DE1520601A1 - Verfahren zur Herstellung ionischer Mischpolymerisate - Google Patents
Verfahren zur Herstellung ionischer MischpolymerisateInfo
- Publication number
- DE1520601A1 DE1520601A1 DE1964P0034008 DEP0034008A DE1520601A1 DE 1520601 A1 DE1520601 A1 DE 1520601A1 DE 1964P0034008 DE1964P0034008 DE 1964P0034008 DE P0034008 A DEP0034008 A DE P0034008A DE 1520601 A1 DE1520601 A1 DE 1520601A1
- Authority
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- Germany
- Prior art keywords
- metal
- metal ions
- carboxyl groups
- ionic
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
- C08K5/098—Metal salts of carboxylic acids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
- B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
- B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
- B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
- B32B17/1055—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer
- B32B17/10743—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer containing acrylate (co)polymers or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F255/00—Macromolecular compounds obtained by polymerising monomers on to polymers of hydrocarbons as defined in group C08F10/00
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/30—Introducing nitrogen atoms or nitrogen-containing groups
- C08F8/32—Introducing nitrogen atoms or nitrogen-containing groups by reaction with amines
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/44—Preparation of metal salts or ammonium salts
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/17—Amines; Quaternary ammonium compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2800/00—Copolymer characterised by the proportions of the comonomers expressed
- C08F2800/20—Copolymer characterised by the proportions of the comonomers expressed as weight or mass percentages
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/04—Homopolymers or copolymers of ethene
- C08L23/08—Copolymers of ethene
- C08L23/0846—Copolymers of ethene with unsaturated hydrocarbons containing other atoms than carbon or hydrogen atoms
- C08L23/0869—Acids or derivatives thereof
- C08L23/0876—Neutralised polymers, i.e. ionomers
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S260/00—Chemistry of carbon compounds
- Y10S260/31—Ionic cross-link
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S273/00—Amusement devices: games
- Y10S273/22—Ionomer
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S36/00—Boots, shoes, and leggings
- Y10S36/02—Plastic
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S428/00—Stock material or miscellaneous articles
- Y10S428/91—Product with molecular orientation
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/13—Hollow or container type article [e.g., tube, vase, etc.]
- Y10T428/1352—Polymer or resin containing [i.e., natural or synthetic]
- Y10T428/139—Open-ended, self-supporting conduit, cylinder, or tube-type article
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/13—Hollow or container type article [e.g., tube, vase, etc.]
- Y10T428/1352—Polymer or resin containing [i.e., natural or synthetic]
- Y10T428/1397—Single layer [continuous layer]
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31678—Of metal
- Y10T428/31692—Next to addition polymer from unsaturated monomers
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31855—Of addition polymer from unsaturated monomers
- Y10T428/31938—Polymer of monoethylenically unsaturated hydrocarbon
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Description
DR.-ING. WALTER ABITZ DR. DIETER MORF
Patentanwälte
WUälSllu6e 38
8 Munch·» AV, HlemaiWUtilSiluft«.
Telefon 483225 und 486415 Telegramme ι Chemlndus Mönchen
1520801
14. Koveeber I968
AD-286? (P 3* 00Ö)
P 15 20 601. 6 Neue Unterlagen
E. I. OCF PONT Wt MSHOORS AND COMPANY
10th and Market Streets« Wilmington, Delaware 19698, V. St. A.
Verfahren zur Herstellung ionischer Mischpolymerisate
(Zusatz zu Patent · (Patentanmeldung P I^ 20 506. 8))
Das Hauptpatent (Patentanmeldung P 15 20 S06. S)
betrifft die Herstellung ionischer Mischpolymerisate aus der
Klasse der Polymerisat« von a-OleKnen der allgemeinen Formel
00SI20/1lii
BAD
worin R Wasserstoff oder einen Alkylrest mit 1-8 Kohlenstoffatomen
bedeutet, mit einem Olefingehalt von zumindest 50 MoI-Jt, bezogen auf das Polymerisat, und einer α,0-äthylenartig
ungesättigten Monocarbonsäure mit einem Säuremonomergehalt von 0,2 bis 25 MoI-Ji1 bezogen auf das Polymerisat, wobei das
Monocarbonsäurepolymerisat in gleichmässiger Verteilung ein ein- bis dreiwertiges Metallion enthält, sowie der Polymerisate
de3 genannten Olefingehalts und einer n,3-äthylenartig ungesättigten
Dlcarbonsäure mit einem Säuregehalt von 0,2 - 25
MoI-Ji, bezogen auf das Polymerisat, wobei das Dicar bonsäure mischpolymerisat
in gleichmässiger Verteilung ein einwertiges Metallion enthält, wobei mindestens 10 Ji der Carbonsäuregruppen
der die einwertige bzw. zweiwertige Carbonsäure aufweisenden Polymerisate durch die Metallionen neutralisiert sind« Diese
Mischpolymerisate werden erhalten, indem bei erhöhten Temperaturen eine ionische Metallverbindung, die in Wasser in
einem Ausmass von mindestens 2 Gew.-Ji löslich ist, in der das
Netall eine Wertigkeit von 1-5 aufweist und deren Nichtmetallrest
bei Vereinigung mit Wasserstoff ein bei der Reaktionstemperatur
flüchtiges Reaktionsprodukt bildet, mit einem Polymerisat eines α«Olefin· der allgemeinen Formel
RCH2-CH2
009820/1586
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worin R Wasserstoff oder einen Aikylreet nit 1-8 Kohlen-Btoffatoaen
bedeutet, nit einen Olefingehalt von mindestens
30 Mol«£, bezogen auf das Polymerisat, und einer or,ß-äthylenartlg
ungesättigten Carbonsäure, die 3-8 Kohlenstoffatome
und 1-2 Carboxylgruppen aufweist, nit einen Gehalt an dem Säureaonoaeren von 0,2 - 25 MoI-Ji, bezogen auf* das Polymerisat,
vernleoht wird, wobei das Hetallion eine Wertigkeit von 1 - 3 '
besitzt, wenn das Polymerisat ein Monooarbonsäuremonomer
enthält, und wobei das Metallion einwertig ist, wenn das PoIy-.norisat
ein Dlearbonsäureaenoaer enthält, und wobei die Menge
der ionischen Metallverbindung ausreicht, um zumindest 10 %
der Carbonsäure zu neutralisieren.
Mach den Hauptpatent (Patentanmeldung F 15 SO 506· 8) «lad
die zur Bildung der ionischen Mischpolymerisate geeigneten
Metallionen nicht koaplex gebundene Metallion*n>. Es wurde nun
gefunden, dass die'Metallionen, die sieh zur Bildung der ionischen
Misohpolynerlsate eignen, in zwei Kategorien eingeteilt
werden kennen, näalloh nicht kocplex gebundene Metallionen, die
Gegenstand de· Kauptpatente (Patentanmeldung F 15 20 506· 8)
sind, und koaplex gebunden· Ngtallienen, άϊ% Gegenstand der
vorliegenden Erfindung sind. Sn den nicht koaplex gebundenen
009820/1586
1520801
Metallionen entspricht die Wertigkeit des Ions der Wertigkeit
des Metalls« Diese Mstallionen werden aus den allgemein bekannten
und verwendeten Metallsalzen erhalten. Die erfindungs-·
geraäss verwendeten, komplex gebundenen Metallionen sind diejenigen, in denen das Metall an mehr als einer Art von Salzgruppe
gebunden ist,.wobei zumindest eine Salzgruppe ionisiert
und zumindest eine Salzgruppe nicht ionisiert ist.
Der Ausdruck "Metallion mit einer oder mehreren
ionisierten Wertigkeitsstufen" bedeutet ein Metallion der allgemeinen
Formel
worin η die ionisohe Ladung bedeutet und zumindest 1 ist« X
eine niohtionisierte Oruppe darstellt und η + ra gleich der
Wertigkeit des Netalls ist. Die Brauchbarkeit von bei der
Bildung von ionischen Mischpolymerisaten verwendeten, komplex gebundenen Netallionen, entspricht bezüglich deren ionisierten Wertig
keiten derjenigen der nicht komplex gebundenen Metallionen.
Die einwertigen Metalle sind naturlich ausgeschlossen, doch
können hShenrortige Metalleeinbesogen werden, Je nachdem,
0 0 9820/1586
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wieviele Metallwertigkeiten komplex gebunden sind, und wie viele
ionisiert werden können. Die bevorzugten komplex gebundenen Metallionen
sind diejenigen, in denen alle Wertigkeiten bis auf eine Metallwertigkeit komplex gebunden sind, und eine leicht
ionisiert wird. Solche Verbindungen sind insbesondere die gemischten Salze von sehr schwachen Säuren, wie beispielsweise
ölsäure und Stearinsäure, und ionisierbaren Säuren, wie beispielsweise
Ameisensäure und Essigsäure.
Zu. komplex gebundenen Metallionen, die sich zur Bildung der
ionischen Mischpolymerisate gemäss der vorliegenden Erfindung eignen, gehören daher die zwei- und dreiwertigen Ionen von
Metallen der Gruppen I, II, III, IV-A und VIII des Periodischen
Systeme der Elemente (gemäse "Handbook of Chemistry and
Physios", Chemical Rubber Publishtog Co., Jf. Ed., Seite 392).
Geeignete zweiwertige Metallionen eind Be+*, Mg+V Ca+V £
Ba++, CAi+V W+V Hg+V Sn+V Pb+*, Fe+V Cb+V Hi+* und Zn
Geeignete dreiwertige Metallionen elnd Al+**, So+**, Pe+** und
* · " -
Die Verwendung von komplex gebundenen Metallionen ermöglicht
die Verwendung von mehrwertigen Metallen al« Ionenvernetzungsmittel
für Mischpolymerisate von Dicarbonsäuren. Viele der korn-
009820/1586
BAD ORfGINAL
plexbildenden MIttel haben auseerdem noch gesonderte Brauchbarkeit
in Polymerisaten. So sind die komplexbildenden Mittel
als Stabilisatoren, Färbemittel, Weichmacher und dgl., wertvoll. Die komplex gebundenen Metallionen ergeben auch einen arbeitsmässigen
Vorteil, da ihr Einbringen in eine Polymerisat-Schmelze
leichter vorzunehmen ist.
Salze von komplex gebundenen Metallionen .können Jn das
Polymerisat in Form dee Salzes selbst oder in Form der Komponenten
des Salzes eingebracht werden, die miteinander unter Bildung des Salzes in situ reagieren.
Die folgenden Beispiele erläutern die Erfindung, ohne sie zu
beschränken.
Zu 50 g eines Mischpolymerisats von Äthylen und Maleinsäureanhydrid
mit einem Gehalt von 7 Gew.-ji oopolyraerisiertem Malein-•Mureanhydrld
und «Ines Scbaelzlndex von 8,5 g/10 Minuten,
das auf eine« Kautsohukaahlwerk bei einer Temperatur von 135*C
behandelt 1st, werden 22,8 g Zlnknonoaoetatmonostearat zügegeben·
Nach 15-minütiger Behandlung auf dem Mahlwerk wird ein
009820/1S86
BAD ORIGINAL
transparentes» zähes, elastisches Polyraerprodukt erhalten, das
einen zur Herstellung von Folien nach Üblichem Schmelzauspressen
ausreichenden Schmelzfluss besitzt. Bei Wiederholung der experimentellen Arbeltsweise mit Zinkacetat wird innerhalb
einer Behandlung auf dem Mahlwerk von 10 Minuten ein nichtbearbeitbares
Kars gebildet« wodurch eine weitere Behandlung auf dem Mahlwerk verhindert wird. Das Harz kann nicht zu einer
Folie unter Anwendung üblichen Sohnelzauspressens ausgepresst werden*
Zu 50 g eines Mischpolymerisats aus Äthylen und Methacrylsäure mit einem Gehalt von 10 Oew.-Ji copolymerisierter Methacrylsäure
und einem Schmelzindex von 5*8 g/10 Minuten« das auf einem Kautschukmahlwerk bei 1J0#C behandelt ist, werden die
folgenden Komponenten in der angegebenen Reihenfolge zugegebenι
(·) 3,25 g Zinkoxyd, (b) 11,7 g Stearinsäure und (0) 2,5 g
Essigsäure. Erst nach der Zugabe der 4KSsIgSaUrO wird die Schmelze
klar, und es wird ein Viskositätsanstieg beobachtet. Nach 10-mlnUtlger weiterer Behandlung auf des Mahlwerk wird das Mlsehpolymerisat
eatftrnt.Der Schneisindex 1st zwar herabgesetzt,
doch eignet sich das erhaltene ionische Mischpolymerisat zur
Schnelzverarbeltung.
009820/1586 .
Claims (1)
- Belegexemplar!Darf nicht geändert werden 1frP 15 20 601. 6 14. November I968B. I· du Pont de Neamin
aod Company AD-2863 (P 34 008)PatentanspruchVerfahren zur Herstellung Ionischer Mischpolymerisate gemässPatent (Patentanmeldung ρ 15 20 5O6. 8), bei demin einem Mischpolymerisat mit einem Schmolzindex von 0,1 hie 100 g/10 Min., das wenigstens 50 Molji Äthyleneinheiten, 0,2 bis 25 MoI^ Einheiten von öl,A-ungesättigten Mono« oder Dicarbonsäuren beziehungsweise Halbestern oder Anhydriden der Dicarbonsäuren und gegebenenfalls Einheiten einea dritten Comonomeren enthält und in bekannter Weise durch direkte Mischpolymerisation der Monomeren hergestellt worden ist, mit einem oder mehreren Netallionen von ionischen Metallverbindungen wenigstens 10 % der Carboxylgruppen neutralisiert werden und wobei ein- bis dreiwertige Metallionen eingesetzt werden, wenn die Carboxylgruppen aus einer Monocarbonsäure und einwertige Metallionen, wenn die Carboxylgruppen aus einer Dicarbonsäure stammen.und die Metallverbindung bei Raumtemperatur zumindest su 2 Gew.-Jt in Wasser löslich sind und deren Nicht metallrest mit den Wasserstoff aus der Carbonsäure bei den Reaktionsbedingungen entfernt werden kann, dadurch gekennzeichnet, dass die ffeutralieatlon bei erhöhter Temperatur mit einem Metalleal« vorgenommen wird, das ein komplexgebundenes Metallion enthält, wobei zumindestens eine Salzgruppe locieiert und zumindest eine Salzgruppe nicht ionisiert ist.009820/1586 BAÖORIGINAL
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US13514761A | 1961-08-31 | 1961-08-31 | |
US16883962A | 1962-01-25 | 1962-01-25 | |
US27147763 US3264272A (en) | 1961-08-31 | 1963-04-08 | Ionic hydrocarbon polymers |
US34829364 US3404134A (en) | 1961-08-31 | 1964-02-28 | Process of crosslinking polymers |
Publications (2)
Publication Number | Publication Date |
---|---|
DE1520601A1 true DE1520601A1 (de) | 1970-05-14 |
DE1520601B2 DE1520601B2 (de) | 1973-01-04 |
Family
ID=27495141
Family Applications (6)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE1962P0030096 Pending DE1520506B2 (de) | 1961-08-31 | 1962-08-27 | Verfahren zum modifizieren von carboxylgruppen enthaltenden aethylenpolymeren |
DE1963P0031004 Pending DE1520518B2 (de) | 1961-08-31 | 1963-01-24 | Verfahren zur herstellung von modifizierten copolymerisaten aus ungesaettigten kohlenwasserstoffen und ungesaettigten carbonsaeuren |
DE1520601A Granted DE1520601B2 (de) | 1961-08-31 | 1964-04-08 | Verfahren zum Modifizieren von Carboxylgruppen enthaltenden Äthylenpolymeren |
DE1745939A Expired DE1745939C3 (de) | 1961-08-31 | 1965-03-01 | Verfahren zum Modifizieren von Carboxylgruppen enthaltenden Äthylenpolymeren |
DE1965P0036183 Granted DE1745938B2 (de) | 1961-08-31 | 1965-03-01 | Verfahren zum modifizieren von carboxylgruppen enthaltenden aethylenpolymeren |
DE1595112A Expired DE1595112C3 (de) | 1961-08-31 | 1965-03-01 | Verfahren zur Herstellung von modifizierten Copolymerisaten aus ungesättigten Kohlenwasserstoffen und ungesättigten Carbonsäuren |
Family Applications Before (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE1962P0030096 Pending DE1520506B2 (de) | 1961-08-31 | 1962-08-27 | Verfahren zum modifizieren von carboxylgruppen enthaltenden aethylenpolymeren |
DE1963P0031004 Pending DE1520518B2 (de) | 1961-08-31 | 1963-01-24 | Verfahren zur herstellung von modifizierten copolymerisaten aus ungesaettigten kohlenwasserstoffen und ungesaettigten carbonsaeuren |
Family Applications After (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE1745939A Expired DE1745939C3 (de) | 1961-08-31 | 1965-03-01 | Verfahren zum Modifizieren von Carboxylgruppen enthaltenden Äthylenpolymeren |
DE1965P0036183 Granted DE1745938B2 (de) | 1961-08-31 | 1965-03-01 | Verfahren zum modifizieren von carboxylgruppen enthaltenden aethylenpolymeren |
DE1595112A Expired DE1595112C3 (de) | 1961-08-31 | 1965-03-01 | Verfahren zur Herstellung von modifizierten Copolymerisaten aus ungesättigten Kohlenwasserstoffen und ungesättigten Carbonsäuren |
Country Status (9)
Country | Link |
---|---|
US (2) | US3264272A (de) |
BE (2) | BE621846A (de) |
CH (2) | CH445861A (de) |
DE (6) | DE1520506B2 (de) |
DK (1) | DK125713B (de) |
FR (1) | FR1430478A (de) |
GB (4) | GB1011981A (de) |
NL (4) | NL282755A (de) |
SE (2) | SE311229B (de) |
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US2646425A (en) * | 1953-07-21 | Ereparation of ethylene polymers | ||
US2607762A (en) * | 1948-12-07 | 1952-08-19 | Monsanto Chemicals | Dry process manufacture of watersoluble derivatives of styrenemaleic anhydride type heteropolymers |
US2757153A (en) * | 1949-12-14 | 1956-07-31 | Monsanto Chemicals | Process for water-soluble styrenemaleic anhydride derivatives |
US2599123A (en) * | 1950-08-18 | 1952-06-03 | Du Pont | Copolymers of ethylene with an alkyl acrylate and an alkyl monoester of a butene-1,4-dioic acid |
US2798053A (en) * | 1952-09-03 | 1957-07-02 | Goodrich Co B F | Carboxylic polymers |
US2757106A (en) * | 1953-05-28 | 1956-07-31 | Rohm & Haas | Coated paper products and method of making |
DE1016228B (de) * | 1955-09-06 | 1957-09-26 | Monsanto Chemicals | Verfahren zum Schlichten von Polyamidfaeden oder -garnen |
US2999056A (en) * | 1956-10-04 | 1961-09-05 | Du Pont | Irradiation bonding of acidic compounds to shaped polymeric structures |
US3132120A (en) * | 1961-02-03 | 1964-05-05 | Du Pont | Method for the preparation of ethylene copolymers |
NL128027C (de) * | 1961-08-31 | 1900-01-01 |
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0
- NL NL128027D patent/NL128027C/xx active
- NL NL129542D patent/NL129542C/xx active
- BE BE627537D patent/BE627537A/xx unknown
- NL NL288151D patent/NL288151A/xx unknown
- NL NL282755D patent/NL282755A/xx unknown
- BE BE621846D patent/BE621846A/xx unknown
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1962
- 1962-08-27 DE DE1962P0030096 patent/DE1520506B2/de active Pending
- 1962-08-28 DK DK376862AA patent/DK125713B/da unknown
- 1962-08-29 SE SE935262A patent/SE311229B/xx unknown
- 1962-08-29 CH CH1029662A patent/CH445861A/de unknown
- 1962-08-30 GB GB3328162A patent/GB1011981A/en not_active Expired
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1963
- 1963-01-18 GB GB230763A patent/GB1029035A/en not_active Expired
- 1963-01-24 DE DE1963P0031004 patent/DE1520518B2/de active Pending
- 1963-01-24 CH CH90163A patent/CH435741A/de unknown
- 1963-01-25 SE SE83063A patent/SE303882B/xx unknown
- 1963-04-08 US US27147763 patent/US3264272A/en not_active Expired - Lifetime
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1964
- 1964-02-28 US US34829364 patent/US3404134A/en not_active Expired - Lifetime
- 1964-04-08 DE DE1520601A patent/DE1520601B2/de active Granted
- 1964-04-08 GB GB1459464A patent/GB1034268A/en not_active Expired
-
1965
- 1965-02-26 FR FR7228A patent/FR1430478A/fr not_active Expired
- 1965-02-26 GB GB840765A patent/GB1063436A/en not_active Expired
- 1965-03-01 DE DE1745939A patent/DE1745939C3/de not_active Expired
- 1965-03-01 DE DE1965P0036183 patent/DE1745938B2/de active Granted
- 1965-03-01 DE DE1595112A patent/DE1595112C3/de not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1992019562A1 (fr) * | 1991-05-07 | 1992-11-12 | Sommer S.A. | Procede de production de revetements de sols ou de murs a base de polymeres et produits obtenus |
BE1004795A3 (fr) * | 1991-05-07 | 1993-02-02 | Eurofloor Sa | Procede de production de revetements de sols ou de murs a base de polyolefines et produits obtenus. |
Also Published As
Publication number | Publication date |
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NL282755A (de) | 1900-01-01 |
NL288151A (de) | 1900-01-01 |
DE1520506B2 (de) | 1971-06-09 |
FR1430478A (fr) | 1966-03-04 |
CH435741A (de) | 1967-05-15 |
CH445861A (de) | 1967-10-31 |
SE311229B (de) | 1969-06-02 |
NL128027C (de) | 1900-01-01 |
GB1063436A (en) | 1967-03-30 |
DK125713B (da) | 1973-03-26 |
GB1011981A (en) | 1965-12-01 |
DE1520506A1 (de) | 1970-02-19 |
DE1745938B2 (de) | 1973-07-19 |
US3404134A (en) | 1968-10-01 |
DE1520518A1 (de) | 1969-07-03 |
DE1595112B2 (de) | 1973-07-05 |
DE1595112A1 (de) | 1970-04-09 |
DE1520518B2 (de) | 1971-07-22 |
NL129542C (de) | 1900-01-01 |
US3264272A (en) | 1966-08-02 |
DE1745939B2 (de) | 1973-07-19 |
DE1745939A1 (de) | 1971-01-14 |
BE621846A (de) | 1900-01-01 |
SE303882B (de) | 1968-09-09 |
DE1520601B2 (de) | 1973-01-04 |
DE1745938A1 (de) | 1971-01-14 |
DE1745939C3 (de) | 1974-02-21 |
DE1595112C3 (de) | 1974-03-14 |
GB1029035A (en) | 1966-05-11 |
GB1034268A (en) | 1966-06-29 |
DE1745938C3 (de) | 1974-02-21 |
BE627537A (de) | 1900-01-01 |
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