing the particle size of particulate materials such as clay, pigments and the like.

Description

United States Patent Donovan [45] 4 [54] APPARATUS AND PROCESS FOR 238,044 2/1881 Luckenbach et al. ...241/39 X SUSPENDING SOLIDS 1,597,656 8/1926 Morton ..24l/39 Inventor: Howard Gleason Donovan west 2,874,095 2/1959 Boisture et al ..241/40 X field Primary Examiner-Granville Y. Custer, Jr. [73] Assignee: Johns-Manville Corporation, New Attorney-John A. McKinney and Robert M. Krone York, NY. [57] v ABS CT [22] Filed: Nov. 20, 1970 A size reduction method and apparatus are provided PP N94 91,276 in which a pair of coaxially aligned opposing nozzles impel liquid streams toward one another between a ..241 5 241 39 P of Panels that form a zone that extends 1,1,, h m [58] Field 241/4 5 39 40 rality of posts protrude into the narrow zone. These posts increase the size reduction capability of the apparatus and are particularly effective in opening [56] Rafe Cited (reducing the diameter of) fibers, such as asbestos, UNITED STATES TENT V and reducing the particle size of particulate materials l ts dth lik 2,974,886 3/1961 Nagel ..241/39 e 8 1,046,290 12/ 1912 Granville ..241/40 12 Claims, 5 Drawing Figures P'A'TENTED um 31 m2 2 Sheets-Sheet 1 INVENTOR HOWARD GLEASON DONOVAN F IG. 2
ATTORNEY PATENTEUBBTIH m2 3,701,484
2 Sheets-Sheet 2 /6O g@@@ g@@@@ HNV ENTOR HOWARD GLEASON DONOVAN ATTORNEY APPARATUS AND PROCESS FORSUSPENDING SOLIDS FIELD OF THE INVENTION BACKGROUND OF THE INVENTION .There has been a continuing search in connection with a variety of products to find more efficient ways to reduce the size of solid particulate matter and fibers incorporated into liquid slurries. For example, in recent years there has been a trend towards the increased usage of suspension fertilizers. Suspensions offer the advantage of liquid solution fertilizers, such as ease of production and ease of handling and application while at the same time allowing use of low cost raw materials. Accordingly, apparatus for placing fertilizer solids into a suitable suspension have taken on increasedcommercial importance.
Suspension fertilizers employ a variety of conventional suspending agents, such as clay. Recently, it has been discovered that asbestos fibers having a relatively short fiber length are particularly desirable for use as a suspending agent in view of the low cost of such fibers and the stability of the suspensions they produce. These asbestos fibers can be derived from asbestos ore or even the tailings remaining after a majority of the fiber is removed from asbestos ore. v,
To create suspension fertilizers; it is desirable to have an inexpensive mixing means which efficiently suspends the suspending agent and other ingredients of the fertilizer in a liquid carrier. The efficiency of the suspending agent in maintaining a suspended composition is normally referred to in terms of buoyancy, which is a measure of the period of time required for settlingout of the suspended solids ingredients of the suspension. For a suspending agent such as clay, buoyancy is related directly to particle size. Accordingly, the mixing means for clay stabilized suspensions should be one which will effectively reduce the particle size of the clay.
For a suspending agent including asbestos fibers, however, buoyancy is not related solely to particle size, and is more directly affected by fiber diameter. For example, for asbestos containing material in which up to about 20 percent by weight of the asbestos fibers normally range in length between about (minus) 14 mesh (McNett standard) down to about 1 micron (equivalent to about 20,000 mesh), buoyancy is not substantially increased by the breaking of the asbestos fibers into shorter lengths. In contrast, buoyancy is substantially increased by further decreasing the average diameter of the fibers.
In the terminology employed in the asbestos fiber industry, when asbestos fibers are further split lengthwise of the fibers, the process is called opening the fibers. In this opening procedure, the average fiber diameter is decreased.
After a suspension fertilizer has been placed in suspension at a manufacturing facility, the suspension has only a limited storage life. Therefore, there also exists a need for an inexpensive and effective homogenizer which can be operated at relatively low pressures for use in thefield to permit users of suspen-.
sion fertilizers to easily resuspend the solids in suspension fertilizers.
Paper'making is another example of a technical area where it is desirable to reduce the size of particulate matter and open fibers. Various size reduction apparatus. and methods are used to condition the solids present in the slurries that are fed to the commonly used Fourdrinier and cylinder paper making machines.
OBJECTS OF THE INVENTION Accordingly, an object of this invention is to provide a process and apparatus that possess improved efficien-' particulate matter, such as clay, in a liquid slurry.
' Additional objects and advantages of the invention will be set forth in part in the description which follows,
and in part will be obvious from the description, or may be learned by practiceof the invention.
SUMMARY OF THE INVENTION The invention provides a method for reducing the size of solid particulate matter in a liquid slurry. Two streams of slurry under a pressure of 500 to 2,000 psi are directed towards each other along a common axis at a high velocity to disintegrate the particles. The merged impacted streams of slurry are then passed at a high velocity through a narrow zone extending radially outwardly from the common axis and into contact with solid posts extending into the zone to further disintegrate the particles. The method of the invention is particularly useful in reducing the average diameter of asbestos fiber.
The invention also provides an improvement in apparatus for reducing the size of solid particulate matter in a liquid slurry that is fed to the apparatus under pressure. The apparatus includes a pair of aligned nozzles having a common discharge axis. The nozzles have spaced discharge ends for directing a discharge of slurry toward each other to disintegrate the particulate matter. The improvement comprises the combination of elements described below. A pair of spaced panels extend transversely of the common axis of the nozzles. The panels form a narrow zone which extends radially outwardly from the common axis and is in fluid flow communication with the discharge ends of said nozzles. Frame means are provided for fixing the position of each of the panels with the panels mounted on the frame means. A plurality of posts are connected to at least one of the panels and extend into the narrow zone between the panels. Further disintegration of particulate matter passing outwardly at a high velocity from the discharge nozzles occurs when the particulate matter hits the posts.
The posts, extending across the narrow zone, are effective to dramatically increase the size reduction capability of the apparatus, with a negligible increase in the power requirements for the increase in size reduction capability that results. The apparatus and method are particularly useful in the opening of asbestos fibers for inclusion in suspension fertilizers, because the diameter of the fibers is efficiently reduced, as is the particle size of other inorganic materials usually present in such fertilizers. The invention also possesses advantages that make its practice useful in manufacturing paper and a variety of other products that have a slurry formed at some stage of their manufacturing process.
DESCRIPTION OF THE DRAWINGS Of the drawings:
FIG. 1 is a diagrammatic cross-sectional elevation of a typical embodiment of the apparatus of this invention, and also illustrates a container, a pumping means, and conduits for cycling and recycling a slurry through the apparatus.
FIG. 2 is an exploded perspective view of the apparatus of FIG. 1 with only one of the six posts illustrated.
FIG. 3 illustrates another embodiment of the invention; and
FIGS. 4A and 4B illustrate the interior faces of the panels of two additional embodiments of the invention and show the posts in cross-section.
DETAILED DESCRIPTION OF THE INVENTION The apparatus and process of this invention are particularly useful in manufacturing a suspension fertilizer. The process and apparatus of the invention intimately mix a solids-containing slurry, and further reduce the particle size of the suspending agent, such as clay or asbestos fibers. Further, the apparatus and method are unexpectedly effective in obtaining improved suspensions by reducing the diameter of asbestos fibers.
Usually, the asbestos fibers present in a composition to be suspended range in length from -l4 mesh (Mc- Nett) down to a composition in which about 20 percent of the fibers are 1 micron or less in length. Preferably, the asbestos fibers range in length from about 30 mesh to about +400 mesh. Preferred suspension fertilizers are obtained when the asbestos fibers are present from about 1.5 to about 30 percent by weight of the total weight of the slurry with total solids preferably ranging from about 45 to 60 percent by weight of the slurry.
In measuring the asbestos fiber lengths in terms of McNett mesh size, an attempt is made to cause the fibers to be presented with the length of the fiber aligned in a plane parallel to the plane of the screen so that the fibers of greater length than the particular mesh size do not pass through the mesh. Therefore, although the term mesh normally denotes particle size, the expression when used in relation to asbestos fibers relates to fiber length. It should be recognized, however, that as the length of the asbestos fibers being measured becomes shorter it becomes more difficult to align the fibers in a plane parallel to the plane of the screen mesh as the fibers approach the mesh. For example, at about -200 mesh, the McNett measurement of asbestos fibers increasingly reflects particle size, rather than length of fibers because of the increased difiiculty in aligning the fibers with the screen.
In accordance with the apparatus of the invention, a pair of aligned nozzles are provided having a common discharge axis. The discharge ends of the nozzles are spaced close together so that the streams of slurry which they emit blast into each other at a high velocity to disintegrate the particulate matter in the stream. As here embodied, and as illustrated-in FIG. 1, a pair of nozzles generally 10 and 12 are formed by openings 23 in a pair of spaced panels 20 and 22. Nozzles l0 and 12 are coaxially aligned along a common axis 14 and have their discharge ends 16, illustrated in FIG. 2, closely spaced for directing a discharge of slurry towards each other.
The pair of spaced panels 20 and 22 extend transversely of the common axis 14. As illustrated in FIG. 2, a threaded nipple 25 is welded to the exterior surface of each of panels 20 and 22 to provide a convenient means for introducing slurry to the nozzles, and to permit mounting the panels within a container 26.
As illustrated in FIG. 1, panels 20 and 22 form a narrow zone 24 therebetween. Zone 24 is in fluid flow communication with the discharge ends 16 of nozzles 10 and 12 and extends radially outwardly from common axis 14. Thus, the streams of slurry are free to flow radially outwardly, but in a narrow constricted flow path so that the slurry retains some of its dynamic energy after the discharged streams of slurry impact upon one another.
In the embodiment illustrated in FIG. 1, the apparatus of the invention is mounted within container 26. Container 26 functions as both a slurry collection reservoir and also as a shield to prevent loss of slurry as the slurry is moved outwardly from between panels 20 and 22. A pump means 30 is provided to supply slurry under pressure to each of the nozzles 10 and 12 through supply lines 32 and 34, respectively. The'terminal portions of the supply lines also serve as a means for mounting the apparatus of the invention in container 26.
The novel apparatus and process of this invention do not require extremely high pump pressures to obtain substantial size reduction and mixing results. However, such high elevated pressures, above 2,000 psi, can be used in the process and apparatus of the invention.
Frame means are provided for fixing the position of the panels with respect to each other. In the embodimerit illustrated in FIGS. 1 and 2, the frame means also function as posts that are impacted by the slurry. The frame means include a plurality of bolts 38 having a threaded end. Bolts 38 extend through holes 40 and 42 in panels 20 and 22, respectively. A nut 44 is screwed on the threaded end of each bolt to hold the panelspressive force on the panels.
In the embodiment illustrated in FIG. 1, the frame means also form the posts that perform an important impact size reduction and mixing function as described In accordance with the invention, a plurality of posts are provided which are each fixed to at least one of the panels. Each post extends into the narrow zone between the panels and further disintegrates particulate matter that strikes the post during passage outwardly through the zone. The posts add significantly to the size reduction capability of a pair of opposed nozzles without causing a large increase in power requirements. Further, the posts are unexpectedly efficient in reducing the diameter of short lengths of inorganic fibers, such as asbestos fibers.
In the embodiment of the invention illustrated in FIGS. 1 and 2, the posts comprise bolts 38 and spacing washers 46 which extend across narrow zone 24 between. panels and 22. Spacing washers 46 preferably are formed of a hard abrasion resistant material, such as tungsten carbide. Washers 46 are removable from bolts 38 when the apparatus is disassembled to permit replacement of the washers after they become excessively abraded during use.
While the surface of the post or spacing washers that is exposed to impact by the slurry is preferably cylindrical, the cross sectional shape of the posts can be varied and may include, square, triangular, hexagonal, or irregular cross sectional shapes.
At least two posts are present in the apparatus of the invention, and the preferred number of posts per pair of nozzles is about 6-12. More than twelve posts can be utilized, if desired. When very large numbers of posts are used, however, the posts may create an undesirably large pressure drop across the narrow zone.
FIG. 3 illustrates another embodiment of the invention in which a pair of opposing panels 50 and 52 each have concave adjacent faces and include a plurality of openings 54 which do not extend all the way across the panels and a pair of openings which do extend all the way across the thickness of the panels for the insertion of a plurality of bolts 56. The depth of the openings 54 in the adjacent faces of the panels and the length of posts 58 which are inserted in openings 54 maintain a predetermined amount of spacing between the panels. Nozzles 60 and 62-are each formed by a tubular conduit having walls that converge towards the discharge end. Panels 50 and 52 include threaded openings (not numbered) and nozzle members 60 and 62 include a male threaded portion which permits screwing the nozzles into position for regulating the distance between opposing nozzles. This threaded construction also provides a fluid-sealing relationship between the outer wall of the nozzles and the threaded openings in panels 50 and 52.
In the embodiment of FIG. 3, where some of the openings 54 extend merely to a predetermined depth that is less than all the way through the panel, facing washers are not required to maintain the predetermined degree of spacing between opposing faces of the support structure. I
The discharge opening of the nozzles, the distance between the opposing nozzles, and the distance between any particular post and the outer diameter of the nozzles must each be sufliciently larger than any particles of the slurry to avoid any significant amount of clogging. On. the other hand, it is necessary that these distances and spacings be small enough to create and preferably maximize the impact of the slurry from one nozzle against the slurry from the opposing nozzle,
and thereafter against the opposite walls and the posts adjacent to the nozzles.
Normally, the diameter of the conduits and the nozzle apertures, the distance between the ends of the nozzles, the distances between the nozzles and adjacent posts, and the distance between any one or more posts range between about one thirty-second inch up to about three-fourths inch for preferred apparatus which are particularly useful in suspending fertilizers containing clay or asbestos suspending agents. In a particularly preferred embodiment, the outer diameter of the posts is up to about five-eighths inch and the distance between opposing faces of the panels ranges from about three-eighths inch adjacent the nozzles to about one-sixteenth inch at the edges of the panels.-
Preferably, a positive-displacement pumping means is provided for producing a liquid slurry pressure ranging from about 500 psi to about 2,000 ps1.
FIGS. 4A and 4B illustrate respectively the interior faces of the panels of two additional embodiments of the invention. Each panel includes a plurality of pairs of opposing nozzles extending from the interior face of the panel. In the embodiment of FIG. 4A, there are three opposing nozzles 60, 62, and 64 extending from each panel 66 and also a plurality of posts 68. Similarly in FIG. 43, three nozzles 70, 72, and 74 and a plurality of posts 76 extend from each panel 78.
For a clearer understanding of the invention, specific examples of it are set forth below. These examples are illustrative, and are not to be understood as limiting the scope and underlying principles of the invention in any way. All percentages listed in the specification and claims are weight percentages unless otherwise noted.
EXAMPLES 1-3 In a series of tests, asbestos ore tailings, (-66 mesh and 30 mesh) are processed through an apparatus constructed in accordance with the invention. A pump provides a line pressure of 500 psi for all tests, and the solids content of the aqueous slurry is maintained at 9 percent. The apparatus used for these tests utilizes nozzles tapered from three-eighths inch id at the inlet to one-fourth inch id. at the discharge end, with the discharge ends spaced approximately one-eighth inch apart. The panels are spaced about one-eighth in. apart.
In the procedure of Example 1, one bolt clad with two inch tungsten carbide washers is positioned with its center line three-fourths inch from the common axis of the nozzles. In the procedure of Example 2, the general procedure of Example I is repeated using an apparatus having three equally spaced bolts with washers and three bolts without washers. The washers are inch tungsten carbide washers and the bolts are positioned about three-fourths inch from the axis of the nozzles. Three V4 inch bolts without washers, in addition to the three bolts described above, are positioned three-sixteenths inch from the center line of the nozzles and equally spaced from each other and from the bolts with washers.
In the procedure of Example 3, six bolts as described above are utilized with the addition of six 20D nails which are positioned approximately one inch from the center line of the nozzles to give a total of 12 posts on which the slurry impinges.
In each of the examples, the slurry is fed from a container which is located above the nozzle assembly, and the slurry is permitted to pass through the nozzle assembly only once. The results of the tests run in Examples 1-3 are shown in Table I below, and compared with a control run in which the 9% solids content slurry was run through the same apparatus, except that no posts were provided. In each of the tests, the slurry is fed from a container located above the nozzle apparatus and the apparatus is suspended in a porous plastic bag. During the pumping of the slurry, the apparatus becomes submerged in the liquid slurry within the bag.
The results tabulated in Table I show that the presence of multiple posts significantly increases the ability of the apparatus to open asbestos fibers. This increased ability to open asbestos fiber is illustrated by each of the three tests; particle size, bulk density, and surface area. Bulk density is generally recognized as one of the most significant and reliable indicators of improved properties for use as a suspending agent with decreases in bulk density providing increases in suspension capabilities.
It should be noted that in the apparatus used in these examples, the suspending apparatus becomes submerged in the slurry during the processing procedure. In an embodiment such as that illustrated in FIG. 1, where the nozzle assembly is maintained at a location above the slurry level, results that are better than those shown in Table I can be expected, because placement of the apparatus below the slurry level creates a back pressure from the surrounding slurry liquid. The back pressure reduces the efficiency of the posts because it reduces the intensity of impact of the slurry against the SS. It should be recognized that the apparatus and process of this invention can be advantageously practiced at plants manufacturing suspensions, such as fertilizer suspensions, and can also be practiced advantageously at the job site. The apparatus can be compactly constructed and is simple to operate and maintain which permits this wide range of potential usage.
What is claimed is:
1. A method for reducing the size of solid particulate matter in a liquid slurry comprising: directing two streams of slurry under a pressure of 500 to 2,000 psi towards each other along a common axis at a high velocity to disintegrate the particles; and passing the merged impacted streams of slurry at a high velocity through a narrow zone extending radially outwardly from the common axis and into contact with a plurality of solid posts extending into the zone to further disinpositioned entirely on the same side of a first plane parallel with and passing through said common axis and at unequal distances therefrom, a portion of each of said two posts lying in a second common plane parallel with and passing through said common axis.
2. The method of claim 1 in which the solid particulate matter includes asbestos fiber.
tegrate the particles, at least two of said posts being 3. The method of claim 1 in which the flow direction of the merged impacted streams of slurry through the narrow zone is changed by about from the flow path of each' of the two streams of slurry before their impact, and this general flow direction is maintained while passing through the narrow zone except in the immediate vicinity of the solid posts.
4. In an apparatus for reducing the size of solid particulate matter in a liquid slurry that is fed to the apparatus under pressure, and including a pair of aligned nozzles having a common discharge axis, said nozzles having spaced discharge ends for directing a discharge of slurry toward each other to disintegrate the particulate matter, the improvement comprising:
a. a pair of spaced panels extending transversely of the common axis of said nozzles, said panels forming a narrow zone in fluid flow communication with the discharge ends of said nozzles, and extending radially outwardly from said common axis;
b. frame means for fixing the position of each of said panels, said panels being mounted on said frame means; and
. a plurality of posts connected to at least one of said panels and extending into the narrow zone between said panels to further disintegrate particulate matter passing outwardly through said zone at a high velocity from the discharge nozzles, each of said posts comprising a pin connecting said panels and a plurality of abrasion resistant washers concentrically mounted on said pin with one face of one washer abutting the interior face of one of said panels and one face of another washer abutting the interior face of the other panel. 5. The apparatus of claim 4 including a container surrounding said panels for collecting the slurry passing radially outwardly from between said panels; and a high pressure displacement pump having its inlet connected to the interior of said container and its outlet connected to the inlet end of said nozzles for pumping slurry to said nozzles.
6. The apparatus of claim 4 in which said panels are spaced from one thirty-second inch to three-fourths inch apart, and the pair of aligned nozzles are spaced from one thirty-second inch to three-fourths inch apart.
7. The apparatus of claim 4 including a high pressure displacement pump having its discharge outlet connected to the inlet end of said nozzles.
8. The apparatus of claim 4 in which said spaced panels are removably mounted on said frame means to permit periodic replacement of said posts when said posts become eroded by abrasion.
9. In an apparatus for reducing the size of solid particulate matter in a liquid slurry that is fed to the apparatus under pressure, and including a pair of aligned nozzles having a common discharge axis, said nozzles having spaced discharge ends for directing a discharge of slurry toward each other to disintegrate the particulate matter, the improvement comprising:
a. a pair of spaced panels extending transversely of the common axis of said nozzles, said panels fonn ing a narrow zone in fluid flow communication with the discharge ends of said nozzles, and extending radially outwardly from said common axis, each of said panels being concave to form a zone that decreases in width in a radially outward direction from the common axis,
b. frame means for fixing the position of each of said panels, said panels being mounted on said frame means; and v c. a plurality of posts connected to at least one of said panels and extending into the narrow zone between said panels to further disintegrate particulate matter passing outwardly through said zone at a high velocity from the discharge nozzles.
' 10. The apparatus of claim in which said posts function as said frame means and connect said panels, and at least one pair of said posts engage said panels to prevent relative movement of said panels.
11. The apparatus of claim 10 in which the end portions of each of said pair of posts extend through said panels, and protrude outwardly from the exterior face of said panel and are threaded to permit nuts to hold the plates together in compression.
12. In an apparatus for reducing the size of solid parpanels, said panels being mounted on said fram means; and
. a plurality of posts connected to at least one of said panels and extending into the narrow zone between said panels to further disintegrate particulate matter passing outwardly through said zone at a high velocity from the discharge nozzles, at least two of said posts being positioned entirely on the same side of a first plane parallel with and passing through said common axis and at unequal distances therefrom, a portion of each of said two posts lying in a second common plane parallel with and passing through said common axis.
. frame means for fixing the position of each of said

Claims (11)

  1. 2. The method of claim 1 in which the solid particulate matter includes asbestos fiber.
  2. 3. The method of claim 1 in which the flow direction of the merged impacted streams of slurry through the narrow zone is changed by about 90* from the flow path of each of the two streams of slurry before their impact, and this general flow direction is maintained while passing through the narrow zone except in the immediate vicinity of the solid posts.
  3. 4. In an apparatus for reducing the size of solid particulate matter in a liquid slurry that is fed to the apparatus under pressure, and including a pair of aligned nozzles having a common discharge axis, said nozzles having spaced discharge ends for directing a discharge of slurry toward each other to disintegrate the particulate matter, the improvement comprising: a. a pair of spaced panels extending transversely of the common axis of said nozzles, said panels forming a narrow zone in fluid flow communication with the discharge ends of said nozzles, and extending radially outwardly from said common axis; b. frame means for fixing the position of each of said panels, said panels being mounted on said frame means; and c. a plurality of posts connected to at least one of said panels and extending into the narrow zone between said panels to further disintegrate particulate matter passing outwardly through said zone at a high velocity from the discharge nozzles, each of said posts comprising a pin connecting said panels and a plurality of abrasion resistant washers concentrically mounted on said pin with one face of one washer abutting the interior face of one of said panels and one face of another washer abutting the interior face of the other panel.
  4. 5. The apparatus of claim 4 including a container surrounding said panels for collecting the slurry passing radially outwardly from between said panels; and a high pressure displacement pump having its inlet connected to the interior of said container and its outlet connected to the inlet end of said nozzles for pumping slurry to said nozzles.
  5. 6. The apparatus of claim 4 in which said panels are spaced from one thirty-second inch to three-fourths inch apart, and the pair of aligned nozzles are spaced from one thirty-second inch to three-fourths inch apart.
  6. 7. The apparatus of claim 4 including a high pressure displacement pump having its discharge outlet connected to the inlet end of said nozzles.
  7. 8. The apparatus of claim 4 in which said spaced panels are removably mounted on said frame means to permit periodic replacement of said posts when said posts become eroded by abrasion.
  8. 9. In an apparatus for reducing the size of solid particulate matter in a liquid slurry that is fed to the apparatus under pressure, and including a pair of aligned nozzles having a common discharge axis, said nozzles having spaced discharge ends for directing a discharge of slurry toward each other to disintegrate the particulate matter, the improvement comprising: a. a pair of spaced panels extending transversely of the common axis of said nozzles, said panels forming a narrow zone in fluid flow communication with the discharge ends of said nozzles, and extending radially outwardly from said common axis, each of said panels beinG concave to form a zone that decreases in width in a radially outward direction from the common axis, b. frame means for fixing the position of each of said panels, said panels being mounted on said frame means; and c. a plurality of posts connected to at least one of said panels and extending into the narrow zone between said panels to further disintegrate particulate matter passing outwardly through said zone at a high velocity from the discharge nozzles.
  9. 10. The apparatus of claim 5 in which said posts function as said frame means and connect said panels, and at least one pair of said posts engage said panels to prevent relative movement of said panels.
  10. 11. The apparatus of claim 10 in which the end portions of each of said pair of posts extend through said panels, and protrude outwardly from the exterior face of said panel and are threaded to permit nuts to hold the plates together in compression.
  11. 12. In an apparatus for reducing the size of solid particulate matter in a liquid slurry that is fed to the apparatus under pressure, and including a pair of aligned nozzles having a common discharge axis, said nozzles having spaced discharge ends for directing a discharge of slurry toward each other to disintegrate the particulate matter, the improvement comprising: a. a pair of spaced panels extending transversely of the common axis of said nozzles, said panels forming a narrow zone in fluid flow communication with the discharge ends of said nozzles, and extending radially outwardly from said common axis; b. frame means for fixing the position of each of said panels, said panels being mounted on said frame means; and c. a plurality of posts connected to at least one of said panels and extending into the narrow zone between said panels to further disintegrate particulate matter passing outwardly through said zone at a high velocity from the discharge nozzles, at least two of said posts being positioned entirely on the same side of a first plane parallel with and passing through said common axis and at unequal distances therefrom, a portion of each of said two posts lying in a second common plane parallel with and passing through said common axis.
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Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4059231A (en) * 1976-07-16 1977-11-22 Grefco, Inc. Method and apparatus for selectively comminuting particles of a frangible material
US4374702A (en) * 1979-12-26 1983-02-22 International Telephone And Telegraph Corporation Microfibrillated cellulose
EP0124493A2 (en) * 1983-05-03 1984-11-07 Italsil S.p.A. Apparatus for the purification of siliceous sand by means of attrition
EP0574175A1 (en) * 1992-06-02 1993-12-15 Ian Macdonald Sinclair Process and apparatus for recovering metal values from ore
US5385640A (en) * 1993-07-09 1995-01-31 Microcell, Inc. Process for making microdenominated cellulose
US5487419A (en) * 1993-07-09 1996-01-30 Microcell, Inc. Redispersible microdenominated cellulose
US5542613A (en) * 1992-12-10 1996-08-06 Nied; Roland Process for impact crushing of solid particles
US20030199595A1 (en) * 2002-04-22 2003-10-23 Kozyuk Oleg V. Device and method of creating hydrodynamic cavitation in fluids
US20060187748A1 (en) * 2005-02-23 2006-08-24 Five Star Technologies, Inc. Methods and devices for mixing fluids
US20110015281A1 (en) * 2008-04-02 2011-01-20 Evonik Degussa Gmbh Apparatus and method for carrying out chemical and physical materials transformations
WO2022106573A1 (en) * 2020-11-20 2022-05-27 Basf Se Jet mill

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4059231A (en) * 1976-07-16 1977-11-22 Grefco, Inc. Method and apparatus for selectively comminuting particles of a frangible material
US4374702A (en) * 1979-12-26 1983-02-22 International Telephone And Telegraph Corporation Microfibrillated cellulose
EP0124493A2 (en) * 1983-05-03 1984-11-07 Italsil S.p.A. Apparatus for the purification of siliceous sand by means of attrition
EP0124493A3 (en) * 1983-05-03 1987-08-19 Italsil S.P.A. Apparatus and method for the purification of siliceous sand by means of attrition
AU665083B2 (en) * 1992-06-02 1995-12-14 Henry Arthur Simonsen Process and apparatus for recovering metal values from ore
EP0574175A1 (en) * 1992-06-02 1993-12-15 Ian Macdonald Sinclair Process and apparatus for recovering metal values from ore
US5542613A (en) * 1992-12-10 1996-08-06 Nied; Roland Process for impact crushing of solid particles
US5487419A (en) * 1993-07-09 1996-01-30 Microcell, Inc. Redispersible microdenominated cellulose
US5385640A (en) * 1993-07-09 1995-01-31 Microcell, Inc. Process for making microdenominated cellulose
US20030199595A1 (en) * 2002-04-22 2003-10-23 Kozyuk Oleg V. Device and method of creating hydrodynamic cavitation in fluids
US20040246815A1 (en) * 2002-04-22 2004-12-09 Kozyuk Oleg V. Device and method of creating hydrodynamic cavitation in fluids
US20060187748A1 (en) * 2005-02-23 2006-08-24 Five Star Technologies, Inc. Methods and devices for mixing fluids
US7422360B2 (en) 2005-02-23 2008-09-09 Cavitech Holdings, Llc Fluid impingement mixing device
US20110015281A1 (en) * 2008-04-02 2011-01-20 Evonik Degussa Gmbh Apparatus and method for carrying out chemical and physical materials transformations
US8313703B2 (en) * 2008-04-02 2012-11-20 Evonik Degussa Gmbh Apparatus and method for carrying out chemical and physical materials transformations
WO2022106573A1 (en) * 2020-11-20 2022-05-27 Basf Se Jet mill

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