US3688150A - Degassing arrangement for electron beam tube including an mk dispenser cathode - Google Patents

Degassing arrangement for electron beam tube including an mk dispenser cathode Download PDF

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US3688150A
US3688150A US763412A US3688150DA US3688150A US 3688150 A US3688150 A US 3688150A US 763412 A US763412 A US 763412A US 3688150D A US3688150D A US 3688150DA US 3688150 A US3688150 A US 3688150A
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electrodes
getter material
carbon
zirconium
cathode
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US763412A
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Manfred Wintzer
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Siemens AG
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Siemens AG
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J41/00Discharge tubes for measuring pressure of introduced gas or for detecting presence of gas; Discharge tubes for evacuation by diffusion of ions
    • H01J41/12Discharge tubes for evacuating by diffusion of ions, e.g. ion pumps, getter ion pumps
    • H01J41/14Discharge tubes for evacuating by diffusion of ions, e.g. ion pumps, getter ion pumps with ionisation by means of thermionic cathodes
    • H01J41/16Discharge tubes for evacuating by diffusion of ions, e.g. ion pumps, getter ion pumps with ionisation by means of thermionic cathodes using gettering substances
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J41/00Discharge tubes for measuring pressure of introduced gas or for detecting presence of gas; Discharge tubes for evacuation by diffusion of ions
    • H01J41/12Discharge tubes for evacuating by diffusion of ions, e.g. ion pumps, getter ion pumps
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J41/00Discharge tubes for measuring pressure of introduced gas or for detecting presence of gas; Discharge tubes for evacuation by diffusion of ions
    • H01J41/12Discharge tubes for evacuating by diffusion of ions, e.g. ion pumps, getter ion pumps
    • H01J41/18Discharge tubes for evacuating by diffusion of ions, e.g. ion pumps, getter ion pumps with ionisation by means of cold cathodes
    • H01J41/20Discharge tubes for evacuating by diffusion of ions, e.g. ion pumps, getter ion pumps with ionisation by means of cold cathodes using gettering substances
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J7/00Details not provided for in the preceding groups and common to two or more basic types of discharge tubes or lamps
    • H01J7/14Means for obtaining or maintaining the desired pressure within the vessel
    • H01J7/18Means for absorbing or adsorbing gas, e.g. by gettering
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J7/00Details not provided for in the preceding groups and common to two or more basic types of discharge tubes or lamps
    • H01J7/14Means for obtaining or maintaining the desired pressure within the vessel
    • H01J7/18Means for absorbing or adsorbing gas, e.g. by gettering
    • H01J7/183Composition or manufacture of getters

Definitions

  • the electrodes are formed by powdered metallurgy by mixing getter material powders such as zirconium, titanium or other getter material powders with carbon powder such as graphite and then forming the electrodes by pressing the mixture into a mold with a small amount of pressure and sintering in the range, for example, of 800 to 1,400 Centigrade to produce the electrodes which have good gas absorption capability and which can be worked with little difficulty.
  • the present invention relates to electrodes for electron tubes for high performance such as, for example, in tubes using a dispenser cathode, in particular an MK- cathode, and which provides mixing a powder of getter materials such as zirconium, titanium, or similar substances, with powdered carbon such as graphite and in which the distributed carbon may amount to up to about 30 percent by weight.
  • a dispenser cathode in particular an MK- cathode
  • powdered carbon such as graphite and in which the distributed carbon may amount to up to about 30 percent by weight.
  • the mixture is then BRIEF DESCRIPTION OF THE DRAWING
  • the FIG. illustrates an electrode according to the invention' mounted in a suitable electron tube.
  • the invention comprises forming working electrodes especially constructed for considerable cathode bombardment and which are completely or partially covered with getter material such as zirconium, titanium, or other suitable getter material.
  • getter material such as zirconium, titanium, or other suitable getter material.
  • Such electrodes may be, for example, anodes used in electron tubes having indirectly heated cathodes of high performance such as, for example, with tubes having cathodes in the form of dispenser cathodes, in particular of an MK- cathode.
  • the working electrodes are constructed by powdered metallurgy in that the getter material such as zirconium, titanium, or other suitable getter material substances are formed into a powder and mixed with a powder of carbon, in particular of electrographite, and with the powders being of approximately the same granulation and with the carbon being up to percent by weight. After the powders have been suitably mixed to form a homogenous mixture, it is then pressed in molds with small pressure into electrodes. The pressure may be up to approximately 3 kp/cm, (kp means kilopounds).
  • Electrodes thus formed may be easily worked and machined.
  • the invention is based upon the discovery that with porous unpressed zirconium bodies, an increase of gas absorption capacity at room temperature of tenfold can be attained.
  • heating of the electrodes by the electron beams cause the zirconium electrodes to be deformed and cracks form in the electrodes, thus decreasing the getter qualities of such zirconium bodies.
  • the present invention which mixes the getter powder with the carbon powder and pressing the mix-
  • the fact that the pressed zirconium-carbon body v continues to be easily workable, even after the use of relatively high sintering temperatures, as, for example, at l,300 C, is a great advantage.
  • zirconium carbide is a strongly pyrophoric material, which comprises an active getter material.
  • FIG. illustrates a cathode according to the present invention comprising an envelope 6 in which the electrode of the present invention is mounted so as to be sealed from the atmosphere.
  • envelope will be evacuated as is well known.
  • the envelope is connected to a support member 3 of cylindrical form, for example, which supports a cathode l by suitable insulating ring 4.
  • An impact'electrode 2 according to the invention is supported adjacent the cathode l.
  • Electrode 2 is supported from the support member 3 by insulating ring 5.
  • the impact electrode 2 is constructed according to the present invention and in a preferred form may be constructed as a disc with cylindrical sides extending toward the cathode 1. It is to be realized, of course, that the electrode 2 may also be disc-shaped, if desired.
  • the electrode 2 is formed by the process described above and includes the getter powder mixed with carbon powder which has been pressed and sintered between 800 C. and l,400 C. so as to produce electrodes that may be easily machined and which have the ability to absorb large quantities of gas.
  • the electrode 2 while providing an excellent working electrode, also serves to reduce and remove gas which is present in the envelope 6 and thus comprises a substantial improvement over working electrodes of prior art.
  • a degassing arrangement for an electron-beam tube having an envelope comprising:
  • an MK-type dispenser cathode mounted in said tube within said envelope
  • an electron emitting member forming a part of said dispenser cathode and an impact electrode insulatingly mounted adjacent said cathode within said envelope and formed of a mixture of getter material and carbon with said carbon being up to 30 percent by weight.

Abstract

Method and apparatus for producing electrodes capable of receiving considerable cathode bombardment and which are formed so as to remove gas from an electron tube, are disclosed. The electrodes are formed by powdered metallurgy by mixing getter material powders such as zirconium, titanium or other getter material powders with carbon powder such as graphite and then forming the electrodes by pressing the mixture into a mold with a small amount of pressure and sintering in the range, for example, of 800* to 1,400* centigrade to produce the electrodes which have good gas absorption capability and which can be worked with little difficulty.

Description

United States Patent Wintzer Aug. 29, 1972 [72] Inventor: Manfred Wintzer, Munich, Germany [73] Assignee: Siemens Aktiengesellschaft, Berlin and Munich, Germany [22] Filed: Sept. 27, 1968 [21] Appl. No.: 763,412
[30] Foreign Application Priority Data Oct. 4, 1967 Germany ..S 112258 [52] US. Cl. ..313/178, 313/179, 313/346 DC [51] Int. Cl. ..H01j 19/06, HOlj 61/26 [58] Field of Search ..313/106, 107, 179, 178, 217, 313/311, 346, 346 R, 346 DC Glaser et a1 ..313/107 X 2,788,460 4/1957 De Santis et al ..313/107 3,389,285 6/1968 Thomson ..313/107 3,416,013 12/1968 Poncelet et al. ..313/311 X 3,454,816 7/1969 Hoffmann et a1 ..313/311 X 3,504,213 3/ 1970 Hix et al. ..313/106 2,929,133 3/1960 Hughes ..313/346 DC Primary Examiner-Roy Lake Assistant ExaminerPalmer C. Demeo Attorney-Hill, Sherman, Meroni, Gross & Simpson [57] ABSTRACT Method and apparatus for producing electrodes capable of receiving considerable cathode bombardment and which are formed so as to remove gas from an electron tube, are disclosed. The electrodes are formed by powdered metallurgy by mixing getter material powders such as zirconium, titanium or other getter material powders with carbon powder such as graphite and then forming the electrodes by pressing the mixture into a mold with a small amount of pressure and sintering in the range, for example, of 800 to 1,400 Centigrade to produce the electrodes which have good gas absorption capability and which can be worked with little difficulty.
5 Claims, 1 Drawing Figure DEGASSING ARRANGEMENT FOR ELECTRON BEAM TUBE INCLUDING AN MK DISPENSER CATI-IODE BACKGROUND OF THE INVENTION 1. Field of the Invention This invention relates in general to electrodes for electron tubes and in particular to electrodes which have high gas absorption capacity.
2. Description of the Prior Art In the prior art it has been known to use molybdenum for constructing electron tube electrodes. Electrodes covered with getter material and consisting of one or more carbon discs have also been known. However, in actual practice, it has become evident that carbon bodies cannot be covered with getter material such as zirconium of arbitrary thickness which would be necessary for attaining higher rates of evacuation and larger gas absorption capabilities. On the other hand, working electrodes constructed of pure zirconium which are produced by pressing and sintering zirconium powder, have a high evacuation rate and large gas absorption capacity at temperatures above 600 centigrade, but at room temperature the gas absorption capacity was small because gas diffusion into the zirconium interior did not take place and only the small surface absorption of the zirconium electrode was effective. However, an increase in the gas absorption capacity of a working electrode at room temperatures is absolutely necessary in order to maintain the necessary vacuum of larger electron tubes while being stored.
SUMMARY OF THE INVENTION The present invention relates to electrodes for electron tubes for high performance such as, for example, in tubes using a dispenser cathode, in particular an MK- cathode, and which provides mixing a powder of getter materials such as zirconium, titanium, or similar substances, with powdered carbon such as graphite and in which the distributed carbon may amount to up to about 30 percent by weight. The mixture is then BRIEF DESCRIPTION OF THE DRAWING The FIG. illustrates an electrode according to the invention' mounted in a suitable electron tube.
DESCRIPTION OF THE PREFERRED EMBODIMENTS The invention comprises forming working electrodes especially constructed for considerable cathode bombardment and which are completely or partially covered with getter material such as zirconium, titanium, or other suitable getter material. Such electrodes may be, for example, anodes used in electron tubes having indirectly heated cathodes of high performance such as, for example, with tubes having cathodes in the form of dispenser cathodes, in particular of an MK- cathode.
The working electrodes are constructed by powdered metallurgy in that the getter material such as zirconium, titanium, or other suitable getter material substances are formed into a powder and mixed with a powder of carbon, in particular of electrographite, and with the powders being of approximately the same granulation and with the carbon being up to percent by weight. After the powders have been suitably mixed to form a homogenous mixture, it is then pressed in molds with small pressure into electrodes. The pressure may be up to approximately 3 kp/cm, (kp means kilopounds).
The electrodes are then sintered in a temperature range between 800 to l,400 centigrade. Electrodes thus formed may be easily worked and machined.
The invention is based upon the discovery that with porous unpressed zirconium bodies, an increase of gas absorption capacity at room temperature of tenfold can be attained. However, heating of the electrodes by the electron beams cause the zirconium electrodes to be deformed and cracks form in the electrodes, thus decreasing the getter qualities of such zirconium bodies. The present invention, which mixes the getter powder with the carbon powder and pressing the mix- The fact that the pressed zirconium-carbon body v continues to be easily workable, even after the use of relatively high sintering temperatures, as, for example, at l,300 C, is a great advantage.
It is possible that an alloy forms at the contact surfaces of the carbon-zirconium which is advantageous because zirconium carbide is a strongly pyrophoric material, which comprises an active getter material.
The FIG. illustrates a cathode according to the present invention comprising an envelope 6 in which the electrode of the present invention is mounted so as to be sealed from the atmosphere. Generally, such envelope will be evacuated as is well known. The envelope is connected to a support member 3 of cylindrical form, for example, which supports a cathode l by suitable insulating ring 4. An impact'electrode 2 according to the invention is supported adjacent the cathode l. Electrode 2 is supported from the support member 3 by insulating ring 5.
The impact electrode 2 is constructed according to the present invention and in a preferred form may be constructed as a disc with cylindrical sides extending toward the cathode 1. It is to be realized, of course, that the electrode 2 may also be disc-shaped, if desired. The electrode 2 is formed by the process described above and includes the getter powder mixed with carbon powder which has been pressed and sintered between 800 C. and l,400 C. so as to produce electrodes that may be easily machined and which have the ability to absorb large quantities of gas. Thus, the electrode 2, while providing an excellent working electrode, also serves to reduce and remove gas which is present in the envelope 6 and thus comprises a substantial improvement over working electrodes of prior art.
Although various minor modifications might be suggested by those versed in the art, it should be understood that I wish to embody within the scope of the patent warranted hereon all such modifications as reasonably and properly come within the scope of my contribution to the art.
I claim as my invention:
l. A degassing arrangement for an electron-beam tube having an envelope comprising:
an MK-type dispenser cathode mounted in said tube within said envelope; and
an electron emitting member forming a part of said dispenser cathode and an impact electrode insulatingly mounted adjacent said cathode within said envelope and formed of a mixture of getter material and carbon with said carbon being up to 30 percent by weight.
2. A degassing arrangement according to claim 1 wherein said getter material is zirconium.
3. A degassing arrangement according to claim 1 wherein said getter material is titanium.
4. A degassing arrangement according to claim 1 wherein said carbon is in the range of 15 to 30 percent by weight.
5. A degassing arrangement according to claim 1 wherein said getter material and said carbon have powder particle sizes.

Claims (5)

1. A degassing arrangement for an electron-beam tube having an envelope comprising: an MK-type dispenser cathode mounted in said tube within said envelope; and an electron emitting member forming a part of said dispenser cathode and an impact electrode insulatingly mounted adjacent said cathode within said envelope and formed of a mixture of getter material and carbon with said carbon being up to 30 percent by weight.
2. A degassing arrangement according to claim 1 wherein said getter material is zirconium.
3. A degassing arrangement according to claim 1 wherein said getter material is titanium.
4. A degassing arrangement according to claim 1 wherein said carbon is in the range of 15 to 30 percent by weight.
5. A degassing arrangement according to claim 1 wherein said getter material and said carbon have powder particle sizes.
US763412A 1965-06-30 1968-09-27 Degassing arrangement for electron beam tube including an mk dispenser cathode Expired - Lifetime US3688150A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DES0097898 1965-06-30
DE1967S0112258 DE1539156B2 (en) 1965-06-30 1967-10-04 GETTER PUMP ARRANGEMENT FOR ELECTRON BEAM TUBES AND METHOD FOR MANUFACTURING GETTERABLE SINTER SHAPED BODIES

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DE (1) DE1539156B2 (en)
FR (1) FR95641E (en)
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NL (1) NL6810879A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2498374A1 (en) * 1981-01-17 1982-07-23 Sperry Ltd GAS FIXER FOR LUMINESCENT DISCHARGE DEVICES
US6415016B1 (en) * 2001-01-09 2002-07-02 Medtronic Ave, Inc. Crystal quartz insulating shell for X-ray catheter
US6546077B2 (en) 2001-01-17 2003-04-08 Medtronic Ave, Inc. Miniature X-ray device and method of its manufacture
US6771737B2 (en) 2001-07-12 2004-08-03 Medtronic Ave, Inc. X-ray catheter with miniature emitter and focusing cup
US6866624B2 (en) 2000-12-08 2005-03-15 Medtronic Ave,Inc. Apparatus and method for treatment of malignant tumors

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US859292A (en) * 1903-12-10 1907-07-09 Gen Electric Electric lighting.
US1985087A (en) * 1931-11-09 1934-12-18 Gen Electric Arc discharge apparatus
US2788460A (en) * 1951-05-23 1957-04-09 Itt Electrodes for electron discharge devices and methods of making same
US2929133A (en) * 1956-09-05 1960-03-22 Philips Corp Dispenser cathode
US3389285A (en) * 1964-09-08 1968-06-18 Int Standard Electric Corp Grid electrode having a barrier layer of metal carbide and a surface coating of metal boride thereon
US3416013A (en) * 1964-07-03 1968-12-10 Commissariat Energie Atomique Composite structure electrode and process for manufacturing such electrode
US3454816A (en) * 1966-08-05 1969-07-08 Siemens Ag Indirectly heated dispenser cathode for electric discharge tube
US3504213A (en) * 1966-08-17 1970-03-31 Tesla Np Nonemissive carbide elements for grids for power tubes

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US859292A (en) * 1903-12-10 1907-07-09 Gen Electric Electric lighting.
US1985087A (en) * 1931-11-09 1934-12-18 Gen Electric Arc discharge apparatus
US2788460A (en) * 1951-05-23 1957-04-09 Itt Electrodes for electron discharge devices and methods of making same
US2929133A (en) * 1956-09-05 1960-03-22 Philips Corp Dispenser cathode
US3416013A (en) * 1964-07-03 1968-12-10 Commissariat Energie Atomique Composite structure electrode and process for manufacturing such electrode
US3389285A (en) * 1964-09-08 1968-06-18 Int Standard Electric Corp Grid electrode having a barrier layer of metal carbide and a surface coating of metal boride thereon
US3454816A (en) * 1966-08-05 1969-07-08 Siemens Ag Indirectly heated dispenser cathode for electric discharge tube
US3504213A (en) * 1966-08-17 1970-03-31 Tesla Np Nonemissive carbide elements for grids for power tubes

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2498374A1 (en) * 1981-01-17 1982-07-23 Sperry Ltd GAS FIXER FOR LUMINESCENT DISCHARGE DEVICES
US6866624B2 (en) 2000-12-08 2005-03-15 Medtronic Ave,Inc. Apparatus and method for treatment of malignant tumors
US6415016B1 (en) * 2001-01-09 2002-07-02 Medtronic Ave, Inc. Crystal quartz insulating shell for X-ray catheter
US6546077B2 (en) 2001-01-17 2003-04-08 Medtronic Ave, Inc. Miniature X-ray device and method of its manufacture
US20030133541A1 (en) * 2001-01-17 2003-07-17 Chornenky Victor I. Method of manufacturing a miniature X-ray device
US7086577B2 (en) 2001-01-17 2006-08-08 Medtronic Vascular, Inc. Method of manufacturing a miniature X-ray device
US6771737B2 (en) 2001-07-12 2004-08-03 Medtronic Ave, Inc. X-ray catheter with miniature emitter and focusing cup

Also Published As

Publication number Publication date
FR95641E (en) 1971-03-26
DE1539156B2 (en) 1976-09-23
NL6810879A (en) 1969-04-09
DE1539156A1 (en) 1970-03-26
GB1172939A (en) 1969-12-03

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