EP1106678A3 - Prilled nonionic surfactant granulate - Google Patents

Prilled nonionic surfactant granulate Download PDF

Info

Publication number
EP1106678A3
EP1106678A3 EP00126126A EP00126126A EP1106678A3 EP 1106678 A3 EP1106678 A3 EP 1106678A3 EP 00126126 A EP00126126 A EP 00126126A EP 00126126 A EP00126126 A EP 00126126A EP 1106678 A3 EP1106678 A3 EP 1106678A3
Authority
EP
European Patent Office
Prior art keywords
prilled
nonionic surfactant
granules
contain
nonionic surfactants
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP00126126A
Other languages
German (de)
French (fr)
Other versions
EP1106678B1 (en
EP1106678A2 (en
Inventor
Wilfried Dr. Rähse
Georg Dr. Assmann
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Publication of EP1106678A2 publication Critical patent/EP1106678A2/en
Publication of EP1106678A3 publication Critical patent/EP1106678A3/en
Application granted granted Critical
Publication of EP1106678B1 publication Critical patent/EP1106678B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/72Ethers of polyoxyalkylene glycols
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions
    • C11D11/0082Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0034Fixed on a solid conventional detergent ingredient
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0039Coated compositions or coated components in the compositions, (micro)capsules
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06Powder; Flakes; Free-flowing mixtures; Sheets
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06Powder; Flakes; Free-flowing mixtures; Sheets
    • C11D17/065High-density particulate detergent compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/18Hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2006Monohydric alcohols
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2075Carboxylic acids-salts thereof
    • C11D3/2079Monocarboxylic acids-salts thereof
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • C11D3/3703Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3707Polyethers, e.g. polyalkyleneoxides

Abstract

Der vorliegenden Erfindung lag somit die Aufgabe zugrunde, Granulate, die einen hohen Gehalt an flüssigen nichtionischen Tensiden, insbesondere über 20 Gew.-%, aufweisen, jedoch im wesentlichen ohne wasserunlösliches Trägermaterial auskommen und sich gut zur Einarbeitung in Wasch- oder Reinigungsmittel eignen, zur Verfügung zu stellen. Es wurde gefunden, daß Granulate bei Raumtemperatur flüssiger nichtionischer Tenside, die als Trägermaterial eine erstarrte Polymerschmelze enthalten, und weniger als 10 Gew.-% anorganischen Träger enthalten, diese Anforderungen erfüllen.The present invention was therefore based on the object of granules that have a high Have content of liquid nonionic surfactants, in particular more than 20% by weight, however, do essentially without water-insoluble carrier material and look good suitable for incorporation in detergents or cleaning agents. It it was found that granules of nonionic surfactants which are liquid at room temperature, which contain a solidified polymer melt as the carrier material, and less than 10 Contain wt .-% inorganic carrier, meet these requirements.

EP00126126A 1999-12-11 2000-11-30 Prilled nonionic surfactant granulate Expired - Lifetime EP1106678B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19959915A DE19959915A1 (en) 1999-12-11 1999-12-11 Nonionic surfactant granules by prilling
DE19959915 1999-12-11

Publications (3)

Publication Number Publication Date
EP1106678A2 EP1106678A2 (en) 2001-06-13
EP1106678A3 true EP1106678A3 (en) 2003-06-04
EP1106678B1 EP1106678B1 (en) 2006-09-06

Family

ID=7932380

Family Applications (1)

Application Number Title Priority Date Filing Date
EP00126126A Expired - Lifetime EP1106678B1 (en) 1999-12-11 2000-11-30 Prilled nonionic surfactant granulate

Country Status (6)

Country Link
US (1) US20010014657A1 (en)
EP (1) EP1106678B1 (en)
AT (1) ATE338811T1 (en)
CA (1) CA2327968A1 (en)
DE (2) DE19959915A1 (en)
ES (1) ES2270777T3 (en)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19959915A1 (en) * 1999-12-11 2001-07-05 Henkel Kgaa Nonionic surfactant granules by prilling
MXPA05008232A (en) * 2003-02-03 2005-10-05 Ciba Sc Holding Ag Washing agent and fabric softener formulations.
DE102004042933A1 (en) * 2004-09-02 2006-03-23 Henkel Kgaa Solid formulated liquids for use in particulate detergents and cleaners
DE102005027660A1 (en) * 2005-06-15 2006-12-28 Henkel Kgaa metering
JP4633657B2 (en) * 2005-09-30 2011-02-16 花王株式会社 Detergent composition for automatic dishwasher
EP3743494A1 (en) 2018-01-26 2020-12-02 Ecolab Usa Inc. Solidifying liquid amine oxide, betaine, and/or sultaine surfactants with a binder and optional carrier
EP3743493A1 (en) 2018-01-26 2020-12-02 Ecolab Usa Inc. Solidifying liquid anionic surfactants
KR20200110683A (en) 2018-01-26 2020-09-24 에코랍 유에스에이 인코퍼레이티드 Solidification of liquid amine oxides, betaines, and/or sultaines surfactants using carriers
US20200399563A1 (en) * 2019-06-21 2020-12-24 Ecolab Usa Inc. Solidifying nonionic surfactants

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4088431A (en) * 1974-05-07 1978-05-09 Imperial Chemical Industries Limited Melt spinning filter
US4545917A (en) * 1984-02-09 1985-10-08 Creative Products Resource Associates Ltd. Automatic dishwasher product in solid form
WO1997010326A1 (en) * 1995-09-14 1997-03-20 The Procter & Gamble Company Process for making a high density detergent composition from a surfactant paste containing a non-aqueous binder
US5739094A (en) * 1997-01-17 1998-04-14 The Procter & Gamble Company Free-flowing particulate detergent admix composition containing nonionic surfactant
DE19718664A1 (en) * 1997-05-02 1998-11-05 Clariant Gmbh Process for the preparation of storage-stable, soil release polymers (Soil Release Polymers, SRP) containing granules and their use for the production of solid detergents and cleaning agents
DE19959915A1 (en) * 1999-12-11 2001-07-05 Henkel Kgaa Nonionic surfactant granules by prilling
DE10021113A1 (en) * 2000-05-02 2001-11-15 Henkel Kgaa Particulate compounds containing non-ionic surfactants

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4088431A (en) * 1974-05-07 1978-05-09 Imperial Chemical Industries Limited Melt spinning filter
US4545917A (en) * 1984-02-09 1985-10-08 Creative Products Resource Associates Ltd. Automatic dishwasher product in solid form
WO1997010326A1 (en) * 1995-09-14 1997-03-20 The Procter & Gamble Company Process for making a high density detergent composition from a surfactant paste containing a non-aqueous binder
US5739094A (en) * 1997-01-17 1998-04-14 The Procter & Gamble Company Free-flowing particulate detergent admix composition containing nonionic surfactant
DE19718664A1 (en) * 1997-05-02 1998-11-05 Clariant Gmbh Process for the preparation of storage-stable, soil release polymers (Soil Release Polymers, SRP) containing granules and their use for the production of solid detergents and cleaning agents
DE19959915A1 (en) * 1999-12-11 2001-07-05 Henkel Kgaa Nonionic surfactant granules by prilling
DE10021113A1 (en) * 2000-05-02 2001-11-15 Henkel Kgaa Particulate compounds containing non-ionic surfactants

Also Published As

Publication number Publication date
CA2327968A1 (en) 2001-06-11
DE50013430D1 (en) 2006-10-19
EP1106678B1 (en) 2006-09-06
DE19959915A1 (en) 2001-07-05
US20010014657A1 (en) 2001-08-16
EP1106678A2 (en) 2001-06-13
ES2270777T3 (en) 2007-04-16
ATE338811T1 (en) 2006-09-15

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