CN103708751B - 包含水泥窑粉尘、玻璃化页岩、沸石和/或无定形二氧化硅的粘结组合物，及相关方法 - Google Patents

包含水泥窑粉尘、玻璃化页岩、沸石和/或无定形二氧化硅的粘结组合物，及相关方法 Download PDF

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CN103708751B
CN103708751B CN201310478308.2A CN201310478308A CN103708751B CN 103708751 B CN103708751 B CN 103708751B CN 201310478308 A CN201310478308 A CN 201310478308A CN 103708751 B CN103708751 B CN 103708751B
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microns
particle diameter
zeolite
kiln dust
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CN103708751A (zh
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C·W·罗迪
R·L·科温顿
J·查特吉
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Halliburton Energy Services Inc
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B18/00—Use of agglomerated or waste materials or refuse as fillers for mortars, concrete or artificial stone; Treatment of agglomerated or waste materials or refuse, specially adapted to enhance their filling properties in mortars, concrete or artificial stone
    • C04B18/04—Waste materials; Refuse
    • C04B18/16—Waste materials; Refuse from building or ceramic industry
    • C04B18/162—Cement kiln dust; Lime kiln dust
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/021—Ash cements, e.g. fly ash cements ; Cements based on incineration residues, e.g. alkali-activated slags from waste incineration ; Kiln dust cements
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C09K8/46—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing inorganic binders, e.g. Portland cement
    • C09K8/467—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing inorganic binders, e.g. Portland cement containing additives for specific purposes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/91—Use of waste materials as fillers for mortars or concrete

Abstract

本申请提供了粘结组合物，其包含水、水泥窑粉尘、玻璃化页岩、沸石和/或无定形二氧化硅，其所具有的堆积体积分数使得液体的固体颗粒材料处于受阻沉降状态。本申请还提供了粘结方法，其使用包含水、水泥窑粉尘、玻璃化页岩、沸石和/或无定形二氧化硅的组合物，其所具有的堆积体积分数使得液体的固体颗粒材料处于受阻沉降状态。

Description

包含水泥窑粉尘、玻璃化页岩、沸石和/或无定形二氧化硅的粘结组合物，及相关方法
本申请是2006年10月4日提交的国际申请号为PCT/GB2006/003696，中国国家申请号为200680055312.6，发明名称为“包含水泥窑粉尘、玻璃化页岩、沸石和/或无定形二氧化硅，具有一定的堆积体积分数的粘结组合物，及相关方法”的发明专利申请的分案申请。
技术领域
本发明涉及粘结操作，更具体地，涉及通过利用一定的堆积体积分数制备的包含水、水泥窑粉尘(“CKD”)、玻璃化页岩(vitrifiedshale)、沸石和/或无定形二氧化硅的粘结组合物的用途，和相关的使用方法。
背景技术
粘结组合物(cementingcompositions)通常用于多种地下操作。可能涉及粘结组合物的地下应用包括但不限于初次注水泥、补注水泥和钻井操作。例如，水泥组合物用于初次注水泥操作，从而使管线(比如外壳和衬套)粘结在井孔中。在进行初次注水泥时，将水泥组合物泵入井孔壁和置于其中的管线的外表面之间的环形空间中。水泥组合物可在环形空间中固化，从而在其中形成硬化的基本不可渗透的水泥的环形壳，其充分支持并定位井孔中的管线，并将管线的外表面结合至井孔壁。水泥组合物还用于堵塞和废弃操作，以及补注水泥操作，比如堵塞井孔中的渗透区或断裂，堵塞管线中的破裂和孔洞等。粘结组合物还可用于表面应用，例如，建筑粘结。
迄今使用的粘结组合物通常包含波特兰水泥。波特兰水泥一般是粘结组合物的成本的主要部分。为了降低这种粘结组合物的成本，除波特兰水泥之外，或代替波特兰水泥，可在粘结组合物中包括其他固体颗粒组分。粘结组合物中的获得的多种固体颗粒材料的组合可引起“沉降效果(settlingeffect)”，其中不同尺寸的颗粒材料以不同的速度分别沉降。水泥组合物中固体的这种沉降可引起有缺陷的粘结过程以及使凝固的水泥不能提供区域隔离。因此，尤其需要用于油井水泥的改进的粘结组合物，其使用时不引起固体颗粒的沉降。
发明内容
本发明涉及粘结操作，更具体地，涉及通过具有一定的堆积体积分数(packingvolumefraction)制备的包含水、CKD、玻璃化页岩、沸石和/或无定形二氧化硅的粘结组合物的用途，和相关的使用方法。
在一个实施方案中，本发明提供一种组合物，其包含：水；和选自下列组中的至少三种颗粒材料：(a)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约7纳米到约50纳米的范围内；(b)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约0.05微米到约0.5微米的范围内；(c)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约0.5微米到约10微米的范围内；(d)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约10微米到约20微米的范围内；(e)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约20微米到约200微米的范围内；(f)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约200微米到约800微米的范围内；和(g)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，粒径大于约1毫米，其中该至少三种颗粒材料的固体体积总量具有最大堆积体积分数。
在一个实施方案中，本发明提供一种方法，其包括提供选自下列组中的至少三种颗粒材料的未水合的混合物：(a)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约7纳米到约50纳米的范围内；(b)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约0.05微米到约0.5微米的范围内；(c)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约0.5微米到约10微米的范围内；(d)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约10微米到约20微米的范围内；(e)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约20微米到约200微米的范围内；(f)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约200微米到约800微米的范围内；和(g)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，粒径大于约1毫米，其中所述至少三种颗粒材料的固体体积总量具有最大堆积体积分数；并向所述未水合的混合物中加入水以形成可固化组合物。
在一个实施方案中，本发明提供一种方法，其包括提供粘结组合物，其中所述粘结组合物包含水；和选自下列组中的至少三种颗粒材料：(a)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约7纳米到约50纳米的范围内；(b)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约0.05微米到约0.5微米的范围内；(c)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约0.5微米到约10微米的范围内；(d)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约10微米到约20微米的范围内；(e)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约20微米到约200微米的范围内；(f)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在约200微米到约800微米的范围内；和(g)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，粒径大于约1毫米，其中所述至少三种颗粒材料的固体体积总量具有最大堆积体积分数；并将所述粘结组合物置于地下构造中。
本发明的特征和优势对本领域技术人员而言是明显的。尽管本领域技术人员可作众多改变，但这些改变都在本发明的精神范围内。
优选实施方案
本发明涉及粘结操作，更具体地，涉及通过利用一定的堆积体积分数制备的包含水、CKD、玻璃化页岩、沸石和/或无定形二氧化硅的粘结组合物的用途，和相关的使用方法。本发明的粘结组合物可用于多种地下应用，包括初次注水泥、补注水泥和钻井操作。本发明的粘结组合物还可用于表面应用，例如，建筑粘结。
在一些实施方案中，本发明的粘结组合物包含水、CKD、玻璃化页岩、沸石和/或无定形二氧化硅，其利用了一定的堆积体积分数。本发明的粘结组合物还可按需包括任选的添加剂，包括但不限于水硬性水泥、其他的材料比如二氧化硅、赤铁矿或其他的铁氧化物、氢氧化钡、碳酸盐、氧化铝等，及有机产品比如塑料废料及其他可共存的废物。所述粘结组合物还可包括缓凝剂、速凝剂、分散剂、液体损失控制剂、轻质添加剂等。
本发明的粘结组合物应利用适合所需的特定应用的堆积体积分数。此处使用的术语“堆积体积分数”指的是液体中的固体颗粒材料的体积除以液体的总体积的值。选择优选的固体颗粒材料的尺寸范围，以及它们各自的比例，以提供最大的(或尽可能最大的)堆积体积分数以使液体处于受阻沉降(hinderedsettling)状态。众所周知，在这样的状态下，固体颗粒材料“一起”表现为多孔固体材料。受阻沉降状态被认为实际上相当于液体中的固体材料浓度比现有技术的高得多。
本发明由至少三个特征的组合组成，以获得最大的堆积体积分数。其一是使用至少三种颗粒材料，其中这至少三种颗粒材料的尺寸范围彼此“不连续”。本发明的另一个特征是这三种颗粒材料的比例的选择与混合相关，使得在混合时液体处于受阻沉降状态。另一个特征是这三种颗粒材料之间的比例的选择，根据它们各自的尺寸范围，使得至少对于液体体系中所有颗粒材料的总和，基本实现最大堆积体积分数。堆积体积分数在美国专利No.5,518,996中有进一步详细的描述，在此以引用的方式将其全部公开内容以引用的方式并入。
本发明使用至少三种颗粒材料，其包含CKD、玻璃化页岩、沸石和/或无定形二氧化硅。这些材料的尺寸可以是“超细”、“很细”、“细”、“小”、“中等”、“大”、“很大”的颗粒材料。“超细”颗粒材料的尺寸可以从约7纳米到约50纳米的范围内。“很细”颗粒材料的尺寸可以在从约0.05微米到约0.5微米的范围内。“细”颗粒材料的尺寸可以在从约0.5微米到约10微米的范围内。“小”颗粒材料的尺寸可以在从约10微米到约20微米的范围内。“中等”颗粒材料的尺寸可以在从约20微米到约200微米的范围内。“大”颗粒材料的尺寸可以在从约200微米到约800微米的范围内。“很大”颗粒材料的尺寸可以大于约1毫米。本领域技术人员可知，在组合物中选择的颗粒的比例取决于最终用途。无论在何种情况中，在给定的组合物中的颗粒和相对尺寸及浓度应基于这里公开的最大堆积体积分数来选择。
在某些实施方案中，本发明的粘结组合物可包含CKD，CKD是在水泥生产过程中产生的废料。此处使用的术语CKD指的是在水泥生产过程中从气流中除去并收集在集尘器中的部分煅烧的窑炉进料。从不同水泥生产得到的CKD的化学分析根据多个因素而变化，包括特定的窑炉进料、水泥生产操作的效率和相关的除尘系统。CKD一般可包含多种氧化物，比如SiO2、Al2O3、Fe2O3、CaO、MgO、SO3、Na2O、和K2O。在一些实施方案中，CKD可以以细颗粒材料存在。在其他的实施方案中，CKD可以小颗粒材料存在。在其他的实施方案中，CKD可以中等颗粒材料存在。在其他的实施方案中，CKD可以大颗粒材料存在。在某些实施方案中，CKD在本发明的粘结组合物中的含量可以在组合物的重量(“bwoc”)的约25%到约75%的范围内。
在某些实施方案中，本发明的粘结组合物包含的玻璃化页岩的量足以提供所需的抗压强度、密度、和/或成本。多种页岩均是合适的，包括那些包含硅、铝、钙和/或镁的页岩。玻璃化页岩的合适的实例包括但不限于“PRESSUR–FINELCM”材料和“PRESSUR-COARSELCM”材料，可从TXIEnergyServices，Inc.，Houston，Texas购得。在某些实施方案中，玻璃化页岩可以大颗粒材料存在。在其他实施方案中，玻璃化页岩可以很大颗粒材料存在。在某些实施方案中，玻璃化页岩在本发明的粘结组合物中的含量可以在bwoc为约10%到约30%的范围内。受益于本发明公开，本领域普通技术人员对于所选的应用可知合适的页岩加入量。
在某些实施方案中，本发明的粘结组合物可包含沸石。在一些实施方案中，沸石可以和玻璃化页岩共同使用。在其他的实施方案中，沸石可以替代玻璃化页岩。该选择可受多个因素的影响，比如水泥的抗压强度的总程度、水泥组合物形成抗压强度的时间，和组合物的密度。沸石一般是多孔的硅酸铝盐矿物，其可以是天然或合成材料。合成沸石基于与天然沸石相同类型的结构单元，可包含铝硅酸盐水合物。此处使用的术语“沸石”指的是所有天然和合成的沸石形式。在某些实施方案中，沸石可以细颗粒材料存在。在其他实施方案中，沸石可以小颗粒材料存在。在其他的实施方案中，沸石可以中等颗粒材料存在。在其他的实施方案中，沸石可以大颗粒材料存在。在某些实施方案中，沸石在本发明的粘结组合物中的含量可以在bwoc为约10%到约25%的范围内。
在某些实施方案中，用于本发明的合适的沸石可包括“方沸石”(水合的硅酸钠铝)、“硅锂铝石”(硅酸锂铝)、“锶沸石”(水合的硅酸锶钡钙铝)、“菱沸石”(水合的硅酸钙铝)、“斜发沸石”(水合的硅酸钠铝)、“八面沸石”(水合的硅酸钠钾钙镁铝)、“交沸石”(水合的硅酸钡铝)、“片沸石”(水合的硅酸钠钙铝)、“浊沸石”(水合的硅酸钙铝)、“中沸石”(硅酸钠钙铝)、“钠沸石”(水合的硅酸钠铝)、“方碱沸石”(水合的硅酸钾钠钙钡铝)、“钙十字沸石”(水合的硅酸钾钠钙铝)、“钙沸石”(水合的硅酸钙铝)、“淡红沸石”(水合的硅酸钙铝)、“辉沸石”(水合的硅酸钠钙铝)和“杆沸石”(水合的硅酸钠钙铝)及它们的组合。在某些实施方案中，用于本发明的合适的沸石包括菱沸石和斜发沸石。合适的沸石源的实例可从C2CZeoliteCorporationofCalgary，Canada获得。
在某些实施方案中，本发明的粘结组合物可包含无定形二氧化硅。无定形二氧化硅一般是硅铁制造方法的副产品，其中无定形二氧化硅可由在该方法的过程中作为中间体形成的气态硅低价氧化物SiO的氧化和冷凝而形成。合适的无定形二氧化硅源的实例可购自HalliburtonEnergyServices，Inc.，Duncan，Oklahoma，商品名为“SILICALITE”。在某些实施方案中，无定形二氧化硅可以很细的颗粒材料存在。在其他的实施方案中，无定形二氧化硅可以细颗粒材料存在。在其他的实施方案中，无定形二氧化硅可以小颗粒材料存在。在其他的实施方案中，无定形二氧化硅可以中等颗粒材料存在。在某些实施方案中，无定形二氧化硅在本发明的粘结组合物中的含量可以在bwoc为约5%到约40%的范围内。
在本发明的粘结组合物中使用的水可包括淡水、盐水(例如，含有一种或多种盐溶解于其中的水)、浓盐溶液(brine)(例如，由地下构造产生的饱和的盐水)、海水、或它们的组合。一般地，所述水可来自任何水源，只要它不含有过量的可能不利地影响粘结组合物中的其他组分的化合物。在一些实施方案中，可包括足以形成可泵浆料的量的水。在一些实施方案中，本发明的粘结组合物中的水的量可以在约40重量%到约200重量%的范围内。此处使用的术语“重量%”指粘结组合物中的组分的百分比，表示相对于粘结组合物中的干燥组分的重量，本发明的粘结组合物中包括的重量。在一些实施方案中，水的含量可以在约40重量%到约150重量%的范围内。
本发明的粘结组合物可任选地包含水硬性水泥。根据本发明，可利用多种水硬性水泥，包括但不限于那些包含钙、铝、硅、氧、铁、和/或硫的水硬性水泥，其通过与水的反应固化并硬化。合适的水硬性水泥包括但不限于波特兰水泥、火山灰水泥、石膏水泥、高铝水泥、矿渣水泥、硅石水泥及它们的组合。在某些实施方案中，水硬性水泥可包含波特兰水泥。在一些实施方案中，适合用于本发明的波特兰水泥根据AmericanPetroleumInstitute，APISpecificationforMaterialsandTestingforWellCements，APISpecification10，FifthEd.,July1，1990，分为A、C、H和G类水泥。在某些实施方案中，水泥在本发明的粘结组合物中的含量可以在bwoc为约20%到约50%的范围内。
在某些实施方案中，本发明的粘结组合物还可包含缓凝剂。此处使用的术语“缓凝剂”指的是延迟本发明的粘结组合物的固化的添加剂。合适的缓凝剂的实例包括但不限于磺基烷基化木质素、羟基羧酸、包含丙烯酸或马来酸的共聚物的铵盐、碱金属盐、碱土金属盐、金属盐，及它们的组合。合适的磺烷基化木质素的一个实例包含磺基甲基化木质素。合适的缓凝剂在美国专利No.Re.31,190中有更详细的披露，在此以引用的方式将其全部公开内容并入。合适的缓凝剂可购自Duncan，Oklahoma的HalliburtonEnergyServices，Inc.，商品名为“”、“”、”、“”、“”、”、“SCRTM100”和“SCRTM500”。一般地，在使用时，本发明的粘结组合物可包括足以提供所需的固化延迟的量的缓凝剂。在一些实施方案中，缓凝剂的含量可以在约0.1重量%到约5重量%的范围内。
任选地，本发明的粘结组合物中可加入其他另外的添加剂，只要本领域技术人员根据本发明的公开认为合适。这样的添加剂的实例包括但不限于加速剂、减重剂(weightreducingadditive)、高比重添加剂(heavyweightadditives)、堵漏材料(lostcirculationmaterial)、过滤控制剂、分散剂及它们的组合。这些添加剂的合适的实例包括结晶二氧化硅化合物、无定形二氧化硅、盐、纤维、水合性粘土、微球体、火山灰、胶乳水泥、触变添加剂、它们的组合等。
本发明的粘结组合物的实例可包含水、水泥、CKD、无定形二氧化硅、和玻璃化页岩。本发明的粘结组合物的另一个实例可包含水、水泥、CKD、无定形二氧化硅、沸石和玻璃化页岩。如本领域普通技术人员所需，受益于本发明公开，本发明的这种粘结组合物还可包含任何上述添加剂，以及任何多种适合地下应用的其他添加剂。
本发明的粘结组合物可用于多种地下应用，包括但不限于初次注水泥、补注水泥和钻井操作。本发明的粘结组合物还可用于表面应用，例如，建筑粘结。
本发明方法的实例包括提供本发明的粘结组合物，该粘结组合物包含水和处于受阻沉降状态的颗粒材料；将粘结组合物置于待粘结处；并使所述粘结组合物在其中固化。在一些实施方案中，待粘结处可在地上，例如，在建筑粘结中。在一些实施方案中，待粘结处可在地下构造(subterraneanformation)中，例如，在地下应用中。如本领域普通技术人员所需，受益于本发明公开，可用于该方法的本发明的粘结组合物还可包含任何上述添加剂，以及任何多种适合地下应用的其他添加剂。
因此，本发明非常适合达到所述的以及固有的目的和优势。尽管本领域技术人员可作诸多改变，这些改变都包含在由所附权利要求限定的本发明的精神范围内。权利要求中的术语为它们简单的、普通的含义，除非专利权人另有明确和清楚的定义。

Claims (34)

1.一种粘结方法，其包括：
使用至少一种颗粒材料，将粘结组合物中的堆积体积分数最大化，所述至少一种颗粒材料选自水泥窑粉尘、玻璃化页岩、沸石及它们的组合；
将所述粘结组合物引入地下构造中；并
使所述粘结组合物在所述地下构造中固化，
其中所述至少一种颗粒材料包含至少三种不同的粒径，所述粒径选自：在7纳米到50纳米的范围内的粒径；在0.05微米到0.5微米的范围内的粒径；在0.5微米到10微米的范围内的粒径；在10微米到20微米的范围内的粒径；在20微米到200微米的范围内的粒径；在200微米到800微米的范围内的粒径；和大于1毫米的粒径。
2.权利要求1的方法，其中所述粘结组合物包含水硬性水泥。
3.权利要求1的方法，其中所述粘结组合物包含波特兰水泥。
4.权利要求1的方法，其中所述至少一种颗粒材料是水泥窑粉尘。
5.权利要求1的方法，其中所述至少一种颗粒材料是玻璃化页岩。
6.权利要求1的方法，其中所述至少一种颗粒材料是沸石。
7.一种粘结方法，其包括：
将粘结组合物引入地下构造中，其中所述粘结组合物包含水、水硬性水泥和至少一种颗粒材料，所述至少一种颗粒材料选自水泥窑粉尘、玻璃化页岩、沸石及它们的组合；
其中所述粘结组合物中的固体体积总量具有最大堆积体积分数；并
使所述粘结组合物在所述地下构造中固化，
其中所述至少一种颗粒材料包含至少三种不同的粒径，所述粒径选自：在7纳米到50纳米的范围内的粒径；在0.05微米到0.5微米的范围内的粒径；在0.5微米到10微米的范围内的粒径；在10微米到20微米的范围内的粒径；在20微米到200微米的范围内的粒径；在200微米到800微米的范围内的粒径；和大于1毫米的粒径。
8.权利要求7的方法，其中所述水硬性水泥包含波特兰水泥。
9.权利要求7的方法，其中所述至少一种颗粒材料是水泥窑粉尘。
10.权利要求7的方法，其中所述至少一种颗粒材料是玻璃化页岩。
11.权利要求7的方法，其中所述至少一种颗粒材料是沸石。
12.一种粘结方法，其包括：
提供选自下列组中的至少三种颗粒材料的未水合的混合物：
(a)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在7纳米到50纳米的范围内；
(b)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在0.05微米到0.5微米的范围内；
(c)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在0.5微米到10微米的范围内；
(d)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在10微米到20微米的范围内；
(e)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在20微米到200微米的范围内；
(f)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在200微米到800微米的范围内；和
(g)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径大于1毫米，
其中所述至少三种颗粒材料的固体体积总量具有最大堆积体积分数；
向所述未水合的混合物中加入水以形成可固化组合物；并
将所述可固化组合物置于地下构造中。
13.权利要求12的方法，其中所述可固化组合物包含水硬性水泥。
14.权利要求12的方法，其中所述未水合的混合物包含至少一种选自二氧化硅、铁氧化物、氢氧化钡、碳酸盐、氧化铝、有机产品及它们的组合的材料。
15.权利要求14的方法，其中所述铁氧化物是赤铁矿。
16.权利要求12的方法，其中所述可固化组合物中水泥窑粉尘的含量在所述可固化组合物的重量的25％到75％的范围内。
17.权利要求12的方法，其中所述可固化组合物中玻璃化页岩的含量在所述可固化组合物的重量的10％到30％的范围内。
18.权利要求12的方法，其中所述可固化组合物中沸石的含量在所述可固化组合物的重量的10％到25％的范围内。
19.权利要求12的方法，其中所述可固化组合物中无定形二氧化硅的含量在所述可固化组合物的重量的5％到40％的范围内。
20.一种方法，其包括：
提供粘结组合物，其中该粘结组合物包含水；和选自下列组中的至少三种颗粒材料：
(a)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在7纳米到50纳米的范围内；
(b)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在0.05微米到0.5微米的范围内；
(c)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在0.5微米到10微米的范围内；
(d)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在10微米到20微米的范围内；
(e)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在20微米到200微米的范围内；
(f)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在200微米到800微米的范围内；和
(g)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径大于1毫米，
其中所述至少三种颗粒材料的固体体积总量具有最大堆积体积分数；并，
将所述粘结组合物置于地下构造中。
21.权利要求20的方法，其还包括使所述粘结组合物在其中固化的步骤。
22.权利要求20的方法，其中所述水选自淡水、盐水、海水以及它们的组合。
23.权利要求22的方法，其中所述水是由地下构造产生的饱和的盐水。
24.权利要求20的方法，其中所述粘结组合物包含水硬性水泥。
25.权利要求20的方法，其中所述粘结组合物包含至少一种选自二氧化硅、铁氧化物、氢氧化钡、碳酸盐、氧化铝、有机产品以及它们的组合的材料。
26.权利要求25的方法，其中所述铁氧化物是赤铁矿。
27.权利要求20的方法，其中所述粘结组合物包含至少一种选自缓凝剂；加速剂；堵漏材料；过滤控制剂；分散剂；及它们的组合的添加剂。
28.权利要求20的方法，其中所述粘结组合物中水泥窑粉尘的含量在所述粘结组合物的重量的25％到75％的范围内。
29.权利要求20的方法，其中所述粘结组合物中玻璃化页岩的含量在所述粘结组合物的重量的10％至30％的范围内。
30.权利要求20的方法，其中所述粘结组合物中沸石的含量在所述粘结组合物的重量的10％至25％的范围内。
31.根据权利要求20的方法，其中所述粘结组合物中无定形二氧化硅的含量在所述粘结组合物的重量的5％至40％的范围内。
32.一种粘结方法，其包括：
将粘结组合物引入地下构造和置于地下构造中的管线之间的环形空间中，其中所述粘结组合物包含水、和选自下列组中的至少三种颗粒材料：
(a)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在7纳米到50纳米的范围内；
(b)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在0.05微米到0.5微米的范围内；
(c)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在0.5微米到10微米的范围内；
(d)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在10微米到20微米的范围内；
(e)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在20微米到200微米的范围内；
(f)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径在200微米到800微米的范围内；和
(g)水泥窑粉尘、玻璃化页岩、沸石、或无定形二氧化硅，其粒径大于1毫米，
其中所述至少三种颗粒材料的固体体积总量具有最大堆积体积分数；并
使所述粘结组合物在所述环形空间中固化。
33.权利要求32的方法，其中所述粘结组合物中水泥窑粉尘的含量在所述粘结组合物的重量的25％到75％的范围内。
34.权利要求32的方法，其中所述粘结组合物中玻璃化页岩的含量在所述粘结组合物的重量的10％至30％的范围内。
CN201310478308.2A 2006-07-12 2006-10-04 包含水泥窑粉尘、玻璃化页岩、沸石和/或无定形二氧化硅的粘结组合物，及相关方法 Expired - Fee Related CN103708751B (zh)

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CA2658155A1 (en) 2008-01-17
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US7213646B2 (en) 2007-05-08
EP2038234A1 (en) 2009-03-25
WO2008007040A1 (en) 2008-01-17
IN2015DN00177A (zh) 2015-07-10
RU2433970C2 (ru) 2011-11-20
CN101484400B (zh) 2013-11-06
NO20085316L (no) 2009-02-11
US20070056732A1 (en) 2007-03-15
RU2009104692A (ru) 2010-08-20
CN101484400A (zh) 2009-07-15
CA2658155C (en) 2013-04-30

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