DE69508859D1 - Verfahren zur Reinigung von (-)-n-Isopulegol sowie gereinigtes (-)-n-Isopulegol enthaltende Zitrusparfümzusammensetzungen - Google Patents

Verfahren zur Reinigung von (-)-n-Isopulegol sowie gereinigtes (-)-n-Isopulegol enthaltende Zitrusparfümzusammensetzungen

Info

Publication number
DE69508859D1
DE69508859D1 DE69508859T DE69508859T DE69508859D1 DE 69508859 D1 DE69508859 D1 DE 69508859D1 DE 69508859 T DE69508859 T DE 69508859T DE 69508859 T DE69508859 T DE 69508859T DE 69508859 D1 DE69508859 D1 DE 69508859D1
Authority
DE
Germany
Prior art keywords
isopulegol
purified
purification
perfume compositions
containing citrus
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69508859T
Other languages
English (en)
Other versions
DE69508859T2 (de
Inventor
Takeshi Yamamoto
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Takasago International Corp
Original Assignee
Takasago International Corp
Takasago Perfumery Industry Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Takasago International Corp, Takasago Perfumery Industry Co filed Critical Takasago International Corp
Publication of DE69508859D1 publication Critical patent/DE69508859D1/de
Application granted granted Critical
Publication of DE69508859T2 publication Critical patent/DE69508859T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/022Refining
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/78Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by condensation or crystallisation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C35/00Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring
    • C07C35/02Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic
    • C07C35/08Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic containing a six-membered rings
    • C07C35/18Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic containing a six-membered rings with unsaturation at least in the ring
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0026Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
    • C11B9/0034Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00Indexing scheme relating to specific properties of organic compounds
    • C07B2200/07Optical isomers
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00Systems containing only non-condensed rings
    • C07C2601/12Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14The ring being saturated
DE69508859T 1994-07-29 1995-07-27 Verfahren zur Reinigung von (-)-n-Isopulegol sowie gereinigtes (-)-n-Isopulegol enthaltende Zitrusparfümzusammensetzungen Expired - Lifetime DE69508859T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP19628294A JP3241542B2 (ja) 1994-07-29 1994-07-29 (−)−n−イソプレゴールの精製方法及びその方法で得られた(−)−n−イソプレゴールを含有するシトラス系香料組成物

Publications (2)

Publication Number Publication Date
DE69508859D1 true DE69508859D1 (de) 1999-05-12
DE69508859T2 DE69508859T2 (de) 1999-10-07

Family

ID=16355215

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69508859T Expired - Lifetime DE69508859T2 (de) 1994-07-29 1995-07-27 Verfahren zur Reinigung von (-)-n-Isopulegol sowie gereinigtes (-)-n-Isopulegol enthaltende Zitrusparfümzusammensetzungen

Country Status (5)

Country Link
US (1) US5773410A (de)
EP (1) EP0694514B1 (de)
JP (1) JP3241542B2 (de)
DE (1) DE69508859T2 (de)
ES (1) ES2131273T3 (de)

Families Citing this family (49)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7470244B2 (en) * 1996-01-26 2008-12-30 Harrison Jr Shelton E Flexion-discouraging splint system, method and device
US8512718B2 (en) 2000-07-03 2013-08-20 Foamix Ltd. Pharmaceutical composition for topical application
CA2427983C (en) 2000-11-06 2009-06-02 Japan Tobacco Inc. Tobacco odor deodorizing perfume compositon, tobacco odor deodorant, cigarette low in sidestream smoke odor, and tobacco package
DE10112362B4 (de) * 2001-03-15 2004-09-30 Bayerische Motoren Werke Ag Montagevorrichtung
IL152486A0 (en) 2002-10-25 2003-05-29 Meir Eini Alcohol-free cosmetic and pharmaceutical foam carrier
US7700076B2 (en) 2002-10-25 2010-04-20 Foamix, Ltd. Penetrating pharmaceutical foam
US8900554B2 (en) 2002-10-25 2014-12-02 Foamix Pharmaceuticals Ltd. Foamable composition and uses thereof
US7820145B2 (en) 2003-08-04 2010-10-26 Foamix Ltd. Oleaginous pharmaceutical and cosmetic foam
US9265725B2 (en) 2002-10-25 2016-02-23 Foamix Pharmaceuticals Ltd. Dicarboxylic acid foamable vehicle and pharmaceutical compositions thereof
KR101108439B1 (ko) 2002-10-25 2012-01-31 포믹스 리미티드 화장료 및 약제용 거품제
US10117812B2 (en) 2002-10-25 2018-11-06 Foamix Pharmaceuticals Ltd. Foamable composition combining a polar solvent and a hydrophobic carrier
US9668972B2 (en) 2002-10-25 2017-06-06 Foamix Pharmaceuticals Ltd. Nonsteroidal immunomodulating kit and composition and uses thereof
US7704518B2 (en) 2003-08-04 2010-04-27 Foamix, Ltd. Foamable vehicle and pharmaceutical compositions thereof
US9211259B2 (en) 2002-11-29 2015-12-15 Foamix Pharmaceuticals Ltd. Antibiotic kit and composition and uses thereof
US20080138296A1 (en) 2002-10-25 2008-06-12 Foamix Ltd. Foam prepared from nanoemulsions and uses
US8486376B2 (en) 2002-10-25 2013-07-16 Foamix Ltd. Moisturizing foam containing lanolin
US7575739B2 (en) 2003-04-28 2009-08-18 Foamix Ltd. Foamable iodine composition
US8795693B2 (en) 2003-08-04 2014-08-05 Foamix Ltd. Compositions with modulating agents
US8486374B2 (en) 2003-08-04 2013-07-16 Foamix Ltd. Hydrophilic, non-aqueous pharmaceutical carriers and compositions and uses
MX2007008154A (es) * 2005-01-04 2007-07-24 Teikoku Pharma Usa Inc Preparacion de parche topico para enfriamiento.
DE102005040655A1 (de) * 2005-08-26 2007-03-01 Basf Ag Verfahren zur Herstellung von angereichertem Isopulegol
BRPI0613067A2 (pt) 2005-10-24 2010-12-21 Teikoku Pharma Usa Inc composições tópicas para alìvio da dor de n,2,3-trimetil-2-isopropilbutamida e métodos de uso das mesmas
US20080260655A1 (en) 2006-11-14 2008-10-23 Dov Tamarkin Substantially non-aqueous foamable petrolatum based pharmaceutical and cosmetic compositions and their uses
US8636982B2 (en) 2007-08-07 2014-01-28 Foamix Ltd. Wax foamable vehicle and pharmaceutical compositions thereof
EP2036875A1 (de) * 2007-09-11 2009-03-18 Basf Se Kontinuierliches Verfahren zur Herstellung von Menthol in reiner oder angereicherter Form
JP5599716B2 (ja) 2007-11-30 2014-10-01 ビーエーエスエフ ソシエタス・ヨーロピア 光学活性ラセミメントールを製造するための方法
US9439857B2 (en) 2007-11-30 2016-09-13 Foamix Pharmaceuticals Ltd. Foam containing benzoyl peroxide
WO2010041141A2 (en) 2008-10-07 2010-04-15 Foamix Ltd. Oil-based foamable carriers and formulations
WO2009072007A2 (en) 2007-12-07 2009-06-11 Foamix Ltd. Carriers, formulations, methods for formulating unstable active agents for external application and uses thereof
CA2712120A1 (en) 2008-01-14 2009-07-23 Foamix Ltd. Poloxamer foamable pharmaceutical compositions with active agents and/or therapeutic cells and uses
CN102143928A (zh) * 2008-09-05 2011-08-03 马克斯普朗克科学促进协会 利用两个连续的结晶步骤对化合物形成的手性体系进行对映体拆分的方法
JP5603884B2 (ja) 2009-02-17 2014-10-08 長岡実業株式会社 天然l−メントールを生成するための方法及び装置
WO2010125470A2 (en) 2009-04-28 2010-11-04 Foamix Ltd. Foamable vehicle and pharmaceutical compositions comprising aprotic polar solvents and uses thereof
WO2011013008A2 (en) 2009-07-29 2011-02-03 Foamix Ltd. Non surface active agent non polymeric agent hydro-alcoholic foamable compositions, breakable foams and their uses
WO2011013009A2 (en) 2009-07-29 2011-02-03 Foamix Ltd. Non surfactant hydro-alcoholic foamable compositions, breakable foams and their uses
US9849142B2 (en) 2009-10-02 2017-12-26 Foamix Pharmaceuticals Ltd. Methods for accelerated return of skin integrity and for the treatment of impetigo
WO2011064631A1 (en) 2009-10-02 2011-06-03 Foamix Ltd. Surfactant-free, water-free, foamable compositions and breakable foams and their uses
JP5780933B2 (ja) * 2010-12-01 2015-09-16 高砂香料工業株式会社 光学活性メントールの製造方法
WO2013033501A1 (en) 2011-09-01 2013-03-07 Takasago International Corp. (Usa) Novel substituted cyclohexane compounds
US20150329452A1 (en) 2012-11-15 2015-11-19 Takasago International Corporation Method for producing optically active isopulegol and optically active menthol
JP7048317B2 (ja) * 2015-02-24 2022-04-05 高砂香料工業株式会社 増強香料組成物
ES2851677T3 (es) * 2016-02-24 2021-09-08 Takasago Perfumery Co Ltd Agente estimulante
US20190054200A1 (en) 2016-02-24 2019-02-21 Takasago International Corporation Household product delivering warming and/or tingling sensations
US11851631B2 (en) 2016-02-24 2023-12-26 Takasago International Corporation Household product delivering cooling sensations
MX2019001455A (es) 2016-08-04 2019-06-20 Takasago Perfumery Co Ltd Compuestos de sensacion de calor.
MX2020012139A (es) 2016-09-08 2021-01-29 Vyne Pharmaceuticals Inc Composiciones y metodos para tratar rosacea y acne.
EP3388411A1 (de) * 2017-04-13 2018-10-17 Sulzer Chemtech AG Verfahren zur reinigung einer rohzusammensetzung mit einer monoterpenverbindung, wie monocyclischer monoterpenalkohol, alkohol durch schichtschmelzkristallisation
EP3900696B1 (de) 2020-04-21 2023-04-19 Takasago International Corporation Eingekapselte duftstoffzusammensetzung
EP3900697B1 (de) 2020-04-21 2023-03-15 Takasago International Corporation Duftstoffzusammensetzung

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3218361A (en) * 1960-06-08 1965-11-16 Glidden Co Process for recovering specific isopulegols
US4217371A (en) * 1978-10-20 1980-08-12 International Flavors & Fragrances Inc. Flavoring with cyclohexene methanol lower alkyl esters
US5545424A (en) * 1994-10-12 1996-08-13 Takasago International Corporation 4-(1-menthoxymethyl)-2-phenyl-1,3-dioxolane or its derivatives and flavor composition containing the same

Also Published As

Publication number Publication date
EP0694514A2 (de) 1996-01-31
US5773410A (en) 1998-06-30
ES2131273T3 (es) 1999-07-16
JPH0840959A (ja) 1996-02-13
EP0694514A3 (de) 1996-03-27
DE69508859T2 (de) 1999-10-07
JP3241542B2 (ja) 2001-12-25
EP0694514B1 (de) 1999-04-07

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