DE59403026D1 - Verfahren zur herstellung kugelförmiger teilchen - Google Patents

Verfahren zur herstellung kugelförmiger teilchen

Info

Publication number
DE59403026D1
DE59403026D1 DE59403026T DE59403026T DE59403026D1 DE 59403026 D1 DE59403026 D1 DE 59403026D1 DE 59403026 T DE59403026 T DE 59403026T DE 59403026 T DE59403026 T DE 59403026T DE 59403026 D1 DE59403026 D1 DE 59403026D1
Authority
DE
Germany
Prior art keywords
pct
sol
reaction zone
spherical particles
date sep
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE59403026T
Other languages
English (en)
Inventor
Helmut Derleth
Karl-Heinz Bretz
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Solvay GmbH
Original Assignee
Solvay Deutschland GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE4405202A external-priority patent/DE4405202A1/de
Application filed by Solvay Deutschland GmbH filed Critical Solvay Deutschland GmbH
Priority to DE59403026T priority Critical patent/DE59403026D1/de
Application granted granted Critical
Publication of DE59403026D1 publication Critical patent/DE59403026D1/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
    • B01J2/04—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a gaseous medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
    • B01J2/06—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a liquid medium
    • B01J2/08—Gelation of a colloidal solution
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0045—Drying a slurry, e.g. spray drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0072—Preparation of particles, e.g. dispersion of droplets in an oil bath
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/34—Methods for preparing oxides or hydroxides in general by oxidation or hydrolysis of sprayed or atomised solutions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/16—Preparation of silica xerogels
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/44—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water
    • C01F7/441—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water by calcination
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/70—Treatment of water, waste water, or sewage by reduction
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C01P2004/52—Particles with a specific particle size distribution highly monodisperse size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/14—Pore volume
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C02F2101/16—Nitrogen compounds, e.g. ammonia
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S210/00—Liquid purification or separation
    • Y10S210/902—Materials removed
    • Y10S210/908—Organic
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S210/00—Liquid purification or separation
    • Y10S210/902—Materials removed
    • Y10S210/908—Organic
    • Y10S210/909—Aromatic compound, e.g. pcb, phenol
DE59403026T 1993-03-05 1994-03-01 Verfahren zur herstellung kugelförmiger teilchen Expired - Fee Related DE59403026D1 (de)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DE59403026T DE59403026D1 (de) 1993-03-05 1994-03-01 Verfahren zur herstellung kugelförmiger teilchen

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE4306875 1993-03-05
DE4405202A DE4405202A1 (de) 1993-03-05 1994-02-18 Verfahren zur Herstellung kugelförmiger Teilchen
PCT/EP1994/000587 WO1994020203A1 (de) 1993-03-05 1994-03-01 Verfahren zur herstellung kugelförmiger teilchen
DE59403026T DE59403026D1 (de) 1993-03-05 1994-03-01 Verfahren zur herstellung kugelförmiger teilchen

Publications (1)

Publication Number Publication Date
DE59403026D1 true DE59403026D1 (de) 1997-07-10

Family

ID=25923665

Family Applications (4)

Application Number Title Priority Date Filing Date
DE4491189T Expired - Fee Related DE4491189D2 (de) 1993-03-05 1994-03-01 Verfahren zur katalytischen Behandlung von organische und anorganische Verbindungen enthaltenden Abwässern, vorzugsweise aus der Epichlorhydrinproduktion
DE59408365T Expired - Fee Related DE59408365D1 (de) 1993-03-05 1994-03-01 Verfahren zur katalytischen behandlung von organische und anorganische verbindungen enthaltenden abwässern, vorzugsweise aus der epichlorhydrinproduktion
DE4491190T Expired - Fee Related DE4491190D2 (de) 1993-03-05 1994-03-01 Verfahren zur Herstellung kugelförmiger Teilchen
DE59403026T Expired - Fee Related DE59403026D1 (de) 1993-03-05 1994-03-01 Verfahren zur herstellung kugelförmiger teilchen

Family Applications Before (3)

Application Number Title Priority Date Filing Date
DE4491189T Expired - Fee Related DE4491189D2 (de) 1993-03-05 1994-03-01 Verfahren zur katalytischen Behandlung von organische und anorganische Verbindungen enthaltenden Abwässern, vorzugsweise aus der Epichlorhydrinproduktion
DE59408365T Expired - Fee Related DE59408365D1 (de) 1993-03-05 1994-03-01 Verfahren zur katalytischen behandlung von organische und anorganische verbindungen enthaltenden abwässern, vorzugsweise aus der epichlorhydrinproduktion
DE4491190T Expired - Fee Related DE4491190D2 (de) 1993-03-05 1994-03-01 Verfahren zur Herstellung kugelförmiger Teilchen

Country Status (7)

Country Link
US (2) US5736118A (de)
EP (2) EP0687199B1 (de)
JP (2) JPH08506988A (de)
AT (2) ATE180754T1 (de)
DE (4) DE4491189D2 (de)
DK (1) DK0687199T3 (de)
WO (2) WO1994020423A1 (de)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
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DE4406588A1 (de) * 1994-03-01 1995-09-07 Solvay Deutschland Verfahren zur katalytischen Behandlung von Abwasser sowie ein Verfahren zur Regenerierung eines Katalysators
JP4004538B2 (ja) * 1994-09-08 2007-11-07 ゾルファイ ウムヴェルトヒエミー ゲゼルシャフト ミット ベシュレンクテル ハフツング 水から接触的還元により塩素酸塩−および臭素酸塩化合物を除去する方法
DE4443884A1 (de) * 1994-12-09 1996-06-13 Solvay Deutschland Verfahren zur katalytischen Behandlung von organische und anorganische Verbindungen enthaltenden Abwässern
US6492572B2 (en) * 1995-08-29 2002-12-10 E. I. Du Pont De Nemours And Company Method for remediating contaminated soils
DE19748513C2 (de) * 1997-11-03 1999-09-09 Sueddeutsche Kalkstickstoff Verfahren zur adsorptiven Entfernung von Kohlenwasserstoffen aus wässrigen Blausäurelösungen
GB2331071A (en) * 1997-11-11 1999-05-12 Solvay Manufacture of micro spherical zeolite containing catalyst particles
DE19757496A1 (de) * 1997-12-23 1999-06-24 Studiengesellschaft Kohle Mbh Hochporöse Photokatalysatoren zur Verwertung von sichtbarem Licht
DE19810565A1 (de) 1998-03-11 1999-09-16 Basf Ag Verfahren zur Trocknung und Herstellung von mikroporösen Teilchen
WO2000071472A1 (fr) * 1999-05-19 2000-11-30 Hitachi Zosen Corporation Procede de decomposition de compose organochlore
DE10113113A1 (de) * 2001-03-16 2002-09-19 Bayer Ag Nitratreduktion durch SO¶2¶
WO2004092053A2 (de) * 2003-04-09 2004-10-28 Silicaglas Ilmenau Gmbh Verfahren zur herstellung eines kieselsäuregranulates und dessen verwendung zur herstellung von kieselglasgranulat
US20040253386A1 (en) * 2003-06-13 2004-12-16 Sarojini Deevi Preparation of intermetallics by metallo-organic decomposition
US20110300446A1 (en) * 2010-06-03 2011-12-08 Hon Hai Precision Industry Co., Ltd. Lithium battery cathode composite material
CN106268733B (zh) * 2016-09-13 2018-11-30 山东大学 一种一维纳米棒自组装形成具有分级结构的栗子壳状三维二氧化钛空心微球的制备方法
JP7039853B2 (ja) * 2017-03-31 2022-03-23 戸田工業株式会社 非晶質アルミノケイ酸塩粒子粉末及びその製造方法、スラリー並びに成形体
CN108499572A (zh) * 2018-04-26 2018-09-07 华电高科环保技术有限公司 蜂窝状低温脱硝催化剂及其制备方法
CN109046338B (zh) * 2018-08-03 2020-08-04 华中科技大学 一种炭材料固载的钯催化剂、其制备和应用
CN109126689B (zh) * 2018-09-27 2020-12-01 广西科学院 一种改性蒙脱石的制备方法及其应用
CN110180517B (zh) * 2019-06-28 2021-06-04 东北大学 一种淀粉/聚乙烯亚胺复合磁性吸附材料的制备方法
CN112121813B (zh) * 2020-09-15 2023-05-30 北京山美水美臭氧高科技有限公司 碱土金属改性的Mn基臭氧氧化催化剂及其应用

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US2467470A (en) * 1945-05-25 1949-04-19 Universal Oil Prod Co Manufacture of spherical particles
US2652371A (en) * 1949-12-20 1953-09-15 Sinclair Refining Co Process of forming spheroidal catalyst particles
AT207393B (de) * 1957-02-14 1960-01-25 Montedison Spa Verfahren und Vorrichtung zur Herstellung von Körnern, insbesondere aus Ammoniumnitrat
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DE4042594A1 (de) * 1990-11-05 1992-07-02 Nukem Gmbh Verfahren zur herstellung von aluminiumoxidkugeln

Also Published As

Publication number Publication date
WO1994020423A1 (de) 1994-09-15
JPH08506988A (ja) 1996-07-30
US5736118A (en) 1998-04-07
WO1994020203A1 (de) 1994-09-15
US5676845A (en) 1997-10-14
DE4491189D2 (de) 1995-04-27
ATE153875T1 (de) 1997-06-15
DE59408365D1 (de) 1999-07-08
ATE180754T1 (de) 1999-06-15
DK0687199T3 (da) 1997-07-14
JPH08506989A (ja) 1996-07-30
EP0687199A1 (de) 1995-12-20
EP0690825B1 (de) 1999-06-02
DE4491190D2 (de) 1995-04-27
EP0690825A1 (de) 1996-01-10
EP0687199B1 (de) 1997-06-04

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee