CN102783741A - Multistage-spreading heat-dissipation fire-proof heat-insulation composite fabric, preparation method and application - Google Patents
Multistage-spreading heat-dissipation fire-proof heat-insulation composite fabric, preparation method and application Download PDFInfo
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- CN102783741A CN102783741A CN2012102932073A CN201210293207A CN102783741A CN 102783741 A CN102783741 A CN 102783741A CN 2012102932073 A CN2012102932073 A CN 2012102932073A CN 201210293207 A CN201210293207 A CN 201210293207A CN 102783741 A CN102783741 A CN 102783741A
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Abstract
The invention relates to a preparation method and an application of multistage-spreading heat-dissipation fire-proof heat-insulation composite fabric. The multistage-spreading heat-dissipation fire-proof heat-insulation composite fabric is formed by successively arranging and laminating a metal foil reflection layer, a phase change temperature limitation layer, an interval composite membrane heat-insulation layer and a flame-retardant comfortable layer, wherein the metal foil reflection layer has high reflectivity and an enhanced heat-dissipation function; the phase change temperature limitation layer has functions of high energy consumption absorption and evenly-distributed heat conduction; the interval composite membrane heat-insulation layer has the functions of reflection insulation and even distribution of heat; and the flame-retardant comfortable layer has the functions of low-contact heat conduction, heat insulation and comfort. When the front side of the multistage-spreading heat-dissipation fire-proof heat-insulation composite fabric is under the action of open fire and strong heat flow environment, the back side of the multistage-spreading heat-dissipation fire-proof heat-insulation composite fabric can be kept below 50DEG C which is near the safe temperature state of the human skin, and the integral structural form and the mechanical property are stable. The natural thickness of the composite fabric is 5-15mm, the compression thickness of the composite fabric is 3-8mm, and the square meter quality of the composite fabric is 400-1500g/m<2>. The composite fabric is fire-proof heat-insulation material which is totally sealed, stuck and sewn and can be used for individual protection and environment heat insulation in special high-temperature occasions, such as fire control, military, exploration, safe escape and industry and the like.
Description
Technical field
It is technological to the present invention relates to the adiabatic frivolous flexible composite with protection of human body or environment temperature, is a kind of preparation and purposes of fire-proof heat-insulating compound fabric of multiple development heat radiation.This fire-proof heat-insulating compound fabric is heat insulation applicable to the physical protection and the environment of special occasions such as fire-fighting, military affairs, exploration, industry, belongs to composite material for weaving and the function technology is used textile field.
Background technology
Under high temperature heat-flash environment such as the scene of a fire, the topmost potential danger of existence comprises: the hot environment in the scene of a fire, especially radiant heat are dangerous to the burn of human body; The protective gear utensil is ignited by flame and contacts the high temp objects surface and causes heat conduction at a high speed, causes the danger of human body burn etc.Therefore, burn and operate as normal for unlikely, fire-fighting and particular job personnel should wear function clothes and carry out effective heat insulation protection.
Data shows, the hot-fluid that is produced by the naked light burning things which may cause a fire disaster removes (the being lower than 30%) convection current of few part, the radiant heat of how propagating with the electromagnetic wave form to around dispel the heat.Because the radiant heat penetration power is strong, be easy to cause the human body burn or burn, so fire-fighting class fire-proof heat-insulating fabric focus on reduce the radiant heat infiltration, reduce the heat conduction, protective garment deep layer programming rate is slowed down.So, the fire-proof heat-insulating fabric not only want the surface to radiant heat have highly reflective can, and itself to have high function of inhaling power consumption and quick heat radiating, also fire-resistant, high temperature resistant, with realize to burning things which may cause a fire disaster or thermal source efficiently completely cut off and to the safe and effective protection of human body.
For the fire-proof heat-insulating kind fabric, more research and patent are arranged in recent years.Be made up of aluminium foil, PET polyester film and aramid fiber plain woven base cloth like fireman's protective clothing for proximity fire fighting lining (patent No. CN200920211471.1), wherein aluminium foil is the thick rolling aluminum foils of 7 μ m; This invention obtains good penetrating quality of anti radiant heat effect, but because the restriction of thickness and PET polyester film fusing point, its thermal protection effect is very limited.Heat resistanceheat resistant radiation heat-resistant fireproof protective garment fabric (patent No. CN200920309275.8) adopts the composite construction of the overcoat of from inside to outside heat-resisting, flame-retardant textile fibrage, adhesive layer and heat resistanceheat resistant radiation, and wherein heat resistanceheat resistant radiation protection layer is the polyester aluminizer of 20～25 μ m; Protective garment fabric of the present invention has heat resistanceheat resistant radiativity preferably, and light weight, high temperature resistant, shrinkage factor is little, but polyester aluminizer resistance to elevated temperatures is limited.
The multi-layer compound fabric that aluminium foil fire-proof and thermal-insulation gloves (patent No. CN201020276197.9) are made up of the layer of anti-flame the, thermal insulation layer and endonexine is processed.Wherein the layer of anti-the flame is composited by the tissue layer that the blending of Ripstop rule weaves by aluminium foil layer with aramid fiber and antistatic cotton; Thermal insulation layer adopts permanent fire retardant nonwoven fabric.Gloves have reduced the danger that contacts with thermal source, have strengthened the isolating and protecting to high temperature.
Heat insulating coat fabric (patent No. CN201010222904.0) with reflecting layer, radiating layer multiplet is made by base cloth and the heat-insulating slurry that is coated on the base cloth, and wherein heat-insulating slurry is for containing nano-TiO
2The radiation function layer with contain the double-layer structure of the reflection function layer of hollow glass microballoon.Coated fabric can be realized good effect of heat insulation through the radiation function of radiating layer after through the reflection function in reflecting layer again, but is inappropriate for the use under the high temperature fire field environment.
The nano combined fabric coating material of anti-optical heat radiation (patent No. CN200910181069.8) can form ceramic photothermal reflectance layer at fabric face through special process, and nanometer titanium compound reflecting layer and stabilized zone play near infrared ray and visible light are reflected.Test result shows that the composite Nano fabric coating can reach more than 81% in the heat reflective radiation.The high temperature resistant lining of heat resistanceheat resistant radiation (patent No. CN201020644530.7), ecto-entad are respectively the resistant to elevated temperatures polyester metallized film overcoat that thickness is 20-25 μ m, polyurethane adhesive gluing layer and the alumina silicate fibre layer that thickness is 2-6 μ m is composited.This lining mainly is to the radiant heat protection, though the polyester metallized film has certain high temperature stability, in the face of the scene of a fire high temperature heat-flash stream environment time, is easy to be melted destruction.
Heat insulating compound film (patent No. CN200510024710.9) is the patent of invention before the applicant, adopt by the high polymer basement membrane of high-strength low heat conductivity coefficient, highly reflective can metal oxide layer and the structure that the outer overlay film of the heat bondable high polymer of low heat conductivity is composited of metal level, high thermal insulation realize efficient, lightweight, the flexible multi-functional thermal protection of (150～120 ℃) under the high and low temperature environment.
Heat insulation soft thin composite fabric (patent No. CN200410066650.2) also is the patent of invention before the applicant; One side adopts the high performance coated fabric of high-and low-temperature resistance; That another side adopts is soft, comfortable, frost prevention, prevent the coated fabric of condensation; The middle high polymer of multilayer insulation and the compound fabric that metal composite film constitutes of adopting; But the lining meshi fabric of tape thickness, dimensionally stable between MULTILAYER COMPOSITE is realized simultaneously can bearing high temperature, low temperature or high and low temperature compound action, and one side keeps 5～35 ℃ of nearly room temperature states; The natural thickness of compound fabric of the present invention is at 3～12mm, and weight per square meter is at 150～550g/m
2, can realize the heat insulation and protection under-130～120 ℃ of conditions.Though widely applicable, effect of heat insulation is limited.This patent is not a fire resistance applications, and both flames of anger radiant heat high reflection layers, do not have the decalescence limit temperature layer that dissipates, and the preparation method is different yet.
By prepared Thermal Protective Fabric of above patented technology or thermal isolation film; Though have the performance of radiation proof heat leak preferably; But in practical application; Owing to receive the restriction of foil polymer matrix and heat conductivility, receive the high temperature heat-flash to do the time spent and cause the material surface heat to concentrate easily to damage, burnt or burn in the utmost point short time like the cognition of end user under 800～1000 ℃ the high temperature scene of a fire with hot-spot.
Summary of the invention
An object of the present invention is to provide the multiple development heat radiation fire-proof heat-insulating compound fabric of a kind of radiation proof heat leak and burn-off function admirable, lightweight, flexibility.Another object of the present invention provides a kind of Preparation method and use of above-mentioned compound fabric.
In order to achieve the above object, principle of the present invention is by metal forming reflecting layer, phase transformation limit temperature layer, composite membrane heat insulation layer and fire-retardant comfort liner realize that the fire-proof heat-insulating Function Decomposition shares and dissipate at interval through design.Realize isolated and to the diffusion of infiltration heat be uniformly distributed with to the photothermal reflection in the scene of a fire with high reflectance and the metal forming reflecting layer that strengthens heat sinking function; Inhale power consumption with height and be uniformly distributed with the absorption dissipation and evenly diffusion of the phase transformation limit temperature layer realization of function infiltration radiant heat and conduction heat with hot conduction; Realize isolated and be uniformly distributed with dissipation to the further emission of fabric heat with reflection, interval composite membrane heat insulation layer isolated and that be uniformly distributed with the heat function; Guarantee the safety of human body and comfortable with low thermal contact conductance and fire-retardant fire-retardant comfort liner; The fire-proof heat-insulating protection system that the compound fabric that is composited with above-mentioned each functional structure layer dispels the heat as multiple development.The fire-proof heat-insulating compound fabric have lightweight, flexibility, flame resistant impact, high high-temp stability and radiant heat barrier propterty good, when being heated surface and internal heat evenly distribute, characteristics such as reusable.This compound fabric is that metal forming reflecting layer, high suction power consumption phase transformation are limit temperature layer, interval composite membrane heat insulation layer and fire-retardant comfort liner, thereby realized that the highly effective and safe to human body protects under the high temperature heat-flash environment of the scene of a fire towards the order of burning things which may cause a fire disaster or thermal source.
A concrete technical scheme of the present invention has provided a kind of fire-proof heat-insulating compound fabric of multiple development heat radiation; It is characterized in that: by having high reflectance and the metal forming reflecting layer that strengthens heat sinking function, having and highly inhale phase transformation limit temperature layer that power consumption and heat conduction be uniformly distributed with function, have reflection, completely cut off and be uniformly distributed with the interval composite membrane heat insulation layer of heat function and have low thermal contact conductance and the fire-retardant comfort liner of fire-retardant and comfortable function is arranged in order and constitutes; Wherein, The metal forming reflecting layer is positive; Towards flame or high temperature source, fire-retardant comfort liner is a reverse side, towards human body.
Preferably, said metal forming reflecting layer bonding being composited of enhancing base cloth of processing by metal forming that is positioned at the outermost top layer and the high temperature resistant yarn that has metallic fiber that is positioned at sublevel;
Metal forming is that thickness is pure aluminum foil or the alloy foil of 5～10 μ m, has good reflect radiation heat performance and leads performance;
High temperature resistant yarn is to be formed by glass fibre or basalt fibre and metallic fiber composite spinning; Metallic fiber is stainless steel fibre or copper fiber; Metallic fiber is 1～10% with the compound ratio of glass fibre or basalt fibre, yarn is strengthened and heat is spread rapidly and be uniformly distributed with.
Utilize the metal forming of high compactness that light, the heat radiation of scene of a fire high temperature intense radiation hot-fluid environment are realized that good reflection is isolated; Metallic fiber in the high temperature resistant yarn can make the heat that penetrates metal forming spread rapidly and be uniformly distributed with.
Preferably; Said phase transformation limit temperature layer by the high-temperature fibre felt that is mixed with broken-staple metal fibre with have leakproof base cloth Compound Machining wiry and form; In the high-temperature fibre felt, the phase transformation powder can be realized the height of radiation osmotic heat and conduction heat is absorbed dissipation 200～400 ℃ of phase transformation powder adherence that solid-liquid phase change can take place;
The high-temperature fibre felt is glass mat or basalt fibre felt, and thermal adaptability is room temperature～800 ℃;
Broken-staple metal fibre is stainless steel short fiber or copper short fiber, with the rapid diffusion that increases heat be distributed in phase transformation heat dissipation in the high-temperature fibre felt, concentrate or hot-spot and reduce heat;
Wire is stainless steel wire or copper wire, to strengthen the leakproof base cloth and to increase the diffusion of after-heat and be uniformly distributed with dissipation;
The leakproof base cloth is that resistant to elevated temperatures basalt fibre or glass fibre and composite yarn wiry are processed woven cloth, is used for preventing that the phase transformation powder is in processing and the leakage used.
The high-temperature fibre felt is as the carrier of broken-staple metal fibre and phase transformation powder, the rapid diffusion that heat is realized in compound back be uniformly distributed with and high the absorption dissipated, concentrate or hot-spot thereby reduce heat.Having leakproof base cloth wiry can increase the diffusion of after-heat and be uniformly distributed with dissipation, and can prevent the leakage of phase transformation powder in processing and use.
Preferably, said interval composite membrane heat insulation layer and said fire-retardant comfort liner be sutured mutually, and said interval composite membrane heat insulation layer is closed by 4～20 layers of plating high polymer complex film layer and forms, and closes the lining meshi fabric at the intermembranous layer of adjacent two layers plating high polymer complex film;
The plating high polymer complex film is the aluminizing of terylene, polyimides or polyamide fibre high polymer base, alloy plating or gold-plated film;
The lining meshi fabric is the gridding lightweight reticulated that adopts weaving method to be shaped by terylene, polyamide fibre or aramid fiber long filament.
Closing the isolated and conduction of the reflection multilayer of realizing heat with the layer of multilayer complex films is uniformly distributed with.
Preferably, said fire-retardant comfort liner is a kind of in flame-proof cotton fabric, flame-resistant terylene fabric or the Nomex fabric.
The residue high temperature (about 100 ℃) that the fire-retardant comfort liner of low thermal contact conductance is primarily aimed at after the aforementioned functional structure sheaf is shared the decomposition in the high temperature scene of a fire carries out follow-up heat insulation and heat control and guarantees that human body is comfortable and easy to wear.
Another technical scheme of the present invention has provided a kind of preparation method of fire-proof heat-insulating compound fabric of above-mentioned multiple development heat radiation; It is characterized in that; Step is: with in the fire-proof heat-insulating compound fabric of above-mentioned multiple development heat radiation except that the metal forming in metal forming reflecting layer Manufactured each layer or organize composite bed and go ahead of the rest after the sutured; Again with metal forming with high temperature resistant binder evenly, point bonding is in the front; Airtight to form, smooth, unabroken natural thickness is 5～15mm, and the actual thickness that compresses is 3～8mm, and square metre quality is at 400～1500g/m
2The fire-proof heat-insulating compound fabric, in this fire-proof heat-insulating compound fabric, comprise the passage that dispels the heat except that all each layer formation multiple developments of lining meshi fabric and fire-retardant comfort liner.
Preferably, the natural thickness≤14mm of said phase transformation limit temperature layer and said interval composite membrane heat insulation layer sum, square metre quality≤1100g/m
2
Another technical scheme of the present invention has provided a kind of purposes of fire-proof heat-insulating compound fabric of above-mentioned multiple development heat radiation, it is characterized in that: be applicable to the heat insulation protective materials of using safely under 500～1000 ℃ of high temperature heat-flash filariasis field environmental conditions.
About the processing of containing metal silk composite yarn with in the application aspect the function fabric, applicant has been applied for related patent U.S. Patent No..In the electromagnetic shielding yarn and production equipment and production method (patent No. CN201110242817.6) of a kind of suction wave height bullet yarn and production equipment and production method (patent No. CN201110242760.X) and wire looping elastic filament; All adopt ring spinning frame to make to have inhale ripple and electro-magnetic screen function by outer felt around the composite yarn formed of bag cored structure yarn section and inner elastic filament, wherein wrap cored structure yarn section and process by the short fiber yarn that wire and helical form are wrapped in outside the wire.Had the spinning technology and equipment of the composite yarn of ripe containing metal silk in the seminar of applicant, made composite yarn obtains effective application in each functional structure layer of the present invention.
The present invention is directed to intense radiation heat and the hot-spot problem of conducting thermo-lag demand and fire-fighting class heat-protective clothing existence at present under the high temperature fire field environment (800～1000 ℃); Adopt suitable stitching and bonding process; The high conduction heat dispersion of high radiation reflecting properties, containing metal silk or the broken-staple metal fibre fabric of comprehensive utilization metal forming, the height of high temperature phase change material (pcm) are inhaled the high thermal insulation of energy-dissipating property and interval composite membrane; Make the fire-proof heat-insulating compound fabric of multiple development heat radiation, to realize under the high temperature fire field environment safe and effective protection to human body.
Compared with prior art, the present invention includes following advantage:
1, the fire-proof heat-insulating compound fabric is four functional layer composite constructions; Except that having strengthened that the radiation osmotic heat in the high temperature scene of a fire and the height of conduction heat are absorbed the dissipation; The smart application of interior metal filament of major function layer or short fiber has been strengthened the rapid deployment heat radiation of heat in each layer and has been uniformly distributed with; Form the multiple development heat dissipation channel, avoided heat to concentrate or hot-spot, realize highly effective and safe protection human body.Add that the people constantly moves and rotates, security and effective storage life significantly increase.
2, fire-proof heat-insulating compound fabric function sharing is reasonable, complete: the metal forming reflecting layer can reflect away the photothermal major part that light, heat radiation thermal source produce; The warm layer of phase transformation limit can realize that the height absorption of radiation osmotic heat and conduction heat dissipates and temperature is ended; The composite membrane heat insulation layer can completely cut off the heat realization reflection multilayer of inside and be uniformly distributed with at interval; Fire-retardant comfort liner can be realized that follow-up low temperature is heat insulation and guarantee human comfort.
3, the fire-proof heat-insulating compound fabric is frivolous, flexible material, radiation proof infiltration and burn-off function admirable, and reusability is strong, can be used for the clothes of the lifesaving environment of speedily carrying out rescue work such as the scene of a fire, battlefield, also can be used for the Aero-Space protective materials.
Description of drawings
Fig. 1 is the layer structure sketch map of the fire-proof heat-insulating compound fabric of multiple development heat radiation.
Among the figure: 1-metal forming reflecting layer (towards open flame source), it comprises 11-high-reflectivity metal paper tinsel, 12-is high temperature resistant enhancing base cloth, 13-wire; 2-phase transformation limit temperature layer, it comprises 21-high-temperature fibre felt, 22-phase transformation powder, the 23-broken-staple metal fibre, 24-strengthens leakproof base cloth, 25-wire; 3-is the composite membrane thermal insulation layer at interval, and it comprises 31-plating high polymer complex film, and 32-serves as a contrast meshi fabric; The fire-retardant comfort liner of 4-is near human body; 5-multiple development heat dissipation channel.
The specific embodiment
For making the present invention more obviously understandable, now with preferred embodiment, and conjunction with figs. elaborates as follows.Should be understood that these embodiment only to be used to the present invention is described and be not used in the restriction scope of the present invention.Should be understood that in addition those skilled in the art can do various changes or modification to the present invention after the content of having read the present invention's instruction, these equivalent form of values fall within the application's appended claims institute restricted portion equally.
As shown in Figure 1; The invention provides a kind of fire-proof heat-insulating compound fabric of multiple development heat radiation; By having high reflectance and the metal forming reflecting layer 1 that strengthens heat sinking function, having and highly inhale phase transformation limit temperature layer 2 that power consumption and heat conduction be uniformly distributed with function, have reflection, completely cut off and be uniformly distributed with the interval composite membrane heat insulation layer 3 of heat function and have low thermal contact conductance and the fire-retardant comfort liner 4 of fire-retardant and comfortable function is arranged in order and constitutes; Wherein, metal forming reflecting layer 1 is positive, towards flame or high temperature source; Fire-retardant comfort liner 4 is a reverse side, towards human body.
Enhancing base cloth 12 bonding being composited that metal forming reflecting layer 1 is processed by metal forming that is positioned at the outermost top layer 11 and the high temperature resistant yarn that has metallic fiber 13 that is positioned at sublevel;
Metal forming 11 is pure aluminum foil or the alloy foil of 5～10 μ m for thickness;
High temperature resistant yarn is to be formed by glass fibre or basalt fibre and metallic fiber 13 composite spinnings; Metallic fiber 13 is stainless steel fibre or copper fiber; The compound ratio that metallic fiber 13 mixes with glass fibre or basalt fibre is 1～10%, yarn is strengthened and heat is spread rapidly and be uniformly distributed with.
Phase transformation limit temperature layer 2 is formed by high-temperature fibre felt that is mixed with broken-staple metal fibre 23 21 and leakproof base cloth 24 Compound Machining that have wire 25, sticks in the high-temperature fibre felt 21 at 200～400 ℃ of phase transformation powder 22 that solid-liquid phase change can take place;
High-temperature fibre felt 21 is glass mat or basalt fibre felt;
Broken-staple metal fibre 23 is stainless steel short fiber or copper short fiber, with the rapid diffusion that increases heat be distributed in phase transformation heat dissipation in the high-temperature fibre felt 21, concentrate or hot-spot and reduce heat;
Wire 25 is stainless steel wire or copper wire, to strengthen leakproof base cloth 24 and to increase the diffusion of after-heat and be uniformly distributed with dissipation;
Leakproof base cloth 24 is processed woven cloth for the composite yarn of resistant to elevated temperatures basalt fibre or glass fibre and wire 25, is used for preventing the leakage of phase transformation powder 22 in processing and use.
Composite membrane heat insulation layer 3 and fire-retardant comfort liner 4 sutured mutually at interval, composite membrane heat insulation layer 3 is closed for 31 layers by 4～20 layers of plating high polymer complex film and forms at interval, closes at the intermembranous layer of adjacent two layers plating high polymer complex film 31 and serves as a contrast meshi fabric 32;
Plating high polymer complex film 31 is the aluminizing of terylene, polyimides or polyamide fibre high polymer base, alloy plating or gold-plated film;
Lining meshi fabric 32 is the gridding lightweight reticulateds that adopt weaving method to be shaped by terylene, polyamide fibre or aramid fiber long filament.
Fire-retardant comfort liner 4 is a kind of in flame-proof cotton fabric, flame-resistant terylene fabric or the Nomex fabric.
The present invention also provides a kind of preparation method of fire-proof heat-insulating compound fabric of above-mentioned multiple development heat radiation; The steps include: with in the fire-proof heat-insulating compound fabric of above-mentioned multiple development heat radiation except that the metal forming 11 in metal forming reflecting layer 1 Manufactured each layer or organize composite bed and go ahead of the rest after the sutured; Again with metal forming 11 usefulness high temperature resistant binders evenly, point bonding is in the front; Airtight to form, smooth, unabroken natural thickness is 5～15mm; The actual thickness that compresses is 3～8mm, and square metre quality is at 400～1500g/m
2The fire-proof heat-insulating compound fabric, in this fire-proof heat-insulating compound fabric, comprise the passage 5 that dispels the heat except that all each layer formation multiple developments of lining meshi fabric 32 and fire-retardant comfort liner 4.
More preferably, the natural thickness≤14mm of phase transformation limit temperature layer 2 and interval composite membrane heat insulation layer 3 sums, square metre quality≤1100g/m
2
Following specific embodiment 1～4th is selected different metallic paper tinsel, fibrous material, phase transformation powder, plating high-polymer membrane material, lining meshi fabric, flame-retardant textile; Different natural thickness, compress thickness, square metre quality; The fire-proof heat-insulating compound fabric of actual fabrication multiple development heat radiation of the present invention; And to the gained compound fabric in the different scenes of a fire and the inboard under the hot conditions be that reverse side limits maximum temperature and lasting maximum duration is surveyed, see following table for details.Simultaneously, the compound fabric that stands behind flame and the high temperature action is done ocular estimate and the measurement and the ocular estimate of repeated test for the second time, the result sees following table and following statement for details.
Embodiment 1
Adopt multiple development of the present invention heat radiation the fire-proof heat-insulating compound fabric four-layer structure and like the material of following table; And adopt the prepared fire-proof heat-insulating compound fabric of preparation method of the present invention; Be placed under 800 ℃ of scene of a fire conditions, the inboard of actual measurement is that the maximum temperature that limits of reverse side and lasting maximum duration thereof are shown in following table embodiment 1 hurdle.Actual visual observations, the surface is excellent, rubs and bend no obvious brittle point or crackle.After cooling, put into same scene of a fire condition once more, shown in qualification maximum temperature when handle the second time of gained and lasting maximum duration thereof see the following form, no change is described; And actual measurement is observed once more, and this compound fabric surface is excellent, rubs and bend no obvious brittle point or crackle.Prove this compound fabric fire-proof heat-insulating stable performance thus, can repeatedly use.If 800 ℃ flames are concentrated in this compound center 2cm scope of knitting sample, 50 ℃ duration of the qualification that the reverse side central point reaches can reach 12.5min, has improved 21.36% relatively, explains that thermal diffusion heat dissipation and effect of heat insulation are obvious.
Embodiment 2
Adopt multiple development of the present invention heat radiation the fire-proof heat-insulating compound fabric four-layer structure and like the material of following table; And adopt the prepared fire-proof heat-insulating compound fabric of preparation method of the present invention; Be placed under 1000 ℃ of scene of a fire conditions, the inboard of actual measurement is that the maximum temperature that limits of reverse side and lasting maximum duration thereof are shown in following table embodiment 2 hurdles.Actual visual observations, the surface is excellent, rubs and bend no obvious brittle point or crackle.After cooling, put into same scene of a fire condition once more, shown in qualification maximum temperature when handle the second time of gained and lasting maximum duration thereof see the following form, no change is described, lasting maximum duration also slightly is increase, is due to the bulking of material; And actual measurement is observed once more, and this compound fabric surface is excellent, rubs and bend no obvious brittle point or crackle.Prove this compound fabric fire-proof heat-insulating stable performance thus, can repeatedly use.If 1000 ℃ flames are concentrated in this compound center 2cm scope of knitting sample, 45 ℃ duration of the qualification that the reverse side central point reaches can reach 13.6min, has improved 24.77% relatively, explains that thermal diffusion heat dissipation and effect of heat insulation are obvious.
Embodiment 3
Adopt multiple development of the present invention heat radiation the fire-proof heat-insulating compound fabric four-layer structure and like the material of following table; And adopt the prepared fire-proof heat-insulating compound fabric of preparation method of the present invention; Be placed under 600 ℃ of scene of a fire conditions, the inboard of actual measurement is that the maximum temperature that limits of reverse side and lasting maximum duration thereof are shown in following table embodiment 3 hurdles.Actual visual observations, the surface is excellent, rubs and bend no obvious brittle point or crackle.After cooling, put into same scene of a fire condition once more, shown in qualification maximum temperature when handle the second time of gained and lasting maximum duration thereof see the following form, no change is described, lasting maximum duration also slightly is increase, is due to the bulking of material; And actual measurement is observed once more, and this compound fabric surface is excellent, rubs and bend no obvious brittle point or crackle.Prove this compound fabric fire-proof heat-insulating stable performance thus, can repeatedly use.If 600 ℃ flames are concentrated in this compound center 2cm scope of knitting sample, 50 ℃ duration of the qualification that the reverse side central point reaches can reach 9.9min, has improved 23.75% relatively, explains that thermal diffusion heat dissipation and effect of heat insulation are obvious.
Embodiment 4
Adopt multiple development of the present invention heat radiation the fire-proof heat-insulating compound fabric four-layer structure and like the material of following table; And adopt the prepared fire-proof heat-insulating compound fabric of preparation method of the present invention; Be placed under 1000 ℃ of scene of a fire conditions; The inboard of actual measurement is that the maximum temperature that limits of reverse side and lasting maximum duration thereof are shown in following table embodiment 4 hurdles; Being that the fire-proof heat-insulating index is optimum in four kinds of samples, mainly is phase transformation limit temperature layer phase transformation amount of powder and the number of plies of composite membrane thermal insulation layer is at interval selected proper.Actual visual observations, the surface is excellent, rubs and bend no obvious brittle point or crackle.After cooling, put into same scene of a fire condition once more, shown in qualification maximum temperature when handle the second time of gained and lasting maximum duration thereof see the following form, no change is described, lasting maximum duration also slightly is increase, is due to the bulking of material; And actual measurement is observed once more, and this compound fabric surface is excellent, rubs and bend no obvious brittle point or crackle.Prove this compound fabric fire-proof heat-insulating stable performance thus, can repeatedly use.If 1000 ℃ flames are concentrated in this compound center 2cm scope of knitting sample, 45 ℃ duration of the qualification that the reverse side central point reaches can reach 15.3min, has improved 26.44% relatively, explains that thermal diffusion heat dissipation and effect of heat insulation are obvious.
Formation, structural parameters and the measured result of the fire-proof heat-insulating compound fabric of multiple development heat radiation
Claims (8)
1. the fire-proof heat-insulating compound fabric of multiple development heat radiation; It is characterized in that: by having high reflectance and the metal forming reflecting layer (1) that strengthens heat sinking function, having and highly inhale phase transformation limit temperature layer (2) that power consumption and heat conduction be uniformly distributed with function, have reflection, completely cut off and be uniformly distributed with the interval composite membrane heat insulation layer (3) of heat function and have low thermal contact conductance and the fire-retardant comfort liner of fire-retardant and comfortable function (4) is arranged in order formation; Wherein, Metal forming reflecting layer (1) is positive; Towards flame or high temperature source, fire-retardant comfort liner (4) is a reverse side, towards human body.
2. the fire-proof heat-insulating compound fabric of a kind of multiple development heat radiation as claimed in claim 1 is characterized in that: said metal forming reflecting layer (1) is by the metal forming that is positioned at the outermost top layer (11) and be positioned at bonding being composited of enhancing base cloth (12) that the high temperature resistant yarn that has metallic fiber (13) of sublevel is processed;
Metal forming (11) is pure aluminum foil or the alloy foil of 5～10 μ m for thickness;
High temperature resistant yarn is to be formed by glass fibre or basalt fibre and metallic fiber (13) composite spinning; Metallic fiber (13) is stainless steel fibre or copper fiber; Metallic fiber (13) is 1～10% with the compound ratio of glass fibre or basalt fibre, yarn is strengthened and heat is spread rapidly and be uniformly distributed with.
3. the fire-proof heat-insulating compound fabric of a kind of multiple development heat radiation as claimed in claim 1; It is characterized in that: said phase transformation limit temperature layer (2) is formed by high-temperature fibre felt (21) that is mixed with broken-staple metal fibre (23) and leakproof base cloth (24) Compound Machining that has wire (25), sticks in the high-temperature fibre felt (21) at 200～400 ℃ of phase transformation powder (22) that solid-liquid phase change can take place;
High-temperature fibre felt (21) is glass mat or basalt fibre felt;
Broken-staple metal fibre (23) is stainless steel short fiber or copper short fiber, with the rapid diffusion that increases heat be distributed in phase transformation heat dissipation in the high-temperature fibre felt (21), concentrate or hot-spot and reduce heat;
Wire (25) is stainless steel wire or copper wire, to strengthen leakproof base cloth (24) and to increase the diffusion of after-heat and be uniformly distributed with dissipation;
Leakproof base cloth (24) is processed woven cloth for the composite yarn of resistant to elevated temperatures basalt fibre or glass fibre and wire (25), is used for preventing the leakage of phase transformation powder (22) in processing and use.
4. the fire-proof heat-insulating compound fabric of a kind of multiple development heat radiation as claimed in claim 1; It is characterized in that: said interval composite membrane heat insulation layer (3) and said fire-retardant comfort liner (4) be sutured mutually; Said interval composite membrane heat insulation layer (3) is closed by 4～20 layers of plating high polymer complex film (31) layers and forms, and closes lining meshi fabric (32) at the intermembranous layer of adjacent two layers plating high polymer complex film (31);
Plating high polymer complex film (31) is the aluminizing of terylene, polyimides or polyamide fibre high polymer base, alloy plating or gold-plated film;
Lining meshi fabric (32) is the gridding lightweight reticulated that adopts weaving method to be shaped by terylene, polyamide fibre or aramid fiber long filament.
5. the fire-proof heat-insulating compound fabric of a kind of multiple development heat radiation as claimed in claim 1 is characterized in that: a kind of in flame-proof cotton fabric, flame-resistant terylene fabric or the Nomex fabric of said fire-retardant comfort liner (4).
6. the preparation method of the fire-proof heat-insulating compound fabric of a multiple development as claimed in claim 1 heat radiation; It is characterized in that; Step is: with in the fire-proof heat-insulating compound fabric of multiple development as claimed in claim 1 heat radiation except that the metal forming (11) of metal forming reflecting layer (1) Manufactured each layer or organize composite bed and go ahead of the rest after the sutured; Again with metal forming (11) with high temperature resistant binder evenly, point bonding is in the front; Airtight to form, smooth, unabroken natural thickness is 5～15mm, and the actual thickness that compresses is 3～8mm, and square metre quality is at 400～1500g/m
2The fire-proof heat-insulating compound fabric, in this fire-proof heat-insulating compound fabric, comprise the passage (5) that dispels the heat except that all each layers formation multiple developments of lining meshi fabric (32) and fire-retardant comfort liner (4).
7. the preparation method of the fire-proof heat-insulating compound fabric of a kind of described multiple development heat radiation as claimed in claim 6; It is characterized in that: the natural thickness≤14mm of said phase transformation limit temperature layer (2) and said interval composite membrane heat insulation layer (3) sum, square metre quality≤1100g/m
2
8. the purposes of the fire-proof heat-insulating compound fabric of a multiple development heat radiation as claimed in claim 1 is characterized in that: be applicable to the heat insulation protective materials of using safely under 500～1000 ℃ of high temperature heat-flash filariasis field environmental conditions.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210293207.3A CN102783741B (en) | 2012-08-16 | 2012-08-16 | Multistage-spreading heat-dissipation fire-proof heat-insulation composite fabric, preparation method and application |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210293207.3A CN102783741B (en) | 2012-08-16 | 2012-08-16 | Multistage-spreading heat-dissipation fire-proof heat-insulation composite fabric, preparation method and application |
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| Publication Number | Publication Date |
|---|---|
| CN102783741A true CN102783741A (en) | 2012-11-21 |
| CN102783741B CN102783741B (en) | 2014-10-15 |
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|---|---|---|---|
| CN201210293207.3A Active CN102783741B (en) | 2012-08-16 | 2012-08-16 | Multistage-spreading heat-dissipation fire-proof heat-insulation composite fabric, preparation method and application |
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