CN1385388A - Ceramic fibre thermal-insulating boara and making method thereof - Google Patents
Ceramic fibre thermal-insulating boara and making method thereof Download PDFInfo
- Publication number
- CN1385388A CN1385388A CN 02120854 CN02120854A CN1385388A CN 1385388 A CN1385388 A CN 1385388A CN 02120854 CN02120854 CN 02120854 CN 02120854 A CN02120854 A CN 02120854A CN 1385388 A CN1385388 A CN 1385388A
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- Prior art keywords
- ceramic fiber
- wet base
- ceramic fibre
- additive
- warming plate
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
Abstract
The ceramic fibre heat-insulating board is made up by using ceramic fiber, inorganic binding agent, organic binding agent and additive according to the weight ratio of 40-60:20-30:0.5-1.5:20-30. Its preparation method includes the following steps: using ceramic fibre as base material, adding inorganic binding agent, organic binding agent, additive and water, fully making pulp, adopting mechanical extrusion forming process or manual forming process to produce wet blank, and drying treatment at 100-150 deg.C so as to obtain the invented heat-insualting board which is high mechanical property and heat-insulating property, can be used as back liner of permanent furnace lining of various kiln and furnaces.
Description
Technical field
The invention belongs to the monoblock fire resisting material field that does not contain clay, relating in particular to a kind of is the warming plate of matrix with the ceramic fiber.
Background technology
The ceramic fiber warming plate of prior art, because the restriction of production technique, surface irregularity presents orange peel shape, adds man-hour owing to fiber interweaving, and mechanical process capacity is poor, and general processor is difficult to satisfy.In addition, because goods are production moulding in mould, easily produce the goods geometry deformation during demoulding, though can repair lining, the surface is still uneven.During construction, because the geometrical dimension out of true of goods, the construction back wall is uneven, the construction slit is big, thermal conductivity is high, increase the application quantity of indefinite form material, thereby limited the big area popularization of product, make the fiber function can not get comprehensive embodiment as construction tackiness agent, coating.
Nineteen ninety-five disclosed state patent application 94102154.8 provides a kind of composite, insulating, light organosilicon wall material, and its major ingredient is: aluminosilicate fiber cotton, perlite, wilkinite, water, asbestos, useless fiber, caustic soda, epoxy glue, stablizer, thickening agents, permeate agent, starch, hydrogen peroxide, starter, cullet silk.Though this material has heat insulation and heat insulation effect, only be suitable for cryogenic material.On March 20th, 2002, disclosed another Chinese patent application 00111348.8 provided a kind of mechanically made ceramic fibre plate, it adopts aluminum silicate fiber, organic bond, inorganic bonding agent and additive to form, and the ratio of aluminum silicate fiber, organic bond, inorganic bonding agent and additive is: 1: 0.05～0.1: 1～1.5: 0.05～0.1.Wherein organic bond is resin, starch and Mierocrystalline cellulose, and inorganic bonding agent is silicon sol and aluminium glue, and additive is alumina powder and clay micro mist.But owing to adopt vacuum forming, the geometrical dimension of finished product still has certain deviation, and heat-insulating property is poor slightly.
Summary of the invention
The purpose of this invention is to provide a kind of ceramic fiber warming plate and its preparation method, the warming plate that especially a kind of geometrical dimension deviation is less, heat-insulating property is good.
Technical scheme of the present invention is: a kind of ceramic fiber warming plate, form by ceramic fiber, inorganic bonding agent, organic bond and additive, it is characterized in that the weight ratio of ceramic fiber, inorganic bonding agent, organic bond and additive is: 60～40: 30～20: 0.5～1.5: 30～20.Ceramic fiber can adopt the alumina-silicate ceramic fibre of different Applicable temperatures; Organic bond is one or more the mixture in polyacrylamide, cationic starch or the carboxymethyl cellulose; Inorganic bonding agent is one or more the mixture in cement, silicon sol, aluminium colloidal sol or the water glass; Additive is one or more the mixture in ground silica, expansion ground silica, swelling perlite powder or the silicon powder.
The preparation method of this ceramic fiber warming plate is to be base material with the ceramic fiber, add inorganic bonding agent, organic bond and additive, carry out abundant slurrying, adopt the mechanical presses method of forming or manual assembly to produce wet base then, drying treatment through 100～150 ℃, remove moisture, impel goods internal junction mixture to carry out gel, sclerosis, reach and to try to achieve hardness.Dried goods utilize that mechanical means is cut, grinding, brill, carry out further deep processing.
The ceramic fiber warming plate after drying because the difference of additive, that warming plate presents is faint yellow, brown or grey, Applicable temperature is extensive, can be used for the backing or the permanent furnace lining of various high, medium and low temperature kilns.
Be the comparison of the present invention and vacuum forming fiberboard below:
| Project | The ceramic fiber warming plate | The vacuum forming fiberboard |
| Length variation mm | ????0????+2 | ????±3 |
| Width difference mm | ????0????±2 | ????±3 |
| Thickness deviation mm | ?????????±0.1 | ????±2 |
| Planeness deviation mm | ?????????±0.5 | ????±1 |
| Ultimate compression strength MPa (thickness direction compression 10%) | ?????????≥0.6 | ????≥0.4 |
| Thermal conductivity W/m.k | 400 ℃ 0.116 of hot side | 300 ℃ 0.122 of hot side |
| 600 ℃ 0.124 of hot side | 400 ℃ 0.136 of hot side | |
| 800 ℃ 0.131 of hot side | 500 ℃ 0.170 of hot side |
Beneficial effect of the present invention is: improved the mechanical property of ceramic fiber warming plate, reduced the size deviation and the thermal conductivity of product, the construction rear surface is smooth, and the construction slit is little, and thermosteresis is few, has improved the heat-insulating property of goods.
Embodiment
Embodiment 1 gets alumina-silicate ceramic fibre 40.0kg, add polyacrylamide 0.5kg, ordinary Portland cement 20.0kg, ground silica 20.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 100 ℃, is finished product after removing moisture.
Embodiment 2 gets alumina-silicate ceramic fibre 40.0kg, add cationic starch 0.5kg, silicon sol 20.0kg, expansion ground silica 20.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 150 ℃, is finished product after removing moisture.
Embodiment 3 gets alumina-silicate ceramic fibre 40.0kg, add carboxymethyl cellulose 0.5kg, aluminium colloidal sol 20.0kg, swelling perlite powder 20.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 48 hours under the temperature about 120 ℃, is finished product after removing moisture.
Embodiment 4 gets alumina-silicate ceramic fibre 40.0kg, add polyacrylamide 0.5kg, water glass 20.0kg, silicon powder 20.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 140 ℃, is finished product after removing moisture.
Embodiment 5 gets alumina-silicate ceramic fibre 60.0kg, add cationic starch 1.5kg, high-alumina cement 30.0kg, ground silica 30.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 100 ℃, is finished product after removing moisture.
Embodiment 6 gets alumina-silicate ceramic fibre 60.0kg, add carboxymethyl cellulose 1.5kg, aluminium colloidal sol 30.0kg, expansion ground silica 30.0kg and water, fully stir, mixed pulp, adopt the hand form block method of forming to produce wet base then, wet base is dry more than 48 hours under the temperature about 130 ℃, is finished product after removing moisture.
Embodiment 7 gets alumina-silicate ceramic fibre 60.0kg, add cationic polyacrylamide 1.5kg, silicon sol 30.0kg, swelling perlite powder 30.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 48 hours under the temperature about 150 ℃, is finished product after removing moisture.
Embodiment 8 gets alumina-silicate ceramic fibre 60.0kg, add cationic starch 1.5kg, water glass 30.0kg, silicon powder 30.0kg and water, fully stir, mixed pulp, adopt hand-mold process to produce wet base then, wet base is dry more than 48 hours under the temperature about 140 ℃, is finished product after removing moisture.
Embodiment 9 gets alumina-silicate ceramic fibre 60.0kg, add anionic polyacrylamide 0.5kg, ordinary Portland cement 20.0kg, ground silica 20.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 100 ℃, is finished product after removing moisture.
Embodiment 10 gets alumina-silicate ceramic fibre 60.0kg, add cationic starch 1.5kg, silicon sol 30.0kg, expansion ground silica 20.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 48 hours under the temperature about 120 ℃, is finished product after removing moisture.
Embodiment 11 gets alumina-silicate ceramic fibre 60.0kg, add carboxymethyl cellulose 0.5kg, aluminium colloidal sol 30.0kg, swelling perlite powder 20.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 150 ℃, is finished product after removing moisture.
Embodiment 12 gets alumina-silicate ceramic fibre 40.0kg, add cationic polyacrylamide 1.0kg, cationic starch 0.5kg, ordinary Portland cement 20.0kg, silicon sol 10.0kg, expansion ground silica 20.0kg, ground silica 10.0kg and water fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 48 hours under the temperature about 100 ℃, is finished product after removing moisture.
Embodiment 13 gets alumina-silicate ceramic fibre 40.0kg, add carboxymethyl cellulose 1.0kg, cationic starch 0.5kg, high-alumina cement 20.0kg, silicon sol 10.0kg, ground silica 20.0kg, expansion ground silica 10.0kg and water fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 100 ℃, is finished product after removing moisture.
Embodiment 14 gets alumina-silicate ceramic fibre 40.0kg, add polyacrylamide 0.5kg, aluminium colloidal sol 15.0kg, water glass 15.0kg, swelling perlite powder 15.0kg, silicon powder 15.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 120 ℃, is finished product after removing moisture.
Embodiment 15 gets alumina-silicate ceramic fibre 40.0kg, add polyacrylamide 0.5kg, carboxymethyl cellulose 1.0kg, silicon sol 10.0kg, aluminium colloidal sol 20.0kg, ground silica 10.0kg, silicon powder 10.0kg and water fully stir, mixed pulp, adopt the hand form block method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 130 ℃, is finished product after removing moisture.
Embodiment 16 gets alumina-silicate ceramic fibre 50.0kg, add anionic polyacrylamide 1.0kg, ordinary Portland cement 25.0kg, ground silica 25.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 48 hours under the temperature about 100 ℃, is finished product after removing moisture.
Embodiment 17 gets alumina-silicate ceramic fibre 50.0kg, add cationic starch 0.5kg, silicon sol 10.0kg, expansion ground silica 20.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 100 ℃, is finished product after removing moisture.
Embodiment 18 gets alumina-silicate ceramic fibre 50.0kg, add carboxymethyl cellulose 1.5kg, aluminium colloidal sol 20.0kg, swelling perlite powder 30.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 140 ℃, is finished product after removing moisture.
Embodiment 19 gets alumina-silicate ceramic fibre 50.0kg, add cationic starch 0.5kg, water glass 30.0kg, silicon powder 20.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 130 ℃, is finished product after removing moisture.
Embodiment 20 gets alumina-silicate ceramic fibre 60.0kg, add polyacrylamide 1.0kg, ordinary Portland cement 25.0kg, ground silica 30.0kg and water, fully stir, mixed pulp, adopt the mechanical presses method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 150 ℃, is finished product after removing moisture.
Embodiment 21 gets alumina-silicate ceramic fibre 40.0kg, add cationic starch 1.0kg, silicon sol 20.0kg, swelling perlite powder 25.0kg and water, fully stir, mixed pulp, adopt manual assembly to produce wet base then, wet base is dry more than 24 hours under the temperature about 100 ℃, is finished product after removing moisture.
Embodiment 22 gets alumina-silicate ceramic fibre 40.0kg, adds polyacrylamide 0.5kg, carboxymethyl cellulose 0.5kg, cationic starch 0.5kg, silicon sol 10.0kg, aluminium colloidal sol 10.0kg, water glass 10.0kg, ground silica 10.0kg, silicon powder 10.0kg, swelling perlite powder 10.0kg and water, fully stir, mixed pulp, adopt the hand form block method of forming to produce wet base then, wet base is dry more than 24 hours under the temperature about 130 ℃, is finished product after removing moisture.
Embodiment 23 gets alumina-silicate ceramic fibre 60.0kg, add polyacrylamide 0.5kg, carboxymethyl cellulose 0.5kg, cationic starch 0.5kg, cement 10.0kg, silicon sol 10.0kg, aluminium colloidal sol 5.0kg, water glass 5.0kg, ground silica 5.0kg, silicon powder 5.0kg, swelling perlite powder 10.0kg, expansion ground silica 10.0kg and water, fully stir, mixed pulp, adopt the hand form block method of forming to produce wet base then, wet base is dry more than 48 hours under the temperature about 100 ℃, is finished product after removing moisture.
Claims (5)
1, a kind of ceramic fiber warming plate, form by ceramic fiber, inorganic bonding agent, organic bond and additive, it is characterized in that the weight ratio of ceramic fiber, inorganic bonding agent, organic bond and additive is: 40～60: 20～30: 0.5～1.5: 20～30.
2, ceramic fiber warming plate according to claim 1 is characterized in that organic bond is one or more the mixture in polyacrylamide, cationic starch or the carboxymethyl cellulose.
3, ceramic fiber warming plate according to claim 1 is characterized in that inorganic bonding agent is one or more the mixture in cement, silicon sol, aluminium colloidal sol or the water glass.
4, ceramic fiber warming plate according to claim 1 is characterized in that additive is one or more the mixture in ground silica, expansion ground silica, swelling perlite powder or the silicon powder.
5, the preparation method of the described ceramic fiber warming plate of a kind of claim 1, it is characterized in that with the ceramic fiber being base material, add inorganic bonding agent, organic bond, additive and water, carry out abundant slurrying, adopt mechanical presses moulding or manual assembly to produce wet base then, through 100～150 ℃ drying treatment.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021208549A CN1186286C (en) | 2002-06-06 | 2002-06-06 | Ceramic fibre thermal-insulating boara and making method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021208549A CN1186286C (en) | 2002-06-06 | 2002-06-06 | Ceramic fibre thermal-insulating boara and making method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN1385388A true CN1385388A (en) | 2002-12-18 |
| CN1186286C CN1186286C (en) | 2005-01-26 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB021208549A Expired - Lifetime CN1186286C (en) | 2002-06-06 | 2002-06-06 | Ceramic fibre thermal-insulating boara and making method thereof |
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Cited By (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1300062C (en) * | 2005-10-14 | 2007-02-14 | 宜兴天霸非金属材料有限公司 | Setting accelerated fibre fire-proof plastic and production thereof |
| CN1308559C (en) * | 2003-11-24 | 2007-04-04 | 山东鲁阳股份有限公司 | Human body fluid soluble inorganic ceramic fiber sound absorption board and process of production |
| US7328756B2 (en) | 2004-01-16 | 2008-02-12 | Halliburton Energy Serivces, Inc. | Settable fluids comprising particle-size distribution-adjusting agents and methods of use |
| CN100396631C (en) * | 2005-08-05 | 2008-06-25 | 山东鲁阳股份有限公司 | Method for producing mullite crystal refractory fiber blanket and its product |
| CN103253943A (en) * | 2013-04-17 | 2013-08-21 | 孝义市和中兴矿产有限公司 | Sintering method for shaped product of fire resistant material by utilizing alumina red mud as binding agent |
| CN104295858A (en) * | 2013-07-15 | 2015-01-21 | 慈溪市飞龙电器有限公司 | Thermal insulating layer structure for refrigerator and freezer |
| CN105271960A (en) * | 2014-07-14 | 2016-01-27 | 北新集团建材股份有限公司 | Electromagnetic radiation resistant heat insulation sheet and making method thereof |
| CN105481339A (en) * | 2015-12-25 | 2016-04-13 | 山东鲁阳节能材料股份有限公司 | Vacuum insulation board core veneer for buildings and preparation method thereof |
| CN105503118A (en) * | 2015-12-15 | 2016-04-20 | 中国地质科学院郑州矿产综合利用研究所 | Perlite insulation board with good comprehensive performance and preparation method thereof |
| CN105732062A (en) * | 2016-01-13 | 2016-07-06 | 洛阳西格马炉业股份有限公司 | Fiber-reinforced composite bearing thermal-insulation board and preparation method thereof |
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| CN106536450A (en) * | 2014-04-25 | 2017-03-22 | 派罗特克工程材料有限公司 | Castable refractory material |
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| CN107698235A (en) * | 2017-10-25 | 2018-02-16 | 福建德化五洲陶瓷股份有限公司 | A kind of high brightness under-glaze red porcelain and its manufacturing process |
| CN110548862A (en) * | 2019-10-18 | 2019-12-10 | 湛江市红鹰铭德新材料科技有限公司 | Ceramic fiber thermal insulation material covered with aluminum film |
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| CN111410544A (en) * | 2020-04-29 | 2020-07-14 | 成都天道化工技术有限公司 | Method for manufacturing non-flexible refractory fiber product |
| CN111662067A (en) * | 2020-06-05 | 2020-09-15 | 深圳市达鸿新材料科技有限公司 | Aluminum silicate high-temperature-resistant cotton for fireproof coiled material and preparation method thereof |
| CN112645677A (en) * | 2020-12-24 | 2021-04-13 | 山东鲁阳节能材料股份有限公司 | High-low temperature composite high-density ceramic fiber board and preparation method thereof |
| CN112710153A (en) * | 2021-02-05 | 2021-04-27 | 中钢南京环境工程技术研究院有限公司 | Preparation method of large-size machinable refractory heat-insulating plate |
| CN114804808A (en) * | 2022-05-30 | 2022-07-29 | 南京赤博环保科技有限公司 | Ceramic fiber filter element and preparation process thereof |
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2002
- 2002-06-06 CN CNB021208549A patent/CN1186286C/en not_active Expired - Lifetime
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| CN1308559C (en) * | 2003-11-24 | 2007-04-04 | 山东鲁阳股份有限公司 | Human body fluid soluble inorganic ceramic fiber sound absorption board and process of production |
| US7328756B2 (en) | 2004-01-16 | 2008-02-12 | Halliburton Energy Serivces, Inc. | Settable fluids comprising particle-size distribution-adjusting agents and methods of use |
| CN100396631C (en) * | 2005-08-05 | 2008-06-25 | 山东鲁阳股份有限公司 | Method for producing mullite crystal refractory fiber blanket and its product |
| CN1300062C (en) * | 2005-10-14 | 2007-02-14 | 宜兴天霸非金属材料有限公司 | Setting accelerated fibre fire-proof plastic and production thereof |
| CN103253943A (en) * | 2013-04-17 | 2013-08-21 | 孝义市和中兴矿产有限公司 | Sintering method for shaped product of fire resistant material by utilizing alumina red mud as binding agent |
| CN104295858A (en) * | 2013-07-15 | 2015-01-21 | 慈溪市飞龙电器有限公司 | Thermal insulating layer structure for refrigerator and freezer |
| CN106536450A (en) * | 2014-04-25 | 2017-03-22 | 派罗特克工程材料有限公司 | Castable refractory material |
| CN105271960A (en) * | 2014-07-14 | 2016-01-27 | 北新集团建材股份有限公司 | Electromagnetic radiation resistant heat insulation sheet and making method thereof |
| CN107116188A (en) * | 2015-10-20 | 2017-09-01 | 派罗特克工程材料有限公司 | Lip for continuous casting process |
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| CN111410544A (en) * | 2020-04-29 | 2020-07-14 | 成都天道化工技术有限公司 | Method for manufacturing non-flexible refractory fiber product |
| CN111662067A (en) * | 2020-06-05 | 2020-09-15 | 深圳市达鸿新材料科技有限公司 | Aluminum silicate high-temperature-resistant cotton for fireproof coiled material and preparation method thereof |
| CN112645677A (en) * | 2020-12-24 | 2021-04-13 | 山东鲁阳节能材料股份有限公司 | High-low temperature composite high-density ceramic fiber board and preparation method thereof |
| CN112645677B (en) * | 2020-12-24 | 2022-11-01 | 山东鲁阳节能材料股份有限公司 | High-low temperature composite high-density ceramic fiber board and preparation method thereof |
| CN112710153A (en) * | 2021-02-05 | 2021-04-27 | 中钢南京环境工程技术研究院有限公司 | Preparation method of large-size machinable refractory heat-insulating plate |
| CN114804808A (en) * | 2022-05-30 | 2022-07-29 | 南京赤博环保科技有限公司 | Ceramic fiber filter element and preparation process thereof |
| CN114956692A (en) * | 2022-06-22 | 2022-08-30 | 宜兴市爱博纤维制品有限公司 | Ceramic fiber simulation fake material and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1186286C (en) | 2005-01-26 |
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