DE69124560D1 - Addition von Additiven zu polymeren Materialien - Google Patents
Addition von Additiven zu polymeren MaterialienInfo
- Publication number
- DE69124560D1 DE69124560D1 DE69124560T DE69124560T DE69124560D1 DE 69124560 D1 DE69124560 D1 DE 69124560D1 DE 69124560 T DE69124560 T DE 69124560T DE 69124560 T DE69124560 T DE 69124560T DE 69124560 D1 DE69124560 D1 DE 69124560D1
- Authority
- DE
- Germany
- Prior art keywords
- additives
- addition
- polymeric materials
- polymeric
- materials
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/20—Compounding polymers with additives, e.g. colouring
- C08J3/205—Compounding polymers with additives, e.g. colouring in the presence of a continuous liquid phase
- C08J3/2053—Compounding polymers with additives, e.g. colouring in the presence of a continuous liquid phase the additives only being premixed with a liquid phase
- C08J3/2056—Compounding polymers with additives, e.g. colouring in the presence of a continuous liquid phase the additives only being premixed with a liquid phase the polymer being pre-melted
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/285—Feeding the extrusion material to the extruder
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/36—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die
- B29C48/365—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using pumps, e.g. piston pumps
- B29C48/37—Gear pumps
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/36—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die
- B29C48/395—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders
- B29C48/40—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders using two or more parallel screws or at least two parallel non-intermeshing screws, e.g. twin screw extruders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/36—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die
- B29C48/395—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders
- B29C48/40—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders using two or more parallel screws or at least two parallel non-intermeshing screws, e.g. twin screw extruders
- B29C48/405—Intermeshing co-rotating screws
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/36—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die
- B29C48/50—Details of extruders
- B29C48/76—Venting, drying means; Degassing means
- B29C48/765—Venting, drying means; Degassing means in the extruder apparatus
- B29C48/766—Venting, drying means; Degassing means in the extruder apparatus in screw extruders
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/20—Compounding polymers with additives, e.g. colouring
- C08J3/22—Compounding polymers with additives, e.g. colouring using masterbatch techniques
- C08J3/226—Compounding polymers with additives, e.g. colouring using masterbatch techniques using a polymer as a carrier
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
- C08J2367/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2377/00—Characterised by the use of polyamides obtained by reactions forming a carboxylic amide link in the main chain; Derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2467/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2477/00—Characterised by the use of polyamides obtained by reactions forming a carboxylic amide link in the main chain; Derivatives of such polymers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
- Y10S8/903—Triple mixture of anionic, cationic, and nonionic emulsifiers for dyeing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
- Y10S8/904—Mixed anionic and nonionic emulsifiers for dyeing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
- Y10S8/905—Mixed anionic and cationic emulsifiers for dyeing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
- Y10S8/906—Mixed cationic and nonionic emulsifiers for dyeing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
- Y10S8/907—Nonionic emulsifiers for dyeing
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US58636590A | 1990-09-21 | 1990-09-21 |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69124560D1 true DE69124560D1 (de) | 1997-03-20 |
DE69124560T2 DE69124560T2 (de) | 1997-05-28 |
Family
ID=24345455
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69124560T Expired - Fee Related DE69124560T2 (de) | 1990-09-21 | 1991-09-07 | Addition von Additiven zu polymeren Materialien |
Country Status (7)
Country | Link |
---|---|
US (1) | US6149850A (de) |
EP (1) | EP0477634B1 (de) |
JP (1) | JPH0777751B2 (de) |
AU (1) | AU641278B2 (de) |
CA (1) | CA2050612A1 (de) |
DE (1) | DE69124560T2 (de) |
ES (1) | ES2097171T3 (de) |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0478987A3 (en) * | 1990-09-21 | 1992-05-20 | Basf Corporation | Addition of additives to polymeric materials |
IT1255233B (it) * | 1992-07-17 | 1995-10-20 | Himont Inc | Procedimento per la stabilizzazione di polimeri olefinici |
US5364582A (en) * | 1993-08-30 | 1994-11-15 | Basf Corporation | Method for producing polymeric fibers with improved anti-static properties and fibers and fabrics produced thereby |
US5543495A (en) * | 1994-03-08 | 1996-08-06 | E. I. Du Pont De Nemours And Company | Process for increasing the molecular weight of polyamides and other condensation polymers |
DE69735865T2 (de) * | 1996-03-04 | 2006-11-16 | Honeywell International Inc. | Verfahren zur Herstellung von Additiven für synthetische Filamente und Einarbeitung dieser Additive in thermoplastische filamentbildende Polymermaterialien |
DE10149163A1 (de) * | 2001-10-04 | 2003-04-17 | Buehler Ag | Kontinuierliche Herstellung von Elastomermischungen für die Gummiherstellung |
US20040186483A1 (en) * | 2003-03-22 | 2004-09-23 | Bagby George W. | Implant driver apparatus and bone joining device |
DE102006052013B4 (de) * | 2005-11-04 | 2010-04-08 | Heubach Gmbh | Verfahren zur Herstellung eines pigmentierten thermoplastischen Materials und Verwendung des pigmentierten thermoplastischen Materials |
US7892461B2 (en) | 2005-11-04 | 2011-02-22 | Heubach Gmbh | Method for the production and use of pigmented thermoplastic material comprising a flow enhancer in the form of a dissolved salt |
US7993560B2 (en) | 2006-04-20 | 2011-08-09 | Curwood, Inc. | Process for introducing an additive into a polymer melt |
WO2009120868A2 (en) * | 2008-03-28 | 2009-10-01 | 3M Innovative Properties Company | Filled resins and method for making filled resins |
DE102008038667A1 (de) * | 2008-08-12 | 2010-02-25 | K+S Ag | Herstellungsverfahren von thermoplastischen Polymeren enthaltend grobskalige und/oder nanoskalige, gecoatete, desagglomerierte Magnesiumhydroxidpartikel und eine Vorrichtung hierzu |
JP5766906B2 (ja) * | 2008-10-30 | 2015-08-19 | 大日精化工業株式会社 | 顔料・樹脂組成物の製造方法 |
BRPI1014911A2 (pt) | 2009-05-26 | 2016-07-26 | 3M Innovative Proferties Company | processo para fabricação de resinas carregadas |
DE102009045122A1 (de) | 2009-09-29 | 2011-03-31 | Evonik Röhm Gmbh | Verfahren und Anlage zur Einfärbung von Kunststoffformmassen |
CN103747957A (zh) * | 2011-06-17 | 2014-04-23 | 嘉洛斯控股有限公司 | 聚合材料 |
US9312047B2 (en) | 2012-06-22 | 2016-04-12 | Honeywell International Inc. | Method and compositions for producing polymer blends |
JP6810605B2 (ja) | 2013-03-15 | 2021-01-06 | アセンド・パフォーマンス・マテリアルズ・オペレーションズ・リミテッド・ライアビリティ・カンパニーAscend Performance Materials Operations Llc | 重合に連結した配合方法 |
EP2886291A1 (de) * | 2013-12-23 | 2015-06-24 | Omya International AG | Polymerzusammensetzung durch kontinuierliche Extrusion von Füllschlamm |
DE102018124523B4 (de) * | 2018-10-04 | 2020-10-22 | Gneuss Gmbh | Verfahren zur Herstellung von Polymeren, in welchen Füllstoffe mit Partikelgrößen kleiner 10 μm eingearbeitet und homogen verteilt sind. |
Family Cites Families (26)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3040005A (en) * | 1959-01-21 | 1962-06-19 | Du Pont | Process for increasing the molecular weight of polyamides |
US3023456A (en) * | 1959-08-03 | 1962-03-06 | Dow Chemical Co | Extruder apparatus |
AT283709B (de) * | 1964-11-26 | 1970-08-25 | Barmag Barmer Maschf | Schneckenpresse zur Verarbeitung thermoplastischer Kunststoffe |
US3376603A (en) * | 1966-05-20 | 1968-04-09 | Lavorazione Mat Plast | Apparatus for manufacturing synthetic textile fibers |
US3607335A (en) * | 1967-11-08 | 1971-09-21 | Basf Ag | Pigment formulations |
US3563514A (en) * | 1968-03-11 | 1971-02-16 | Borg Warner | Plasticizer with full diameter rotor |
US3742093A (en) * | 1970-04-08 | 1973-06-26 | Welding Engineers | Method of separating an insoluble liquid from polymer composition |
US3846507A (en) * | 1972-04-06 | 1974-11-05 | Union Carbide Canada Ltd | Polyamide blends with one polyamide containing phthalate sulfonate moieties and terphthalate on isophthalate residues |
NL7503986A (nl) * | 1974-04-11 | 1975-10-14 | Basf Ag | Werkwijze voor het inmengen van toevoegsels in kunststoffen onder gelijktijdig verwijderen van vluchtige bestanddelen. |
DE2444584C3 (de) * | 1974-09-18 | 1982-01-21 | Basf Ag, 6700 Ludwigshafen | Thermoplastische Polyesterformmassen |
US4002593A (en) * | 1975-07-17 | 1977-01-11 | Hercules Incorporated | Process for producing dispersions of pigments in condensation type polymers |
US4098741A (en) * | 1976-09-30 | 1978-07-04 | Basf Wyandotte Corporation | Phosphorus-containing polyester and size compositions |
DE2801288C2 (de) * | 1978-01-13 | 1985-06-20 | Hoechst Ag, 6230 Frankfurt | Verwendung von wasserunlöslichen Diazomethinverbindungen zum Färben von thermoplastischen Polyestern in der Masse und in der Spinnfärbung von thermoplastischen Polyestern |
JPS5817539B2 (ja) * | 1978-09-18 | 1983-04-07 | 旭化成株式会社 | メラミンシアヌレ−ト含有ポリアミド組成物の製造方法 |
US4374641A (en) * | 1979-08-01 | 1983-02-22 | Badische Corporation | Polymeric color concentrates for thermoplastic polymeric materials |
NL7908964A (nl) * | 1979-12-13 | 1981-07-16 | Akzo Nv | Werkwijze ter bereiding van masterbatches van peroxyden in polymeren. |
DE3166871D1 (en) * | 1981-01-09 | 1984-11-29 | Basf Ag | Preparation process of thermoplastic moulding masses |
DE3135328A1 (de) * | 1981-09-05 | 1983-03-24 | Hoechst Ag, 6000 Frankfurt | Verfahren zum faerben von thermoplastischen kunststoffen in der masse |
US4755585A (en) * | 1982-08-06 | 1988-07-05 | Amoco Corporation | Injection moldable polyamide imide from trimellitic anhydride end capped with aniline |
DE3313919A1 (de) * | 1983-04-16 | 1984-10-18 | Basf Ag, 6700 Ludwigshafen | Schlagzaehe thermoplastische formmassen und verfahren zu ihrer herstellung |
CA1272339A (en) * | 1984-06-25 | 1990-07-31 | Paul James Mollinger | Process for pelletization of powder materials and products therefrom |
JPS61284497A (ja) * | 1985-06-11 | 1986-12-15 | 日立精工株式会社 | 自動製図機用ペン上下動制御装置 |
US4750910A (en) * | 1986-01-22 | 1988-06-14 | Mitsui Toatsu Chemicals, Incorporated | Indigo blue-colored bioabsorbable surgical fibers and production process thereof |
EP0266754A3 (de) * | 1986-11-05 | 1989-02-22 | Nippon Ester Company Ltd. | Farbstoff und damit in der Masse gefärbte, verformte Polyestergegenstände |
DE3713746A1 (de) * | 1987-04-24 | 1988-11-17 | Basf Ag | Brandgeschuetzte, roten phosphor enthaltende thermoplastische formmassen auf der basis von polyestern oder polyamiden |
EP0478987A3 (en) * | 1990-09-21 | 1992-05-20 | Basf Corporation | Addition of additives to polymeric materials |
-
1991
- 1991-09-04 CA CA002050612A patent/CA2050612A1/en not_active Abandoned
- 1991-09-07 ES ES91115155T patent/ES2097171T3/es not_active Expired - Lifetime
- 1991-09-07 DE DE69124560T patent/DE69124560T2/de not_active Expired - Fee Related
- 1991-09-07 EP EP91115155A patent/EP0477634B1/de not_active Expired - Lifetime
- 1991-09-20 AU AU84673/91A patent/AU641278B2/en not_active Ceased
- 1991-09-20 JP JP3240831A patent/JPH0777751B2/ja not_active Expired - Lifetime
-
1993
- 1993-12-10 US US08/166,168 patent/US6149850A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
JPH0777751B2 (ja) | 1995-08-23 |
US6149850A (en) | 2000-11-21 |
CA2050612A1 (en) | 1992-03-22 |
EP0477634A2 (de) | 1992-04-01 |
EP0477634B1 (de) | 1997-02-05 |
JPH05169515A (ja) | 1993-07-09 |
DE69124560T2 (de) | 1997-05-28 |
AU8467391A (en) | 1992-03-26 |
AU641278B2 (en) | 1993-09-16 |
ES2097171T3 (es) | 1997-04-01 |
EP0477634A3 (en) | 1992-05-20 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition | ||
8339 | Ceased/non-payment of the annual fee |