CN106036981A - Milk-flavored tobacco flavor based on spice threshold and allocation method of tobacco flavor - Google Patents
Milk-flavored tobacco flavor based on spice threshold and allocation method of tobacco flavor Download PDFInfo
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- CN106036981A CN106036981A CN201610422430.1A CN201610422430A CN106036981A CN 106036981 A CN106036981 A CN 106036981A CN 201610422430 A CN201610422430 A CN 201610422430A CN 106036981 A CN106036981 A CN 106036981A
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- threshold value
- acid
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- spice
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Abstract
The invention relates to a milk-flavored tobacco flavor based on a spice threshold and an allocation method of the tobacco flavor. The tobacco flavor consists of the following raw materials in percentage by weight: 1-50% of an aroma base and 50-99% of a solvent, wherein the aroma base consists of the following components in parts by weight: 0.02-6 parts of 3-methyl pentanoic acid, 0.1-5 parts of ethyl vanillin, 0.1-5 parts of butanedione, 0.1-5 parts of [gamma]-valerolactone, 0.05-10 parts of isobutyric acid, 0.1-10 parts of vanillin, 0.1-10 parts of [gamma]-butyrolactone, 1-3 parts of 4-methyl pentanoic acid and 0.1-2 parts of 2-methylbutanoic acid. The milk-flavored tobacco flavor disclosed by the invention is added to tobacco shreds and a cigarette product is made by virtue of a conventional technology in the field; the result of a sensory evaluation test shows that compared with a blank sample which is free from the milk-flavored tobacco flavor disclosed by the invention, a cigarette sample, which is added with the milk-flavored tobacco flavor, has better aroma quality and obvious milk smell; and in addition, aftertaste is improved and offensive odor is masked.
Description
Technical field
The invention belongs to essence technical field, be specifically related to a kind of milk odor type flavouring essence for tobacco based on spice threshold value and
Concocting method.
Background technology
Along with improving constantly of our people's living standard, consumer is to the sucking quality of Medicated cigarette and safety the most increasingly
Pay close attention to.State Tobacco Monopoly Bureau changing and the development trend of domestic and international tobacco business according to cigarette market, it is proposed that " with harm reduction
The burnt engineering of fall is served as theme, and attaches most importance to developing Chinese-style cigarette, General Promotion Chinese tobacco scientific and technological level " developing direction.Along with
Carrying out of lowering harm and decreasing coking engineering, the burnt technology fragrant with guarantor of fall has become the key of restriction Medicated cigarette development, particularly at current tar content
In the case of having had the biggest decline, the most significantly dropping Jiao while keeping cigarette odor-absorbing, its difficulty will be got over
Come the biggest.How while reducing cigarette tar content, make Medicated cigarette fragrance remain to as consumer and accepted, have become as Medicated cigarette
The main attack problem of industry, is also to affect the key factor that China's cigarette product tar reduces.
Essence and flavoring agent not only can give the unique taste of Medicated cigarette and style, and can cover Medicated cigarette shortcoming, improves Medicated cigarette
Fragrance and jealous, promotes Medicated cigarette physical property.Along with country's " perfumery engineering " implementation, essence and flavoring agent is at Chinese-style cigarette core
Effect during heart technology is formed is more and more important, especially in terms of constructing Medicated cigarette category differentiation.This category difference causes
People bring style and features and the product individuality of uniqueness when aspirating kinds of cigarettes brand, become consumer and rely selection consumption
Key foundation.
Milk note is a kind of very important note in Virginian-type cigarette aromatic style.Exploitation has the cigarette of typical milk
With essence, and it is applied to Medicated cigarette, can not only effectively highlight Medicated cigarette milk aromatic style, and Medicated cigarette can be significantly improved and produce
Product quality.But, milk odor type flavouring essence for tobacco and concocting method thereof there is not yet correlational study report up to now.
Currently, Medicated cigarette perfumery relies primarily on experience and the talent of perfumer, lacks theoretical direction and data supporting.In Medicated cigarette
Threshold value refer to the least concentration value that fragrance matter is experienced by the sense organ of people in cigarette smoke.Different cigarettes is fragrant
Expecting the threshold value of Medicated cigarette is deposited difference, Medicated cigarette perfumery is had important practical significance by this diversity.Threshold value is the least
Spice, the strongest to the effect showing Medicated cigarette odor characteristic of the same race, contribution the biggest, vice versa.The cigarette that Medicated cigarette perfumery obtains is used
Essence is a kind of complicated flavor system being made up of Multiple components, constitute the content of each of this system cigarette monomer perfume with
The ratio of threshold value can be described as this spice activity threshold in system, and according to the different tobacco aromatics using active thresholds in system
Value size, can determine whether that different tobacco aromatics using is to the action effect of fragrance complex system and percentage contribution.It can thus be seen that according to
Threshold value size, in conjunction with Financial cost factor, in rational allocation target flavor systems, the activity threshold of each constituent, has
Carry out Medicated cigarette perfumery pointedly, the utilization rate of tobacco aromatics using can be effectively improved, strengthen the high efficiency of Medicated cigarette perfumery.
Therefore, it is necessary to by the threshold value using for reference tobacco aromatics using, with the work of constituent each in target flavor systems
Property threshold value be measurement index, design milk flavor essence concocting method, and carry out Medicated cigarette perfumery according to the method, it is thus achieved that performance is excellent
Milk odor type flavouring essence for tobacco more.
Summary of the invention
Theoretical direction and the defect of data supporting is lacked, by using for reference during present invention aim to overcome that Medicated cigarette perfumery
Tobacco aromatics using threshold value, and combine spice Costco Wholesale, in target flavor systems, the activity threshold of each constituent is for weighing apparatus
Figureofmerit, carries out cigarette flavoring essence allotment, it is thus achieved that a kind of novel milk odor type flavouring essence for tobacco, this flavouring essence for tobacco can not only be the most convex
The milk aromatic style of aobvious Medicated cigarette, and cigarette product quality can be significantly improved.
For achieving the above object, the present invention adopts the following technical scheme that
A kind of milk odor type flavouring essence for tobacco concocting method based on spice threshold value, comprises the steps:
(1) first determine that material based on spice threshold value screens and ratio Controlling principle:
1. first-selected little (the threshold value ＜ 1.0 × 10 of threshold value-6 Ng/ props up) spice as material of main part, the work of material of main part
Property threshold value sum accounts for the 55-85% of all spices activity threshold summation.Compared with the spice that threshold value is big, threshold value is little
Spice is bigger to the contribution improving cigarette quality, highlights Medicated cigarette milk better, therefore using the little spice of threshold value as
Main body spice, when allotment, the most uses, make the activity threshold sum of these spice account for the activity threshold summation of all spices
The 55-85% of (gross activity threshold value).
2. by relatively big for threshold value (threshold value >=1.0 × 10-6 Ng/ props up) but the perfume (or spice) of price relatively low (500 yuan/kg of price ＜)
Material accounts for the 10-30% of all spices activity threshold summation as auxiliary material, the activity threshold sum of auxiliary material.Due to threshold value
Less main body spice also needs other taste condiments to assist, therefore, relatively big in threshold value and close to time, in conjunction with its Financial cost,
The spice that preferably price is relatively low, makes the activity threshold sum of these spice account for the 10-30% of gross activity threshold value.
3. (threshold value >=1.0 × 10 big for threshold value-6 Ng/ props up) and price higher (price >=500 yuan/kg)
Spice, then as far as possible few with (but except the spice of cigarette sensory quality can be obviously improved), make these spice activity threshold it
With the 5-15% accounting for gross activity threshold value.
(2) material is collected and is investigated
Collect have carry raise the conventional tobacco aromatics using vanillin of milk, ethyl vanillin, diacetyl, gamma-valerolactone, isopropylformic acid.,
3 methylvaleric acid, gamma-butyrolacton, 4-methylvaleric acid, succinic acid, caproic acid, 3 methylvaleric acid, 2-penetenoic acid and 2-Methyl Butyric Acid
Deng, and investigate each conventional tobacco aromatics using threshold value in Medicated cigarette and price.
(3) material screening and flavor deployment
The flavor deployment principle determined according to step (1) carries out material screening:
1. ethyl vanillin, diacetyl, gamma-valerolactone, 3 methylvaleric acid threshold value less, respectively less than 1.0 × 10-6 ng/
, therefore be material of main part；
2. other spice threshold values are the biggest, are all higher than 1.0 × 10-6 Ng/ props up, but wherein vanillin, isopropylformic acid., γ-Ding Nei
The price of ester is respectively less than 500 yuan/kg, and Financial cost is low, will be as auxiliary material；
3. residue spice threshold value is all higher than 1.0 × 10-6 Ng/ props up and price is all higher than 500 yuan/kg, therefore in formula to the greatest extent
The few use of amount, but wherein 4-methylvaleric acid, 2-Methyl Butyric Acid can be obviously improved cigarette sensory quality, therefore also into composition.
In the present invention, the evaluation reference literature of each tobacco aromatics using threshold value (Chen Zhifei, Yang Jing, Ma Yuping, etc. Nicotiana tabacum L.
The foundation of spice threshold value sensory evaluation method and application [J]. Nicotiana tabacum L. science and technology, 2016,49(4): the method in 30-36) is entered
OK.
After determining material of main part and auxiliary material, first adjust the ratio of each perfume monomer, it is thus achieved that smell perfume (or spice) relatively harmony
Initial formulation, then with blank Medicated cigarette as carrier, formula is finely adjusted, is finally obtained one and can highlight milk note
The novel milk odor type flavouring essence for tobacco of cigarette product quality can be improved again.That is, a kind of milk odor type cigarette based on spice threshold value is used
Essence, it is made up of the raw material of following weight percentage ratio: perfume base 1-50%, solvent 50-99%；Wherein, the weight of each component of perfume base
Amount part composition see table:
。
Concrete, described solvent be the one in ethanol, propylene glycol, triacetyl glycerine, water, triethyl citrate and glycerol or
Two or more mixture.
The application in Medicated cigarette of the above-mentioned milk odor type flavouring essence for tobacco, wherein, described milk odor type flavouring essence for tobacco is in Medicated cigarette
Addition be preferably 0.05wt%.
Compared to the prior art, beneficial effects of the present invention:
1) present invention innovatively during Medicated cigarette perfumery introduce spice threshold value, integrated economics cost factor, have for
Property ground carry out Medicated cigarette perfumery, it is thus achieved that the milk flavouring essence for tobacco of superior performance, effectively enhance the high efficiency of Medicated cigarette perfumery, improve
The utilization rate of tobacco aromatics using, reduces Medicated cigarette perfumery Financial cost.Meanwhile, overcome conventional Medicated cigarette perfumery and purely rely on experience
Defect, provides new approaches for Modern cigarette industry perfumery.
2) milk odor type flavouring essence for tobacco of the present invention is added in tobacco shred, use this area routine techniques to make Medicated cigarette and produce
Product, sensory evaluation result of the test shows: compare with the blank sample being not added with milk odor type flavouring essence for tobacco of the present invention, the volume after interpolation
Cigarette sample aroma quality improves, and milk breath is obvious, and improves pleasant impression, masks miscellaneous QI.
Detailed description of the invention
Below in conjunction with embodiment, technical scheme is discussed in detail further, but protection scope of the present invention
It is not limited thereto.
A kind of milk odor type flavouring essence for tobacco concocting method based on spice threshold value, comprises the steps:
(1) first determine that material based on spice threshold value screens and ratio Controlling principle:
1. first-selected little (the threshold value ＜ 1.0 × 10 of threshold value-6 Ng/ props up) spice as material of main part, the work of material of main part
Property threshold value sum accounts for the 55-85% of all spices activity threshold summation.Compared with the spice that threshold value is big, threshold value is little
Spice is bigger to the contribution improving cigarette quality, highlights Medicated cigarette milk better, therefore using the little spice of threshold value as
Main body spice, when allotment, the most uses, make the activity threshold sum of these spice account for the activity threshold summation of all spices
The 55-85% of (gross activity threshold value).
2. by relatively big for threshold value (threshold value >=1.0 × 10-6 Ng/ props up) but the perfume (or spice) of price relatively low (500 yuan/kg of price ＜)
Material accounts for the 10-30% of all spices activity threshold summation as auxiliary material, the activity threshold sum of auxiliary material.Due to threshold value
Less main body spice also needs other taste condiments to assist, therefore, relatively big in threshold value and close to time, in conjunction with its Financial cost,
The spice that preferably price is relatively low, makes the activity threshold sum of these spice account for the 10-30% of gross activity threshold value.
3. (threshold value >=1.0 × 10 big for threshold value-6 Ng/ props up) and price higher (price >=500 yuan/kg)
Spice, then as far as possible few with (but except the spice of cigarette sensory quality can be obviously improved), make these spice activity threshold it
With the 5-15% accounting for gross activity threshold value.
(2) material is collected and is investigated
Collect have carry raise the conventional tobacco aromatics using vanillin of milk, ethyl vanillin, diacetyl, gamma-valerolactone, isopropylformic acid.,
3 methylvaleric acid, gamma-butyrolacton, 4-methylvaleric acid, succinic acid, caproic acid, 3 methylvaleric acid, 2-penetenoic acid and 2-Methyl Butyric Acid
Deng, and investigate each conventional tobacco aromatics using threshold value in Medicated cigarette and price.
(3) material screening and flavor deployment
The flavor deployment principle determined according to step (1) carries out material screening:
1. ethyl vanillin, diacetyl, gamma-valerolactone, 3 methylvaleric acid threshold value less, respectively less than 1.0 × 10-6 ng/
, therefore be material of main part；
2. other spice threshold values are the biggest, are all higher than 1.0 × 10-6 Ng/ props up, but wherein vanillin, isopropylformic acid., γ-Ding Nei
The price of ester is respectively less than 500 yuan/kg, and Financial cost is low, will be as auxiliary material；
3. residue spice threshold value is all higher than 1.0 × 10-6 Ng/ props up and price is all higher than 500 yuan/kg, therefore in formula to the greatest extent
The few use of amount, but wherein 4-methylvaleric acid, 2-Methyl Butyric Acid can be obviously improved cigarette sensory quality, therefore also into composition.
Embodiment 1-3
Each raw material weight proportioning of milk odor type flavouring essence for tobacco described in embodiment 1 to 3 is as shown in table 1 to table 3, wherein, and embodiment 1
Middle solvent is ethanol, and in embodiment 2, solvent is propylene glycol, and in embodiment 3, solvent is triethyl citrate.
The proportioning raw materials of milk odor type flavouring essence for tobacco described in table 1 embodiment 1
| Raw material | Quality (g) | Activity threshold accounting (%) |
| 3 methylvaleric acid | 0.05 | 15 |
| Ethyl vanillin | 0.15 | 8 |
| Diacetyl | 0.4 | 15 |
| Gamma-valerolactone | 1.4 | 31 |
| Isopropylformic acid. | 2.5 | 1.5 |
| Vanillin | 4.0 | 1.5 |
| Gamma-butyrolacton | 2.0 | 15 |
| 4-methylvaleric acid | 1.5 | 8 |
| 2-Methyl Butyric Acid | 0.6 | 5 |
| Solvent | 87.40 | - |
The proportioning raw materials of milk odor type flavouring essence for tobacco described in table 2 embodiment 2
| Raw material | Quality (g) | Activity threshold accounting (%) |
| 3 methylvaleric acid | 0.10 | 27 |
| Ethyl vanillin | 0.15 | 7 |
| Diacetyl | 0.2 | 7 |
| Gamma-valerolactone | 1.4 | 27 |
| Isopropylformic acid. | 5 | 3 |
| Vanillin | 4.0 | 2 |
| Gamma-butyrolacton | 3.0 | 20 |
| 4-methylvaleric acid | 0.3 | 2 |
| 2-Methyl Butyric Acid | 0.8 | 5 |
| Solvent | 85.05 | - |
The proportioning raw materials of milk odor type flavouring essence for tobacco described in table 3 embodiment 3
| Raw material | Quality (g) | Activity threshold accounting (%) |
| 3 methylvaleric acid | 0.05 | 13 |
| Ethyl vanillin | 0.6 | 26 |
| Diacetyl | 0.8 | 26 |
| Gamma-valerolactone | 0.7 | 13 |
| Isopropylformic acid. | 2.5 | 1 |
| Vanillin | 4.0 | 1 |
| Gamma-butyrolacton | 2.0 | 13 |
| 4-methylvaleric acid | 1.2 | 5 |
| 2-Methyl Butyric Acid | 0.4 | 2 |
| Solvent | 87.75 | - |
The preparation method of milk odor type flavouring essence for tobacco described in above-described embodiment 1-3, particularly as follows: take each component in proportion and mix
Obtaining perfume base, joined by perfume base in solvent, stirring, to being completely dissolved, to obtain final product.
The milk odor type flavouring essence for tobacco that embodiment 1-3 is allocated is added in tobacco shred in the ratio of 0.05wt%, uses this
Field routine techniques makes cigarette product.Then according to " YC/T 415-2011 Nicotiana tabacum L. is in goods sensory evaluation method " is carried out
Sensory evaluation.Result is as shown in table 4 and 5.
Table 4 sense organ evaluating meter
| Group | Sensory evaluation |
| Blank | Aroma quality is medium, and perfume quantity is less, flue gas slightly bitterness, slightly miscellaneous QI |
| Embodiment 1 | Aroma quality improves, and perfume quantity is relatively sufficient, and slightly milk breath, zest alleviates, and pleasant impression is the most comfortable |
| Embodiment 2 | Aroma quality improves, and perfume quantity is relatively sufficient, and milk breath is obvious, and micro-have miscellaneous QI, and pleasant impression is the most comfortable |
| Embodiment 3 | Aroma quality improves, and perfume quantity is relatively sufficient, and milk breath is denseer, and micro-have miscellaneous QI, and pleasant impression is the most comfortable |
Table 5 sense organ evaluating meter (GB marking)
| Group | Gloss (5) | Fragrance (32) | Harmony (6) | Miscellaneous QI (12) | Zest (20) | Pleasant impression (25) | Add up to |
| Blank | 5.00 | 29.00 | 5.00 | 10.50 | 17.50 | 22.00 | 89.00 |
| Embodiment 1 | 5.00 | 29.08 | 5.00 | 10.61 | 17.83 | 22.07 | 89.59 |
| Embodiment 2 | 5.00 | 29.17 | 5.00 | 10.68 | 17.85 | 22.15 | 89.85 |
| Embodiment 3 | 5.00 | 29.26 | 5.00 | 10.73 | 17.93 | 22.24 | 90.16 |
Result shows: comparing with blank sample, the aroma quality of the cigarette sample adding milk odor type flavouring essence for tobacco improves, milk note
Significantly improving, can improve pleasant impression simultaneously, cover miscellaneous QI, milk note score value all improves more than 0.5 point.
Claims (5)
1. a milk odor type flavouring essence for tobacco based on spice threshold value, it is characterised in that by the raw material group of following weight percentage ratio
Become: perfume base 1-50%, solvent 50-99%；Wherein, the weight portion composition of each component of perfume base see table:
。
2. milk odor type flavouring essence for tobacco as claimed in claim 1, it is characterised in that described solvent is ethanol, propylene glycol, three vinegar
One or more mixture in acid glyceride, water, triethyl citrate and glycerol.
3. milk odor type flavouring essence for tobacco application in Medicated cigarette described in claim 1 or 2.
4. milk odor type flavouring essence for tobacco application in Medicated cigarette as claimed in claim 3, it is characterised in that described milk odor type cigarette
It is 0.05wt% with essence addition in Medicated cigarette.
5. the concocting method of milk odor type flavouring essence for tobacco described in a claim 1, it is characterised in that comprise the steps:
(1) flavor deployment principle determines
First determine that material based on spice threshold value screens and ratio Controlling principle:
1. first-selected threshold value ＜ 1.0 × 10-6 The spice that ng/ props up accounts for as material of main part, the activity threshold sum of material of main part
The 55-85% of all spices activity threshold summation；
2. by threshold value >=1.0 × 10-6Ng/ props up but the spice of 500 yuan/kg of price ＜ is as auxiliary material, auxiliary material
Activity threshold sum accounts for the 10-30% of all spices activity threshold summation；
3. for threshold value >=1.0 × 10-6Ng/ props up and the spice of price >=500 yuan/kg, and use less makes the work of these spice
Property threshold value sum accounts for the 5-15% of all spices activity threshold summation；
(2) material is collected and is investigated
Collect have carry raise the conventional tobacco aromatics using vanillin of milk, ethyl vanillin, diacetyl, gamma-valerolactone, isopropylformic acid.,
3 methylvaleric acid, gamma-butyrolacton, 4-methylvaleric acid, succinic acid, caproic acid, 3 methylvaleric acid, 2-penetenoic acid and 2-Methyl Butyric Acid,
And investigate each conventional tobacco aromatics using threshold value in Medicated cigarette and price；
(3) material screening and flavor deployment
The flavor deployment principle determined according to step (1) carries out material screening:
1. ethyl vanillin, diacetyl, gamma-valerolactone, the threshold value of 3 methylvaleric acid are respectively less than 1.0 × 10-6Ng/ props up, therefore
As material of main part；
2. vanillin, isopropylformic acid., the threshold value of gamma-butyrolacton are all higher than 1.0 × 10-6Ng/ prop up but price be respectively less than 500 yuan/
Kg, pretends as auxiliary material；
3. 4-methylvaleric acid, 2-Methyl Butyric Acid threshold value are more than 1.0 × 10-6Ng/ props up and price is more than 500 yuan/kg, but can carry
Rise cigarette sensory quality, therefore also into composition.
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|---|---|---|---|
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109135922A (en) * | 2018-07-25 | 2019-01-04 | 河南中烟工业有限责任公司 | A kind of recombination maple maple flavour, its reconstructing method and application in cigarette based on Low Flavour Threshold |
| CN112237296A (en) * | 2019-07-18 | 2021-01-19 | 深圳市潘虎包装设计有限公司 | Original flavor yoghourt capsule for cigarettes and preparation method thereof |
| CN115725367A (en) * | 2022-11-22 | 2023-03-03 | 浙江中烟工业有限责任公司 | Tobacco essence containing tobacco flower extract and preparation method and application thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109135922A (en) * | 2018-07-25 | 2019-01-04 | 河南中烟工业有限责任公司 | A kind of recombination maple maple flavour, its reconstructing method and application in cigarette based on Low Flavour Threshold |
| CN109135922B (en) * | 2018-07-25 | 2021-12-17 | 河南中烟工业有限责任公司 | Recombinant maple essence based on aroma threshold, reconstruction method thereof and application of recombinant maple essence in cigarettes |
| CN112237296A (en) * | 2019-07-18 | 2021-01-19 | 深圳市潘虎包装设计有限公司 | Original flavor yoghourt capsule for cigarettes and preparation method thereof |
| CN115725367A (en) * | 2022-11-22 | 2023-03-03 | 浙江中烟工业有限责任公司 | Tobacco essence containing tobacco flower extract and preparation method and application thereof |
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| Publication number | Publication date |
|---|---|
| CN106036981B (en) | 2018-06-26 |
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