CN102871853A - Composition for enhancing and prolonging cooling feeling and application thereof - Google Patents
Composition for enhancing and prolonging cooling feeling and application thereof Download PDFInfo
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- CN102871853A CN102871853A CN2012103628719A CN201210362871A CN102871853A CN 102871853 A CN102871853 A CN 102871853A CN 2012103628719 A CN2012103628719 A CN 2012103628719A CN 201210362871 A CN201210362871 A CN 201210362871A CN 102871853 A CN102871853 A CN 102871853A
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Abstract
The invention aims to disclose a composition for enhancing and prolonging a cooling feeling and application thereof. The composition comprises the following components in percentage by mass: 40 to 80 percent of borneol, 10 to 50 percent of mint amide and 5 to 30 percent of butyl vanillin. Compared with the prior art, the composition has the advantages that the borneol, the butyl vanillin and the mint amide are combined, so the cooling degree is effectively enhanced, and the cooling duration is prolonged; and a skin-care product manufactured by using the composition for enhancing and prolonging the cooling feeling has a cool sense, brings continual cooling and refreshing feeling besides moisturizing and nourishing and is mild, safe and stimulation-free in the absence of any artificial essence, and the aims of the composition are fulfilled.
Description
Technical field
The present invention relates to a kind of compositions and application thereof, particularly a kind of compositions and application thereof that is applicable to the enhancing of skin care item and prolongs refrigerant sense.
Background technology
In summer, freshener is a lot of in the application of skin care item, such as the energy adjustment health breast of nursing gel, Lancome behind the lucky palpus and mousse Cleansing Foam of Dior etc., is subject to liking of some consumers of liking refrigerant impression.
The freshener that present these products on the market use mainly is menthyl lactate, and its persistence has certain effect, but burst and refrigerant degree are inadequate.
People have to add Mentholum in order to obtain the explosive high product of strong and refrigerant degree, but because the refrigerant persistent period of Mentholum is shorter, in order to continue the refrigerant necessary addition that improves it, but its characteristic odor will be denseer like this, so that fragrance has sizable difficulty to its covering, thereby diminish the image of high-grade skin care item.
Therefore, need especially a kind of compositions and application thereof that strengthens and prolong refrigerant sense, solved the problem of above-mentioned existing existence.
Summary of the invention
The object of the present invention is to provide a kind of compositions and application thereof that strengthens and prolong refrigerant sense, for the deficiencies in the prior art, effectively strengthen refrigerant degree, prolong refrigerant persistence, satisfied the refrigerant skin care item development requirement of each class.
Technical problem solved by the invention can realize by the following technical solutions:
On the one hand, the invention provides a kind of compositions that strengthens and prolong refrigerant sense, it is characterized in that, it comprises the component of following mass percent: Borneolum Syntheticum 40-80%, amide of mint 10-50% and butyl Rhizoma et radix valerianae ester 5-30%.
In one embodiment of the invention, preferably, Borneolum Syntheticum is 50-70%, and amide of mint is 25-40%, and butyl Rhizoma et radix valerianae ester is 10-20%.
On the other hand, the invention provides a kind of application that strengthens and prolong the compositions of refrigerant sense, it is characterized in that, described enhancing also prolongs the application of compositions in the skin care item such as Cool cream of refrigerant sense.
Enhancing of the present invention also prolongs compositions and the application thereof of refrigerant sense, compared with prior art, combination by Borneolum Syntheticum, butyl Rhizoma et radix valerianae ester and amide of mint, effectively strengthen refrigerant degree, prolong refrigerant persistence, the skin care item that use enhancing of the present invention and prolong the compositions manufacturing of refrigerant sense have the refreshing texture of ice, in moisturizing, bring the endlessly refrigerant impression of soothing the spirit, do not add any artificial essence, gentle safe and non-stimulating, realize purpose of the present invention.
Characteristics of the present invention can be consulted the detailed description of the graphic and following better embodiment of this case and be obtained to be well understood to.
Description of drawings
Fig. 1 is the schematic diagram of refrigerant intensity in the embodiments of the invention;
Fig. 2 is the schematic diagram of calorific intensity in the embodiments of the invention;
Fig. 3 is the schematic diagram of refrigerant persistent period in the embodiments of the invention.
The specific embodiment
For technological means, creation characteristic that the present invention is realized, reach purpose and effect is easy to understand, below in conjunction with concrete diagram, further set forth the present invention.
On the one hand, enhancing of the present invention also prolongs the compositions of refrigerant sense, and it comprises the component of following mass percent: Borneolum Syntheticum 40-80%, amide of mint 10-50% and butyl Rhizoma et radix valerianae ester 5-30%.
Preferably, Borneolum Syntheticum is 50-70%, and amide of mint is 25-40%, and butyl Rhizoma et radix valerianae ester is 10-20%.
Borneolum Syntheticum, its characteristic: clearing heat for detumescence; Penetration enhancing effect; Cooperate Mentholum, can suitably increase refrigerant sense.
Amide of mint, its characteristic: cooling sensation is stable and enhancing at leisure; Without mint flavored; Prolong refrigerant.
Butyl Rhizoma et radix valerianae ester, its characteristic: strong hotness; Than other exothermic mixture safety; Low irritant; Long-acting hotness; Blood circulation promoting; Menthol and butyl Rhizoma et radix valerianae ester are used in conjunction with, and can strengthen its creeping chill intensity, prolong simultaneously the creeping chill time.
Enhancing of the present invention and the compositions that prolongs refrigerant sense can play the effect of further enhancing and prolongation according to the principle of refrigerant illusion.
Amide of mint is a kind of exothermic mixture, research conclusion: 0.5% amide of mint can promote the local blood circulation amount to increase by 66.4%, and is effectively instant, and obviously onset reached peak value after 30 minutes after 10 minutes.
Conclusion is hemoperfusion amount rising effective time length more than 30 minutes.Say from angles of product, refrigerant sense stiffening effect continues more than 30 minutes.The actual test of sample according to 1%, effective time reaches 120 minutes.But owing to being exothermic mixture, if dosage is excessive, can manifest heating effect the latter stage that disappears in refrigerant sense, and this need to be avoided.
On the other hand, enhancing of the present invention also prolongs the application of the compositions of refrigerant sense, and described enhancing also prolongs the application of compositions in the skin care item such as Cool cream of refrigerant sense.
Enhancing of the present invention and to prolong the compositions of refrigerant sense as follows for the preparation of the step of skin care item:
1, the preparation in early stage:
Oil phase: take by weighing respectively octadecanol, Emulium Delta, glyceryl monostearate, Mentholum, isononyl isononanoate, the IPM of formula ratio in beaker, ℃ heating also is stirred to fully fusing a little in temperature 70 C ~ 80, and is for subsequent use.
Water: take by weighing in proportion deionized water and Acritamer 940 in beaker, rapid stirring disperses and is heated to 70 ℃～80 ℃, and is for subsequent use.
Take by weighing Borneolum Syntheticum, amide of mint, butyl Rhizoma et radix valerianae ester, D5, sodium hydroxide solution, antiseptic GPL by formula ratio, for subsequent use.
2, preparation skin care articles:
Borneolum Syntheticum, amide of mint are added above-mentioned high temperature oil phase, be stirred to dissolving, oil phase is slowly poured into water and stirring again, stirred first 5 minutes, homogenizing is 2 minutes again.
About 75 ℃, stir insulation 15 minutes.
Begin to cool down, temperature of charge in the emulsifying pot is down to 60 ℃, add D5.
Be cooled to 50 ℃, add sodium hydroxide solution.
Be cooled to 40 ℃, add butyl Rhizoma et radix valerianae ester and GPL and stirred 15 minutes, close stirring, complete.
Test recipe design: add Borneolum Syntheticum, butyl Rhizoma et radix valerianae ester, the amide of mint of different proportion on the basic components basis, the gained sample arises from inboard arm with standard substance one and smears and compare test.
Verification method:
Clinical trial
Scheme-IN VIVO test:
20 experimenters through training
Specimen:
Standard substance (the o/w cream frost that does not contain refrigerant combination) VS. contains the o/w cream frost of refrigerant combination
Experimental condition: 12 independently room (temperature and humidity are constant)
Use 2 specimen (standard substance and the cream frost that contains refrigerant combination) at the both sides forearm simultaneously
Behind the application testing sample, begin timing, in the time of first 10 minutes, the refrigerant sense intensity of assess sample.Continue test subsequently until refrigerant sense disappears, timing if there is this moment the heating sense to produce, is recorded its calorific intensity in the lump.
Cool cream orthogonal test such as following table:
Cool feeling standards of grading: (referring to Fig. 1)
0=does not have refrigerant sense
The refrigerant sense that 10=is strong
Hotness standards of grading (referring to Fig. 2)
The 0=sense of not generating heat
The heating sense that 10=is strong
The refrigerant persistent period (referring to Fig. 3)
The checking conclusion:
Obtain a kind of not only acomia hotness but also can strengthen and prolong the portfolio ratio of refrigerant sense by the orthonormal design of experiments to Cool cream, accounting is respectively: Borneolum Syntheticum 40-80%, amide of mint 10-50%, butyl Rhizoma et radix valerianae ester 5-30%
Best proportion is: Borneolum Syntheticum 50-70%, amide of mint 25-40%, butyl Rhizoma et radix valerianae ester 10-20%.
The pH value of this Cool cream is 6.56, and by stability experiment, its result meets QB/T1857-2004.
Above demonstration and described ultimate principle of the present invention and principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; that describes in above-described embodiment and the description just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications; these changes and improvements all fall in the claimed scope of the invention, and the claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (3)
1. a compositions that strengthens and prolong refrigerant sense is characterized in that, it comprises the component of following mass percent: Borneolum Syntheticum 40-80%, amide of mint 10-50% and butyl Rhizoma et radix valerianae ester 5-30%.
2. enhancing as claimed in claim 1 and prolong the compositions of refrigerant sense is characterized in that preferably, Borneolum Syntheticum is 50-70%, and amide of mint is 25-40%, and butyl Rhizoma et radix valerianae ester is 10-20%.
3. an application that strengthens and prolong the compositions of refrigerant sense is characterized in that, described enhancing also prolongs the application of compositions in the skin care item such as Cool cream of refrigerant sense.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210362871.9A CN102871853B (en) | 2012-09-25 | 2012-09-25 | Composition for enhancing and prolonging cooling feeling and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210362871.9A CN102871853B (en) | 2012-09-25 | 2012-09-25 | Composition for enhancing and prolonging cooling feeling and application thereof |
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| Publication Number | Publication Date |
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| CN102871853A true CN102871853A (en) | 2013-01-16 |
| CN102871853B CN102871853B (en) | 2015-02-04 |
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| CN201210362871.9A Active CN102871853B (en) | 2012-09-25 | 2012-09-25 | Composition for enhancing and prolonging cooling feeling and application thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104027754A (en) * | 2013-03-08 | 2014-09-10 | 广东雅威生物科技有限公司 | Cervical vertebra easing composition |
| CN104491092A (en) * | 2014-12-12 | 2015-04-08 | 湖南天龙制药有限公司 | Composition for refreshing brain and regaining consciousness and preparation method thereof |
| CN109431871A (en) * | 2018-12-25 | 2019-03-08 | 安徽爱迪香料股份有限公司 | A kind of preparation method for the long-acting refrigerant preparation making an addition to the cool cream of external application |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6328982B1 (en) * | 1998-08-04 | 2001-12-11 | Takasago International Corporation | Cool feeling composition |
| CN102006786A (en) * | 2008-04-15 | 2011-04-06 | 弗门尼舍有限公司 | Warming sensate composition |
-
2012
- 2012-09-25 CN CN201210362871.9A patent/CN102871853B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6328982B1 (en) * | 1998-08-04 | 2001-12-11 | Takasago International Corporation | Cool feeling composition |
| CN102006786A (en) * | 2008-04-15 | 2011-04-06 | 弗门尼舍有限公司 | Warming sensate composition |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104027754A (en) * | 2013-03-08 | 2014-09-10 | 广东雅威生物科技有限公司 | Cervical vertebra easing composition |
| CN104491092A (en) * | 2014-12-12 | 2015-04-08 | 湖南天龙制药有限公司 | Composition for refreshing brain and regaining consciousness and preparation method thereof |
| CN104491092B (en) * | 2014-12-12 | 2017-07-04 | 湖南天龙制药有限公司 | One kind refreshes the mind composition and preparation method thereof |
| CN109431871A (en) * | 2018-12-25 | 2019-03-08 | 安徽爱迪香料股份有限公司 | A kind of preparation method for the long-acting refrigerant preparation making an addition to the cool cream of external application |
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| Publication number | Publication date |
|---|---|
| CN102871853B (en) | 2015-02-04 |
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