CN102190954A - Wear-resistant nonskid polyurethane deck paint, and manufacture method thereof - Google Patents
Wear-resistant nonskid polyurethane deck paint, and manufacture method thereof Download PDFInfo
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Abstract
The invention relates to a wear-resistant nonskid polyurethane deck paint, and a manufacture method thereof. The manufacture method comprises the following steps of: adding a hydroxyl acrylic resin, polyether polyol, hydroxyl-containing fluorocarbon acrylic resin, a polyacrylate copolymer solution, poly(methyl alkyl siloxane) solution and [b-[3-(2-H-benzotriazol-2-yl)-5-(1,1-dimethylethyl)-4-hydroxyphenyl]-1-oxopropyl]-hydroxypoly(oxo-1,2-ethanediyl) to a mixed solvent of xylene, n-butyl acetate, methyl isobutyl ketone and butanone for high-speed stirring; adding rutile titanium white powder, talcum powder, aluminum oxide ceramic powder, sericite powder, silicon micropowder, carbon black and gas-phased silicon dioxide; milling with a sand mill while controlling fineness of a mixture not higher than 60 mu m to obtain a liquid A; and forming a liquid B by a mixed solution of 1,6-hexamethylene diisocyanate tripolymer, anhydrous xylene and n-butyl acetate, and mixing 1 weight part of the liquid A with 0.2-1.0 weight part of the liquid B for use. The obtained wear-resistant nonskid polyurethane deck paint can be used for the corrosion protection of the steel surfaces of deck and ocean facilities.
Description
Technical field
The present invention relates to a kind of wear-resisting anti-skidding urethane porch paint and manufacture method, being used for boats and ships, ocean platform etc. needs the anticorrosion of the deck of weather-proof, anti-skid wearable, seawater corrosion resistance and other maritime facilities steel surfaces.
Background technology
Existing porch paint is used for the protection against corrosion of boats and ships, harbour and other maritime facilities steel surfaces, better weather, salt fog resistance are arranged, its weak point is that the paint film wear resistance is relatively poor, fillers such as quartz sand, rubber grain are added in the need back increases anti-skid, and paint film is rigidity, and shock-resistance is relatively poor.
Summary of the invention
The purpose of this invention is to provide a kind of wear-resisting anti-skidding urethane porch paint and manufacture method.
Wear-resisting anti-skidding urethane porch paint of the present invention, it is made up of A liquid and B liquid, and wherein A liquid is by 1 weight part Hydroxylated acrylic resin, 0.1～0.8 weight part polyether glycol, 0.1～0.8 weight part hydroxyl fluorocarbon acrylic acid resin, 0.1～1.0 weight part dimethylbenzene, 0.1～1.0 weight part n-butyl acetates, 0.01～0.15 weight part mibk, 0.05～0.15 weight part butanone, 0.1～1.0 weight part Rutile type Titanium Dioxides, 0.01～0.5 weight part talcum powder, 0.01～0.8 weight part alumina-ceramic powder, 0.01～0.8 weight part sericite in powder, 0.01～0.6 weight part silicon powder, 0.01～0.2 weight part carbon black, 0.01～0.1 weight part polyacrylic ester interpolymer solution, 0.01～0.1 weight part gathers methyl alkyl siloxane solution, 0.01～0.1 weight part b-[3-(2-H-benzotriazole-2-yl)-4-hydroxyl-5-tert-butyl-phenyl]-propionic acid Liquid Macrogol ester, 0.005～0.1 weight part aerosil is formed; B liquid is made up of 1 weight part hexamethylene diisocyanate tripolymer, 0.1～0.5 weight part anhydrous dimethyl benzene, 0.1～0.5 weight part n-butyl acetate mixing solutions, is made up of 1 weight part A liquid and 0.2～1.0 weight part B liquid during use.
The wear-resisting anti-skidding urethane porch paint that the present invention is more excellent, it is characterized in that being made up of A liquid and B liquid, wherein A liquid is by 1 weight part Hydroxylated acrylic resin, 0.5 weight part polyether glycol, 0.3 weight part hydroxyl fluorocarbon acrylic acid resin, 0.05 weight part polyacrylic ester interpolymer solution, 0.06 weight part gathers methyl alkyl siloxane solution, 0.03 weight part b-[3-(2-H-benzotriazole-2-yl)-4-hydroxyl-5-tert-butyl-phenyl]-propionic acid Liquid Macrogol ester, 1.0 weight part dimethylbenzene, 1.0 weight part n-butyl acetate, 0.1 weight part mibk, 0.1 weight part butanone, 0.3 weight part Rutile type Titanium Dioxide, 0.05 weight part talcum powder, 0.4 weight part alumina-ceramic powder, 0.2 weight part sericite in powder, 0.3 weight part silicon powder, 0.05 weight part carbon black, 0.01 the weight part aerosil is made A liquid; Form B liquid by 1 weight part hexamethylene diisocyanate tripolymer, 0.1 weight part anhydrous dimethyl benzene, 0.1 weight part n-butyl acetate mixing solutions, form by 1 weight part A liquid and 0.7 weight part B liquid during use.
The manufacture method of wear-resisting anti-skidding urethane porch paint of the present invention, it is characterized in that 1 weight part Hydroxylated acrylic resin, 0.1～0.8 weight part polyether glycol, 0.1～0.8 weight part hydroxyl fluorocarbon acrylic acid resin, 0.01～0.1 weight part polyacrylic ester interpolymer solution, 0.01～0.1 weight part gathers methyl alkyl siloxane solution, 0.01～0.1 weight part b-[3-(2-H-benzotriazole-2-yl)-4-hydroxyl-5-tert-butyl-phenyl]-propionic acid Liquid Macrogol ester joins 0.1～1.0 dimethylbenzene, 0.1～1.0 n-butyl acetates, 0.01～0.15 mibk, 0.05 dispersing and dissolving in addition in the mixed solvent of～0.15 butanone, after the high-speed stirring 0.5, under condition of stirring, add 0.1～1.0 weight part Rutile type Titanium Dioxide, 0.01～0.5 weight part talcum powder, 0.01～0.8 weight part alumina-ceramic powder, 0.01～0.8 weight part sericite in powder, 0.01～0.6 weight part silicon powder, 0.01～0.2 weight part carbon black, 0.005～0.1 weight part aerosil, grind 0.5～1h with sand mill then, control mixture fineness is not higher than 60 μ m, makes A liquid; Form B liquid by 1 weight part hexamethylene diisocyanate tripolymer, 0.1～0.5 weight part anhydrous dimethyl benzene, 0.1～0.5 weight part n-butyl acetate mixing solutions, form by 1 weight part A liquid and 0.2～1.0 weight part B liquid during use.
The manufacture method of more excellent wear-resisting anti-skidding urethane porch paint, it is characterized in that forming by A liquid and B liquid, wherein A liquid is by 1 weight part Hydroxylated acrylic resin, 0.5 weight part polyether glycol, 0.3 weight part hydroxyl fluorocarbon acrylic acid resin, 0.05 weight part polyacrylic ester interpolymer solution, 0.06 weight part gathers methyl alkyl siloxane solution, 0.03 weight part b-[3-(2-H-benzotriazole-2-yl)-4-hydroxyl-5-tert-butyl-phenyl]-propionic acid Liquid Macrogol ester joins 1.0 weight part dimethylbenzene, 1.0 weight part n-butyl acetate, 0.1 weight part mibk, 0.1 dispersing and dissolving in addition in the mixed solvent of weight part butanone, after the high-speed stirring 0.5, under condition of stirring, add 0.3 weight part Rutile type Titanium Dioxide, 0.05 weight part talcum powder, 0.4 weight part alumina-ceramic powder, 0.2 weight part sericite in powder, 0.3 weight part silicon powder, 0.05 weight part carbon black, 0.01 weight part aerosil, grind 0.5～1h with sand mill then, control mixture fineness is not higher than 60 μ m, makes A liquid; Form B liquid by 1 weight part hexamethylene diisocyanate tripolymer, 0.1 weight part anhydrous dimethyl benzene, 0.1 weight part n-butyl acetate mixing solutions, form by 1 weight part A liquid and 0.7 weight part B liquid during use.
Wear-resisting anti-skidding urethane porch paint of the present invention and manufacture method by Hydroxylated acrylic resin, polyether glycol, hydroxyl fluorocarbon acrylic acid mixed resin solution, add that weather-proof, the wear-resisting color stuffing of a spot of auxiliary agent and some amount is formulated.In the Hydroxylated acrylic resin molecular structure that in manufacturing processed, uses a large amount of groups such as hydroxyl are arranged, with 1, the reaction of hexamethylene-diisocyanate tripolymer forms the macromolecule polymkeric substance, has good resistance to UV aging, contain a large amount of hydroxyls and ehter bond in the polymkeric substance that forms, strengthened the sticking power of coating and base material.Polyether polyol resin, the fluorine-carbon modified acrylic resin of hydroxyl are in the weathering resistance that improves paint film, can be with 1, the hexamethylene-diisocyanate tripolymer forms the rubber-like inierpeneirating network structure in film-forming, increase compactness, the weathering resistance of paint film, improved wear resistance, shock resistance and the erosion resistance of paint film.The Rutile type Titanium Dioxide that uses in the pigment, sericite in powder absorb ultraviolet trough and reach more than 85%, have protected the c h bond in the macromolecular material, thereby have improved the weathering resistance of paint film, postpone the film efflorescence variable color.The sheet structure of sericite in powder, the permeation pathway that has prolonged the ion pair paint film has improved the resistance to salt water and the salt spray resistance of paint film.Alumina-ceramic powder, the silicon powder that uses in the pigment has good performances such as good chemical stability, acid-alkali-corrosive-resisting, hardness be big, after adding alumina-ceramic powder, silicon powder in the coating, can further improve the corrodibility such as wear resistance, sea water resistance of paint film.
B-[3-(2-H-benzotriazole-2-the yl)-4-hydroxyl-5-tert-butyl-phenyl that uses]-propionic acid Liquid Macrogol ester is as ultraviolet absorbers, have light shield, absorb ultraviolet ray, quencher excited state or catch function such as free radical, can suppress UV-light the macromolecular material photodegradation.The polyacrylic ester interpolymer solution that uses improves levelling property and gloss, produces the long wave effect, and prevents the shrinkage cavity of system.Poly-methyl alkyl siloxane solution reduces the surface tension of coating system, has improved to flow and levelling property and help to eliminate bubble in the coating.The aerosil that uses helps to improve the thixotropy and the application property of coating, improves the stability in storage of coating.The different zincic acid zinc of promotor that uses can fast reaction speed, forms stable paint film.
The present invention's beneficial effect compared with prior art
1, wear-resisting anti-skidding urethane porch paint of the present invention, its coating has good sticking power, wear resistance, weathering resistance, light fastness aging, sea water resistance and salt fog resistance, wherein anti-artificial weathering test (ultraviolet resistance UVB-313) reaches 4000h, wear resistance (1000g/1000r) is not more than 30mg, it is intact that salt-fog resistant test reaches the 2000h coating, anti-synthetic sea water is not less than 720h, and anti-skid is not less than 0.9.Can be used for boats and ships, ocean platform etc. and need the anticorrosion of the deck of weather-proof, anti-skid wearable, seawater corrosion resistance and other maritime facilities steel surfaces.
2, the manufacture method of wear-resisting anti-skidding urethane porch paint of the present invention, technology is simple, need not specific installation, price is lower.
Embodiment
Embodiment 1
The manufacture method of wear-resisting anti-skidding urethane porch paint of the present invention, in stainless charging basket, add 1 weight part Hydroxylated acrylic resin earlier, 0.5 weight part polyether glycol, 0.3 weight part hydroxyl fluorocarbon acrylic acid resin, 0.05 weight part polyacrylic ester interpolymer solution, 0.06 weight part gathers methyl alkyl siloxane solution, 0.03 weight part b-[3-(2-H-benzotriazole-2-yl)-4-hydroxyl-5-tert-butyl-phenyl]-propionic acid Liquid Macrogol ester joins 1.0 weight part dimethylbenzene, 1.0 weight part n-butyl acetate, 0.1 weight part mibk, 0.1 dispersing and dissolving in addition in the mixed solvent of weight part butanone, behind the high-speed stirring 0.5h, under condition of stirring, add 0.3 weight part Rutile type Titanium Dioxide, 0.05 weight part talcum powder, 0.4 weight part alumina-ceramic powder, 0.2 weight part sericite in powder, 0.3 weight part silicon powder, 0.05 weight part carbon black, 0.01 weight part aerosil, grind 1h with sand mill then, control mixture fineness is not higher than 60 μ m, makes A liquid; Form B liquid by 1 weight part hexamethylene diisocyanate tripolymer, 0.1 weight part anhydrous dimethyl benzene, 0.1 weight part n-butyl acetate mixing solutions, form by 1 weight part A liquid and 0.7 weight part B liquid during use.
Embodiment 2
The manufacture method of wear-resisting anti-skidding urethane porch paint of the present invention, in stainless charging basket, add 1 weight part Hydroxylated acrylic resin earlier, 0.4 weight part polyether glycol, 0.2 weight part hydroxyl fluorocarbon acrylic acid resin, 0.04 weight part polyacrylic ester interpolymer solution, 0.05 weight part gathers methyl alkyl siloxane solution, 0.02 weight part b-[3-(2-H-benzotriazole-2-yl)-4-hydroxyl-5-tert-butyl-phenyl]-propionic acid Liquid Macrogol ester joins 0.8 weight part dimethylbenzene, 0.8 weight part n-butyl acetate, 0.05 weight part mibk, 0.05 dispersing and dissolving in addition in the mixed solvent of weight part butanone, behind the high-speed stirring 0.5h, under condition of stirring, add 0.2 weight part Rutile type Titanium Dioxide, 0.03 weight part talcum powder, 0.3 weight part alumina-ceramic powder, 0.2 weight part sericite in powder, 0.4 weight part silicon powder, 0.03 weight part carbon black, 0.01 weight part aerosil, grind 0.5～1h with sand mill then, control mixture fineness is not higher than 60 μ m, makes A liquid; Form B liquid by 1 weight part hexamethylene diisocyanate tripolymer, 0.15 weight part anhydrous dimethyl benzene, 0.15 weight part n-butyl acetate mixing solutions, form by 1 weight part A liquid and 0.6 weight part B liquid during use.
The raw materials used commercially available product that all adopts.
Claims (4)
1. wear-resisting anti-skidding urethane porch paint, it is characterized in that being made up of A liquid and B liquid, wherein A liquid is by weight by 1 part of Hydroxylated acrylic resin, 0.1～0.8 part of polyether glycol, 0.1～0.8 part of hydroxyl fluorocarbon acrylic acid resin, 0.1～1.0 parts of dimethylbenzene, 0.1～1.0 parts of n-butyl acetates, 0.01～0.15 part of mibk, 0.05～0.15 part of butanone, 0.1～1.0 parts of Rutile type Titanium Dioxides, 0.01～0.5 part of talcum powder, 0.01～0.8 part of alumina-ceramic powder, 0.01～0.8 part of sericite in powder, 0.01～0.6 part of silicon powder, 0.01～0.2 part of carbon black, 0.01～0.1 part of polyacrylic ester interpolymer solution, 0.01～0.1 part of poly-methyl alkyl siloxane solution, 0.01～0.1 part of b-[3-(2-H-benzotriazole-2-yl)-4-hydroxyl-5-tert-butyl-phenyl]-propionic acid Liquid Macrogol ester, 0.005～0.1 part of aerosil is formed; B liquid is made up of 1 part of hexamethylene diisocyanate tripolymer, 0.1～0.5 part of anhydrous dimethyl benzene, 0.1～0.5 part of n-butyl acetate mixing solutions by weight, is made up of 1 weight part A liquid and 0.2～1.0 weight part B liquid during use.
2. wear-resisting anti-skidding urethane porch paint according to claim 1, it is characterized in that being made up of A liquid and B liquid, wherein A liquid is by 1 weight part Hydroxylated acrylic resin, 0.5 weight part polyether glycol, 0.3 weight part hydroxyl fluorocarbon acrylic acid resin, 0.05 weight part polyacrylic ester interpolymer solution, 0.06 weight part gathers methyl alkyl siloxane solution, 0.03 weight part b-[3-(2-H-benzotriazole-2-yl)-4-hydroxyl-5-tert-butyl-phenyl]-propionic acid Liquid Macrogol ester, 1.0 weight part dimethylbenzene, 1.0 weight part n-butyl acetate, 0.1 weight part mibk, 0.1 weight part butanone, 0.3 weight part Rutile type Titanium Dioxide, 0.05 weight part talcum powder, 0.4 weight part alumina-ceramic powder, 0.2 weight part sericite in powder, 0.3 weight part silicon powder, 0.05 weight part carbon black, 0.01 the weight part aerosil is made A liquid; Form B liquid by 1 weight part hexamethylene diisocyanate tripolymer, 0.1 weight part anhydrous dimethyl benzene, 0.1 weight part n-butyl acetate mixing solutions, form by 1 weight part A liquid and 0.7 weight part B liquid during use.
3. the manufacture method of the described wear-resisting anti-skidding urethane porch paint of claim 1, it is characterized in that by weight with 1 part of Hydroxylated acrylic resin, 0.1～0.8 part of polyether glycol, 0.1～0.8 part of hydroxyl fluorocarbon acrylic acid resin, 0.01～0.1 part of polyacrylic ester interpolymer solution, 0.01～0.1 part of poly-methyl alkyl siloxane solution, 0.01～0.1 part of b-[3-(2-H-benzotriazole-2-yl)-4-hydroxyl-5-tert-butyl-phenyl]-propionic acid Liquid Macrogol ester joins 0.1～1.0 dimethylbenzene, 0.1～1.0 parts of n-butyl acetates, 0.01～0.15 part of mibk, 0.05 dispersing and dissolving in addition in the mixed solvent of～0.15 part of butanone, behind the high-speed stirring 0.5h, under condition of stirring, add 0.1～1.0 part of Rutile type Titanium Dioxide, 0.01～0.5 part of talcum powder, 0.01～0.8 part of alumina-ceramic powder, 0.01～0.8 part of sericite in powder, 0.01～0.6 part of silicon powder, 0.01～0.2 part of carbon black, 0.005～0.1 part of aerosil, grind 0.5～1h with sand mill then, control mixture fineness is not higher than 60 μ m, makes A liquid; Form B liquid by 1 weight part hexamethylene diisocyanate tripolymer, 0.1～0.5 weight part anhydrous dimethyl benzene, 0.1～0.5 weight part n-butyl acetate mixing solutions, form by 1 weight part A liquid and 0.2～1.0 weight part B liquid during use.
4. the manufacture method of wear-resisting anti-skidding urethane porch paint according to claim 3, it is characterized in that by weight with 1 part of Hydroxylated acrylic resin, 0.5 part polyether glycol, 0.3 part hydroxyl fluorocarbon acrylic acid resin, 0.05 part polyacrylic ester interpolymer solution, 0.06 part poly-methyl alkyl siloxane solution, 0.03 part b-[3-(2-H-benzotriazole-2-yl)-4-hydroxyl-5-tert-butyl-phenyl]-propionic acid Liquid Macrogol ester joins 1.0 dimethylbenzene, 1.0 n-butyl acetate, 0.1 part mibk, 0.1 dispersing and dissolving in addition in the mixed solvent of part butanone, behind the high-speed stirring 0.5h, under condition of stirring, add 0.3 part of Rutile type Titanium Dioxide, 0.05 part talcum powder, 0.4 part alumina-ceramic powder, 0.2 part sericite in powder, 0.3 part silicon powder, 0.05 part carbon black, 0.01 part aerosil, grind 0.5～1h with sand mill then, control mixture fineness is not higher than 60 μ m, makes A liquid; Form B liquid by 1 weight part hexamethylene diisocyanate tripolymer, 0.1 weight part anhydrous dimethyl benzene, 0.1 weight part n-butyl acetate mixing solutions, form by 1 weight part A liquid and 0.7 weight part B liquid during use.
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| CN 201110164091 CN102190954B (en) | 2011-06-17 | 2011-06-17 | Wear-resistant nonskid polyurethane deck paint, and manufacture method thereof |
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| CN 201110164091 CN102190954B (en) | 2011-06-17 | 2011-06-17 | Wear-resistant nonskid polyurethane deck paint, and manufacture method thereof |
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| CN102190954B CN102190954B (en) | 2012-08-15 |
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| CN103450721A (en) * | 2012-06-01 | 2013-12-18 | 天津中油渤星工程科技有限公司 | Epoxy deck paint and manufacture method thereof |
| CN103725127A (en) * | 2013-12-12 | 2014-04-16 | 青岛海洋新材料科技有限公司 | Marine climate resistant high-strength coating and preparation process thereof |
| CN103820007A (en) * | 2013-12-11 | 2014-05-28 | 青岛海洋新材料科技有限公司 | Elastic antiskid deck paint and preparation method thereof |
| CN104449335A (en) * | 2014-12-03 | 2015-03-25 | 中国石油天然气集团公司 | High-temperature, high-humidity and high-salt mist-resistant polyurethane coating and preparation method thereof |
| CN104845468A (en) * | 2015-05-15 | 2015-08-19 | 上海海悦涂料有限公司 | Hydrophilic deck finishing coat, preparation method thereof and anti-skid treatment method of deck |
| CN107974185A (en) * | 2017-12-11 | 2018-05-01 | 湖南太子化工涂料有限公司 | A kind of pavement antiskid paint and its application |
| CN112430424A (en) * | 2020-11-24 | 2021-03-02 | 厦门双瑞船舶涂料有限公司 | Antiskid wear-resistant polyurethane deck paint and preparation method thereof |
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| CN107974185A (en) * | 2017-12-11 | 2018-05-01 | 湖南太子化工涂料有限公司 | A kind of pavement antiskid paint and its application |
| CN112430424A (en) * | 2020-11-24 | 2021-03-02 | 厦门双瑞船舶涂料有限公司 | Antiskid wear-resistant polyurethane deck paint and preparation method thereof |
| CN112430424B (en) * | 2020-11-24 | 2021-11-16 | 厦门双瑞船舶涂料有限公司 | Antiskid wear-resistant polyurethane deck paint and preparation method thereof |
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| CN102190954B (en) | 2012-08-15 |
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