CN103437191B - Nano cannabis sativa oil microcapsule, nano cannabis sativa oil microcapsule fabric, preparation method of nano cannabis sativa oil microcapsule fabric and prepared product - Google Patents
Nano cannabis sativa oil microcapsule, nano cannabis sativa oil microcapsule fabric, preparation method of nano cannabis sativa oil microcapsule fabric and prepared product Download PDFInfo
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- CN103437191B CN103437191B CN201310331825.7A CN201310331825A CN103437191B CN 103437191 B CN103437191 B CN 103437191B CN 201310331825 A CN201310331825 A CN 201310331825A CN 103437191 B CN103437191 B CN 103437191B
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Abstract
The invention relates to a nano cannabis sativa oil microcapsule, nano cannabis sativa oil microcapsule fabric, a preparation method of the nano cannabis sativa oil microcapsule fabric, and a prepared product. A nano cannabis sativa oil microcapsule finishing agent comprises a cannabis sativa oil inner core and a microcapsule outer membrane at a weight ratio of (0.1-10):1, wherein the cannabis sativa oil inner core adopts pure cannabis sativa oil, or a mixture of the cannabis sativa oil and an organic matter; and the microcapsule outer membrane comprises polylactic acid, a cosolvent, an emolsifier and a crosslinking agent at a weight ratio of 100:(20-1000):(20:500):(10-500). The nano cannabis sativa oil microcapsule fabric has excellent health care performances and stable and durable functions, is washable and environment-friendly, meets requirements of human on health care textile, can effectively maintain human health and is a new hot spot in a textile market. The product can be widely applied to clothing, undergarments, gloves, sheets, quilt covers, summer sleeping mats, towels, shirts, socks, medical auxiliary materials, health care products and the like, and has a good effect and a wide prospect.
Description
Technical field
The present invention relates to a kind of technical scheme of Textile Manufacturing Industry, especially relate to a kind of nanometer fire sesame oil microcapsule dressing agent; Through the nanometer fire sesame oil microcapsule textile of this nanometer fire sesame oil microcapsule dressing agent Multifunctional finishing; And the preparation method of this nanometer fire sesame oil microcapsule textile and prepared product.
Background technology
Along with modern society's industry and civilized fast development, the earth environment that the mankind depend on for existence worsens increasingly, and atmosphere pollution causes great destruction to environment.In densely populated inhabitation, workplace, the use of a large amount of air-conditioning and various electric equipment, IAQ is worsened, in addition, the various coal smokes of automobile exhaust gas, plant emissions, pollution when burning away the refuse, the factors such as the pollution of agricultural chemicals and organic compound are used to make air quality be subject to pollution in various degree and run down, environmental pollution is day by day serious, and the health of the mankind is on the hazard.Therefore, increasing people starts to advocate health, naturally life style, and nowadays, back to nature, pursuing health quietly becomes the new fashion in city.
For textiles closely-related with human lives, be proposed higher requirement, just be not satisfied with original basic functions such as warming, comfortable, more focus on the intension pursuing textiles, wish that it has the specific functions such as health care, comfortable, safety, environmental protection, can health be of value to, even can also diseases prevention, cure the disease, alleviate the injury that causes to the mankind of environmental pollution.Therefore, the heath-function of textiles arranges and is more and more valued by the people.The mankind are entering the New Times of giving fabric and having real health care.
Modern pharmacology result of study is verified, and in fiery sesame oil, unsaturated fatty acid content is up to more than 70%, is the soprano of unsaturated fatty acid content in all Vegetable Oils.It has skin makeup key body, increase the elasticity of skin and gloss, relax bowel, the effect of reducing blood lipid, and has and delay artery sclerosis, prevention cardiovascular and cerebrovascular disease, cancer-resisting, long-lived effect.
But, in prior art, not yet occur that being convenient to people utilizes fiery sesame oil to carry out the technical scheme of product or the method kept healthy chronically, easily.
Summary of the invention
The object of the invention is the shortcomings and deficiencies existed for existing health care textiles, develops a kind of nanometer fire sesame oil microcapsule dressing agent; Through the nanometer fire sesame oil microcapsule textile of this nanometer fire sesame oil microcapsule dressing agent Multifunctional finishing; And the preparation method of this nanometer fire sesame oil microcapsule textile
with prepared product.So that people utilize fiery sesame oil to keep healthy chronically, easily.Nanometer fire sesame oil microcapsules Multifunctional finishing fabric after the present invention arranges, health properties is excellent, and washable, environmental protection, function-stable are lasting, meet the demand of the mankind to health care textiles, effectively can safeguard health, become the new focus of piece market.Product can be widely used in clothes, underwear, gloves, sheet, quilt cover, summer sleeping mat, towel, underwear, shirt, socks, clothes, medical accessory, health product etc., has good effect and wide prospect.
To achieve these goals, technical scheme of the present invention is as follows: a kind of nanometer fire sesame oil microcapsule dressing agent, comprise fiery sesame oil inner core and microcapsules adventitia, it is characterized in that, described fiery sesame oil inner core and the weight ratio of microcapsules adventitia are: 0.1-10:1.
Further optimization, the weight ratio of fiery sesame oil inner core of the present invention and microcapsules adventitia is: 1-2:1.
Described fiery sesame oil inner core adopts pure fiery sesame oil; Also fiery sesame oil and one or more organic mixtures can be adopted; Such as: the mixture of fiery sesame oil and linseed oil, fiery sesame oil and essence or/and the mixture of natural fragrant essence, the mixture etc. of fiery sesame oil and vitamin;
Described microcapsules adventitia is made up of PLA, cosolvent, emulsifying agent and crosslinking agent; The weight ratio of described PLA, cosolvent, emulsifying agent and crosslinking agent is: 100:20-1000:20-500:10-500.
Further optimization, the weight ratio of PLA of the present invention, cosolvent, emulsifying agent and crosslinking agent is: 100:200-500:50-200:50-200.
Described PLA can adopt molecular weight to be one or more in 0.5 ten thousand ~ 600,000; Described cosolvent can adopt in acetone, chloroform, toluene or other organic solvents one or more; Described emulsifying agent can adopt in alkylphenol polyoxyethylene, fatty alcohol-polyoxyethylene ether or fatty alcohol sulfate salt one or more; Described crosslinking agent can adopt aziridine or aziridine or/and end group aziridine blocked isocyanate compounds.
Described nanometer fire sesame oil microcapsule dressing agent also can regard a kind of composition that have capsule of nano form, that can use as fabric finishing agent as.
Described nanometer fire sesame oil microcapsule dressing agent, its particle diameter is 20-900nm, and average grain diameter is 50-300nm.
The preparation method of this nanometer fire sesame oil microcapsules, step is as follows:
(1). fiery sesame oil, PLA, cosolvent, emulsifying agent and crosslinking agent are mixed in proportion, and is heated to 50-90 degree;
(2). add the pure water of 60-90% at reactor, reactor is heated to 90-95 degree;
(3). under high-speed stirred condition, be slowly added dropwise to the above-mentioned mixed liquor of 10-30%, instillation time 5-500 minute, that optimum is 30-120 minute;
(4). be cooled to 30-40 degree;
(5). spraying dry, namely obtains nanometer fire sesame oil microcapsules.
The technical scheme completing the application's second invention task is, a kind of nanometer fire sesame oil microcapsule textile, is characterized in that, described fabric is the fabric through above-mentioned nanometer fire sesame oil microcapsule dressing agent Multifunctional finishing; Described Multifunctional finishing can be padding method, the afterfinish method such as Decal and infusion process.
Nanometer fire sesame oil microcapsule textile and goods, its core-clad material storage life is not less than 5 years (or 50 DEG C are not less than 6 months).
By the method for testing that National Textile washing standard specifies, after 30 washings, fabric is still no less than 20% containing core-clad material.
This fiery sesame oil capsule of nano fabric and goods have good whiteness, coloured light, gas permeability, hygroscopicity, brute force and elasticity.
Nanometer fire sesame oil microcapsule textile and goods, not containing the not environmentally composition such as formaldehyde, heavy metal and azo-compound, meet " the basic security technical requirement of GB 18401-2003 textile product ".
The technical scheme completing the application's the 3rd invention task is, the preparation method of above-mentioned nanometer fire sesame oil microcapsule textile, and it is characterized in that, step is as follows:
Step (1)-be (5) first prepare nanometer fire sesame oil microcapsules:
(1). fiery sesame oil, PLA, cosolvent, emulsifying agent and crosslinking agent are mixed in proportion, and is heated to 50-90 degree;
(2). add the pure water of 60-90% at reactor, reactor is heated to 90-95 degree;
(3). under high-speed stirred condition, be slowly added dropwise to the above-mentioned mixed liquor of 10-30%, instillation time 5-500 minute, that optimum is 30-120 minute;
(4). be cooled to 30-40 degree;
(5). spraying dry, grain size grading, namely obtains nanometer fire sesame oil microcapsules.
(6). in fabric to be arranged, add the nanometer fire sesame oil microcapsule dressing agent that (5) step obtains, the method added can adopt padding method, the afterfinish method such as Decal and infusion process;
(7). through the fabric drying technique that nanometer fire sesame oil microcapsule dressing agent arranged.
Nanometer fire sesame oil microcapsules of the present invention have reactable, are directly bonded on textiles with the form of chemical bond by crosslinking agent.The capsule of nano that nanometer fire sesame oil microcapsules are prepared as wall material raw material by PLA, maximum particle diameter is less than 300nm, average grain diameter 50nm, and its physical property meets fabric finishing requirement completely, comfortable and easy to wear.
The present invention develops three kinds of afterfinish methods, is applied to different fabrics.
1.padding method: be applied to woven fabric
Technical recipe: nanometer fire sesame oil microcapsules 40-60g/L
Crosslinking agent 40-60g/L
Material operation (to prepare 100Kg solution): the hot water (85-90 DEG C) first adding 80Kg in material bucket, then add nanometer fire sesame oil microcapsules, stirring stirs evenly, and then adds crosslinking agent, finally adds remaining water, stirs, is incubated 80 DEG C.
Technological process: fabric → pad (pick-up rate 70-80%) → oven dry (80-100 DEG C) → finished product
2.decal: the fabric being applied to stamp requirement
Technical recipe: nanometer fire sesame oil microcapsules 4-8%
Pigment printing paste 1-10%
Adhesive 15-20%
Thickener 1-2%
Material operates: in material bucket, first prepare print slurry, then stirring adds SCM, stirs.
Technological process: stamp → oven dry (50-100 DEG C) → tentering (100-120 DEG C) → finished product.
3.infusion process: be applied to towel, knit goods
Technical recipe: nanometer fire sesame oil microcapsules 5-10%
Crosslinking agent 5-8%.
Material operates: first add the hot water (more than 80 DEG C) of 80%, then adds nanometer fire sesame oil microcapsules, is stirred to and dissolves completely, then add crosslinking agent, stir, finally add remaining water, stir evenly.
Technological process: bleaching and dyeing the fabric → dipping solution after oven dry (bath raio 1:10,85 DEG C of x30-40 min) → dehydration → oven dry (80-110 DEG C) → finished product.
The technical scheme completing the application's the 4th invention task is, above-mentioned nanometer fire sesame oil microcapsule textile, application in preparation textile product (namely, textile product prepared by nanometer fire sesame oil microcapsule textile), it is characterized in that, described textile product comprises: coat, shirt, underwear, gloves, sheet, quilt cover, summer sleeping mat, towel, socks, medical accessory, and health treatment.
Nanometer fire sesame oil microcapsules Multifunctional finishing fabric after the present invention arranges, health properties is excellent, and washable, environmental protection, function-stable are lasting, meet the demand of the mankind to health care textiles, effectively can safeguard health, become the new focus of piece market.Product can be widely used in clothes, underwear, gloves, sheet, quilt cover, summer sleeping mat, towel, underwear, shirt, socks, medical accessory, health product etc., has good effect and wide prospect.If the textile fabric of being together morning and night with human body is endowed the health care of fiery sesame oil, then health care makes textiles will enter a frontier.
Detailed description of the invention
Below the present invention is further detailed.
Embodiment 1, nanometer fire sesame oil microcapsules multifunction finishing agent, consists of by mass percentage:
By mass percentage, its component comprises: nanometer fire sesame oil microcapsules 4% ~ 8%
Crosslinking agent 4% ~ 8% water surplus.
Described crosslinking agent is low temperature sticking agent SLT or SCJ939, purchased from Beijing Jie Ershuan High Seience Technology Co., Ltd..
Embodiment 2
A kind of nanometer fire sesame oil microcapsules multifunction finishing agent, consists of by mass percentage:
By mass percentage, its component comprises: nanometer fire sesame oil microcapsules 6%
Low temperature sticking agent SLT 6% water surplus.
Adopt gained finishing agent to arrange fabric, fabric is first through dipping, and then padding machine pads, and adjustment platen pressure, the liquid carrying rate making fabric is 70%, finally dries.
Embodiment 2
A kind of nanometer fire sesame oil microcapsules multifunction finishing agent, consists of by mass percentage:
By mass percentage, its component comprises: nanometer fire sesame oil microcapsules 6%
Low temperature sticking agent SLT 6%
NON IONIC SOFTNER 3% water surplus.
Adopt gained finishing agent to arrange fabric, fabric is first through dipping, and then padding machine pads, and adjustment platen pressure, the liquid carrying rate making fabric is 70%, finally dries.
Testing result and application
Adopt above-described embodiment scheme, the nanometer fire sesame oil microcapsules Multifunctional finishing fabric after the present invention arranges, after testing, in fabric, linoleic acid content: 40mg/100g, oleic acid content: 60mg/100g, palmitic acid content: 70mg/100g, stearic acid content: 30mg/100g.Microcapsules maximum particle diameter is less than 300nm, average grain diameter 50nm, and its physical property meets fabric finishing requirement completely, comfortable and easy to wear.Its core-clad material storage life is not less than 5 years (or 50 DEG C are not less than 6 months).By the method for testing that National Textile washing standard specifies, after 30 washings, fabric is still no less than 20% containing core-clad material.This fiery sesame oil capsule of nano finish fabric and goods have good whiteness, coloured light, gas permeability, hygroscopicity, brute force and elasticity.Not containing the not environmentally composition such as formaldehyde, heavy metal and azo-compound, meet " the basic security technical requirement of GB 18401-2003 textile product ".
Scape aspect before application, the domestic and international demand to nanometer fire sesame oil microcapsules Multifunctional finishing fabric and goods has certain market at present, and the healthcare industry potential market especially for the elderly is very large.Nanometer fire sesame oil microcapsules Multifunctional finishing fabric after the present invention arranges, health properties is excellent, and washable, environmental protection, function-stable are lasting, meet the demand of the mankind to health care textiles, effectively can safeguard health, become the new focus of piece market.Product can be widely used in clothes, underwear, gloves, sheet, quilt cover, summer sleeping mat, towel, underwear, shirt, socks, clothes, medical accessory, health product etc., has good effect and wide prospect.
Claims (5)
1. a nanometer fire sesame oil microcapsule dressing agent, comprise fiery sesame oil inner core and the microcapsules adventitia of microcapsules, it is characterized in that, the fiery sesame oil inner core of described microcapsules and the weight ratio of microcapsules adventitia are: 0.1-10:1;
Described fiery sesame oil inner core adopts pure fiery sesame oil; Or adopt fiery sesame oil and one or more organic mixtures;
Adopt fiery sesame oil and one or more organic mixtures, refer to: the mixture of fiery sesame oil and linseed oil, fiery sesame oil and essence or/and the mixture of natural fragrant essence, or, the mixture of fiery sesame oil and vitamin;
Described microcapsules adventitia is made up of PLA, cosolvent, emulsifying agent and crosslinking agent; The weight ratio of described PLA, cosolvent, emulsifying agent and crosslinking agent is: 100:20-1000:20-500:10-500;
Described PLA adopts molecular weight to be one or more in 0.5 ten thousand ~ 600,000; Described cosolvent adopt in acetone, chloroform, toluene or other organic solvents one or more; Described emulsifying agent adopt in alkylphenol polyoxyethylene, fatty alcohol-polyoxyethylene ether or fatty alcohol sulfate salt one or more; Described crosslinking agent adopts aziridine or/and end group aziridine blocked isocyanate compounds.
2. nanometer fire sesame oil microcapsule dressing agent according to claim 1, is characterized in that,
Described fiery sesame oil inner core and the weight ratio of microcapsules adventitia are: 1-2:1;
The weight ratio of described PLA, cosolvent, emulsifying agent and crosslinking agent is: 100:200-500:50-200:50-200.
3. nanometer fire sesame oil microcapsule dressing agent according to claim 1 and 2, is characterized in that, described nanometer fire sesame oil microcapsule dressing agent, its maximum particle diameter is less than 900nm, average grain diameter 50-300nm.
4. through the nanometer fire sesame oil microcapsule textile that nanometer fire sesame oil microcapsule dressing agent according to claim 1 arranges, it is characterized in that, described fabric is the fabric through above-mentioned nanometer fire sesame oil microcapsule dressing agent Multifunctional finishing; Described Multifunctional finishing technique refers to padding method, Decal or infusion process.
5. the application of nanometer fire sesame oil microcapsule textile according to claim 4 in preparation textile product, it is characterized in that, described textile product comprises: coat, shirt, underwear, gloves, sheet, quilt cover, summer sleeping mat, towel, socks, medical accessory, and health treatment.
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| CN201310331825.7A CN103437191B (en) | 2013-08-02 | 2013-08-02 | Nano cannabis sativa oil microcapsule, nano cannabis sativa oil microcapsule fabric, preparation method of nano cannabis sativa oil microcapsule fabric and prepared product |
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| CN201310331825.7A CN103437191B (en) | 2013-08-02 | 2013-08-02 | Nano cannabis sativa oil microcapsule, nano cannabis sativa oil microcapsule fabric, preparation method of nano cannabis sativa oil microcapsule fabric and prepared product |
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| CN105054695A (en) * | 2015-08-05 | 2015-11-18 | 汪建 | Summer sleeping mat or pillowcase with fragrance |
| CN111893772B (en) * | 2020-08-06 | 2022-11-08 | 河南优思特医疗科技有限公司 | Manufacturing method of fragrant fabric and fragrant fabric |
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Effective date of registration: 20170907 Address after: 211100, No. five, Hopewell Road, five mile Industrial Zone, Pukou District, Jiangsu, Nanjing, 6 Patentee after: Nanjing Tianmai Health Technology Development Co. Ltd. Address before: Pukou Economic Development Zone, Nanjing City, Jiangsu province 211800 Pu Chu Road No. 8 Patentee before: Nanjing Tianmai Health Management Co., Ltd. |
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