CN101816423A - Purple perilla seed oil lipid emulsion oral solution, beverage and manufacturing method thereof - Google Patents
Purple perilla seed oil lipid emulsion oral solution, beverage and manufacturing method thereof Download PDFInfo
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- CN101816423A CN101816423A CN201010158588A CN201010158588A CN101816423A CN 101816423 A CN101816423 A CN 101816423A CN 201010158588 A CN201010158588 A CN 201010158588A CN 201010158588 A CN201010158588 A CN 201010158588A CN 101816423 A CN101816423 A CN 101816423A
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- purple perilla
- seed oil
- perilla seed
- oral solution
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Abstract
The invention provides purple perilla seed oil lipid emulsion oral solution, a beverage and a manufacturing method thereof. The purple perilla seed oil lipid emulsion oral solution is prepared from refined purple perilla seed oil, refined lecithin, glycerin, sterile pure water, an antioxidant, a stabilizer, a pH regulator, flavorings, species and the like serving as raw materials. A manufacturing process comprises the following steps of: under the protection of nitrogen, heating the refined purple perilla seed oil and the refined lecithin to dissolve the mixture into oil phase liquid; mixing the glycerin, the antioxidant, the stabilizer, the flavorings, the spices and the sterile pure water and dissolving the solution into water phase liquid; adding the oil phase liquid into the strongly stirred water phase liquid slowly; shearing the solution to form primary emulsion at a high speed; regulating the pH value of the primary emulsion to be between 6.5 and 8.5 with a little pH regulator; emulsifying the primary emulsion with a high pressure homogenizer; filtering the solution with a microporous membrane filter; bottling and sealing the obtained solution; sterilizing the solution by microwave; and heating the solution for sterilization to obtain the purple perilla seed oil lipid emulsion oral solution which has 1 to 50 percent of the purple perilla seed oil. The purple perilla seed oil lipid emulsion oral solution is applicable to the field of healthy food; the purple perilla seed oil lipid emulsion oral solution having a high concentration of 5 to 50 percent can serve as a functionally nutritious health beverage; and the purple perilla seed oil lipid emulsion oral solution having a low concentration of 1 to 20 percent can serve as drinks for dinner and popular drinks.
Description
Technical field
The invention belongs to the healthy food field, relate to a kind of purple perilla seed oil lipid emulsion oral solution, beverage and manufacture method, this invention is by Purple Perilla Seed Oil, emulsifying agent, water after emulsification, makes oil droplet size less than below 800 nanoscales, form chylomicron, oral back enters blood circulation, directly by body or cell institute digestibility and utilization in the easier absorption of intestines and stomach.
The fat emulsion oral solution of 5-50% high concentration is as trophism functional health drink, and the fat emulsion oral solution of 1-20% low concentration is as dining table beverage and popular drink.
This purple perilla seed oil lipid emulsion oral solution, beverage are used for pregnant woman, infant, children, student, a middle-aged person, the elderly, provide with added body in essential fatty acid;
Purple perilla seed oil lipid emulsion oral solution, the research and development of beverage and production for directly drinking Purple Perilla Seed Oil, replenish essential fatty acid, and a reliable and effective method and approach are provided.
Background technology
Purple Perilla Seed Oil (Perilla Oil) is the herbal seed purple perilla seed of labiate purple perilla (Perilla frutescens L.), and cold press or hot moulding are produced, and gets Purple Perilla Seed Oil through making with extra care.
Modern science and technology studies show that, contain amounts of protein and fat in the purple perilla seed, its vegetalitas unsaturated fatty acid content 〉=90%, ω-6 linoleic acid and ω-3 linolenic acid content 〉=75%, alpha-linolenic acid is up to 65%, and in common vegetable oil, the alpha-linolenic acid content ratio is quite high.
Purple Perilla Seed Oil and the contrast of other edible oil main components
In the table as can be seen in the Purple Perilla Seed Oil polyunsaturated fatty acid reach more than 75%, its main component is an alpha-linolenic acid, content is up to more than 65%, saturated fatty acid content is minimum.
Be rich in the serial polyunsaturated fatty acid of ω-3 in the Purple Perilla Seed Oil, Main Ingredients and Appearance is an alpha-linolenic acid, belongs to essential fatty acid, can't transform synthetic, necessary additional by taking in absorption in the food at human body self.
Other edible oil main components are saturated fatty acid and monounsaturated fatty acids, and these all are non-essential fatty acids, and human body can be synthetic naturally by sugar and protein.Long-term edible these oil products, the saturated fatty acid of hyperabsorption can cause the bad reaction and the side effect of human body, then causes the shortage of interior DHA of human body and EPA, directly influences eubolism in the body, cause body biochemical metabolism confusion not normal, cause the generation of metabolic disease.As multiple diseases such as obesity, hypertension, high fat of blood, diabetes, coronary heart disease, artery sclerosis and cardiovascular and cerebrovasculars.
The three big functional mass that maintain the life normal need are EPA (eicosapentaenoic acid), DPA (clupanodonic acid), DHA (DHA).
Alpha-linolenic acid is that ω-3 is the hyle of unrighted acid, is again that ω-3 is the parent of unrighted acid, and after absorbing in human body, under the transformation of biology enzyme, by liver, but metabolism produces three big materials of needed by human:
(EPA) eicosapentaenoic acid (C20:5, ω-3) (EicosapetaenoicAcid): its major function is: the content that has improved cholesterol (HDL-C), reduce the content of bad cholesterol (LDL-C), and and the triglyceride in blood effect, reduce its molecular weight, excrete by liver, intestines, stomach, have the double effects of not only clearing up blood but also washing blood vessel;
(DPA) clupanodonic acid (C22:5, ω-3) (DocosapetaenoicAcid): it mainly acts on is the transmitting medium that forms human nerve, it acts on brain optic nerve and memory organization, can improve the transmission speed of information between brain cell, make the people react quick, the high speed channel of formation information conduction;
(DHA) DHA (C22:6, ω-3) (Docosa-HexaenoicAcid): it mainly generates the brain component, it accounts for 1/2 of total amount in the fat of brain cell constitutes, mainly concentrate on brain information interchange, thinking center and the retina, be used to drive the mass activity of brain, can slow down the brain cell aging, strengthen memory.
Alpha-linolenic acid is the basic substance that constitutes cell membrane and biology enzyme, health played a decisive role, and be indispensable in the health, generally lack again, and be badly in need of additional a kind of essential nutritional factors.When lacking alpha-linolenic acid in human body, nutrients such as vitamin, mineral matter, protein can not effectively be absorbed and be utilized, and cause nutrition leak.In our daily life, at any time, or additional frequently alpha-linolenic acid is the key that prevents nutrition leak for this reason.
U.S. FDA studies have shown that: lack alpha-linolenic acid and will cause children's brain and retinal development slow, notice can not be concentrated, and nutrition is unbalanced, can not effectively absorb nutriment, directly cause: MR, exercise not harmony, a little less than the eyesight, hyperactivity, fat, apocleisis is grown slowly more than 30 kind of symptom such as hypoimmunity and disease.
Often edible Purple Perilla Seed Oil, improve the alpha-linolenic acid intake, impel and be converted into DHA and ARA in vivo more, help and improve children's intelligence and IQ, except alpha-linolenic acid be the essential fatty acid of building brain tissue and nerve fiber, healthy development to fetus and baby's brain, retina, skin and renal function is very important, simultaneously, content of phospholipid in the Purple Perilla Seed Oil is abundant, can increase cytoactive, can improve memory and intellectual level, be important benefit brain element, also is that baby's cerebral nerve and visual performance are grown necessary nutrition.The pregnant woman, fetus and baby, should strengthen replenishing of Purple Perilla Seed Oil at the Childhood for this reason.
Have only Purple Perilla Seed Oil crude oil products and Purple Perilla Seed Oil soft capsule on the domestic market at present, Purple Perilla Seed Oil is directly taken and is difficult for absorption, or absorbs not exclusively, takes Purple Perilla Seed Oil especially in a large number or for a long time and can cause the secondary work of diarrhoea.
For this reason, this invention be Purple Perilla Seed Oil by emulsification after, particle diameter reaches below 800 nanoscales, forms chylomicron, oral back enters blood circulation, directly by body or cell institute digestibility and utilization in the easier absorption of intestines and stomach.
Purple perilla seed oil lipid emulsion oral solution, the research and development of beverage and production for directly drinking Purple Perilla Seed Oil, replenish essential fatty acid, and a reliable and effective method and approach are provided.
Summary of the invention
The object of the invention provides a kind of purple perilla seed oil lipid emulsion oral solution, beverage and manufacture method.
Purple Perilla Seed Oil (Perilla Oil) is the herbal seed purple perilla seed of labiate purple perilla (Perilla frutescens L.), and cold press or hot moulding are produced, and gets Purple Perilla Seed Oil through making with extra care.
Purple perilla seed oil lipid emulsion oral solution, beverage formula are: every 1000ml fat breast contains refining Purple Perilla Seed Oil 1-50%, emulsion 1.0-15.0%, isotonic regulator 1.0-5.0%, antioxidant 0.01-0.5%, stabilizing agent 0.1-10%, it is 6.5-8.5 that flavor enhancement 0.01-10%, pH conditioning agent are transferred fat emulsion pH, and all the other are sterile pure water.
Purple perilla seed oil lipid emulsion oral solution, drink and production process flow process are:
A) under nitrogen protection, will make with extra care Purple Perilla Seed Oil and be heated to 70-90 ℃, stir the adding emulsifying agent and form oil phase liquid until dissolving;
B) with glycerine, antioxidant, stabilizing agent, flavor enhancement, join in the aseptic pyrogen-free sterile pure water, stirring and dissolving forms water liquid;
C) under nitrogen protection, in the intensively stirred water liquid of the slow adding of oil phase liquid, strong agitation forms colostric fluid;
D), regulate the pH to 6.5-8.5 of colostric fluid with a spot of pH conditioning agent;
E) use high pressure homogenizer under the pressure of 500-25000psi, with colostrum emulsifying repeatedly, the granularity of prepared fat breast is less than 2 microns, and its average particle size range is the 20-500 nanometer;
F) with the filtration sterilization of the process of the fats emulsion behind homogeneous 0.22-0.8 micron microporous membrane filters, under aseptic GMP clean environment, quantitatively pour in the packing container (the glass bottle, mould bottle, PVC bag, non-PVC bag, mould packaging paper product and metal can packing), seal behind the inflated with nitrogen;
G) the fats emulsion goods with package encapsulation place microwave bacteria degermer sterilization or heat sterilization.
The specific embodiment
Below the present invention is described, but the present invention is limited in the example not exclusively by concrete case study on implementation.
Embodiment one,
Prescription: refining Purple Perilla Seed Oil 50g, edible lecithin 3g, edible glycerol 6g, stabilizing agent is an amount of, sweetener is an amount of, flavoring essence is an amount of, and the NaOH thin liquid is an amount of, and sterile pure water adds to 1000ml.
1, preparation oil phase liquid: get the edible refining Purple Perilla Seed Oil of formula ratio, edible lecithin, under nitrogen protection, be heated to 80 ℃ of stirrings and make that to be dissolved into oil phase liquid standby;
2, preparation water liquid: it is standby that edible glycerol, stabilizing agent, sweetener, flavoring essence and the sterile pure water of getting formula ratio is stirred into water liquid;
3, first emulsion: under nitrogen protection, under water liquid high-speed stirred, lentamente oil phase liquid is splashed into water liquid, after dripping off, use the high speed shear agitator, first emulsification 15 minutes;
4, regulate pH: under agitation, transfer pH7.4, and add sterile pure water to the full dose of filling a prescription with dilute sodium hydroxide water liquid;
5, emulsifying: utilize the high pressure homogenization machine with colostric fluid homogeneous repeatedly, adjusting pressure is 15000psi, and homogeneous 3-6 time is in the 100-400nm scope up to the newborn particle diameter of fat;
6, filter can: fats emulsion behind the filtering with microporous membrane in 0.8 μ m aperture, is poured into 600ml and moulds in the bottle, fill nitrogen, sealing;
7, sterilization: place the rotary steam Sterilization Kettle to sterilize the fats emulsion of filling and sealing, sterilized F0 value 15 minutes 30 minutes for 115 ℃.Promptly get finally 5% purple perilla seed oil lipid emulsion oral beverage products.
Embodiment two,
Prescription: refining Purple Perilla Seed Oil 300g, edible lecithin 18g, edible glycerol 30g, stabilizing agent is an amount of, sweetener is an amount of, essence is an amount of, and the NaOH thin liquid is an amount of, and sterile pure water adds to 1000ml.
1, preparation oil phase liquid: get the edible refining Purple Perilla Seed Oil of formula ratio, edible lecithin, under nitrogen protection, be heated to 80 ℃ of stirrings and make that to be dissolved into oil phase liquid standby;
2, preparation water liquid: it is standby that edible glycerol, stabilizing agent and the sterile pure water of getting formula ratio is stirred into water liquid;
3, first emulsion: under nitrogen protection, under water liquid high-speed stirred, lentamente oil phase liquid is splashed into water liquid, after dripping off, use the high speed shear agitator, first emulsification 15 minutes;
4, regulate pH: under agitation, transfer pH7.4, add sweetener, flavoring essence, and add sterile pure water to the full dose of filling a prescription with dilute sodium hydroxide water liquid;
5, emulsifying: utilize the high pressure homogenization machine with colostric fluid homogeneous repeatedly, adjusting pressure is 15000psi, and homogeneous 3-6 time is in the 100-400nm scope up to the newborn particle diameter of fat;
6, filter can: fats emulsion behind the filtering with microporous membrane in 0.8 μ m aperture, is poured in the 10ml glass bottle, fill nitrogen, sealing;
7, sterilization: the fats emulsion of filling and sealing is placed the microwave bacteria degermer sterilization, promptly get finally 30% purple perilla seed oil lipid emulsion oral solution, as trophism functional health drink.
Embodiment three,
Prescription: refining Purple Perilla Seed Oil 100g, edible lecithin 6g, edible glycerol 12g, stabilizing agent is an amount of, sweetener is an amount of, essence is an amount of, and the NaOH thin liquid is an amount of, and sterile pure water adds to 1000ml.
1, preparation oil phase liquid: get the edible refining Purple Perilla Seed Oil of formula ratio, edible lecithin, under nitrogen protection, be heated to 80 ℃ of stirrings and make that to be dissolved into oil phase liquid standby;
2, preparation water liquid: it is standby that edible glycerol, stabilizing agent, sweetener, flavoring essence and the sterile pure water of getting formula ratio is stirred into water liquid;
3, first emulsion: under nitrogen protection, under water liquid high-speed stirred, lentamente oil phase liquid is splashed into water liquid, after dripping off, use the high speed shear agitator, first emulsification 15 minutes;
4, regulate pH: under agitation, transfer pH7.4, and add sterile pure water to the full dose of filling a prescription with dilute sodium hydroxide water liquid;
5, emulsifying: utilize the high pressure homogenization machine with colostric fluid homogeneous repeatedly, adjusting pressure is 15000psi, and homogeneous 3-6 time is in the 100-400nm scope up to the newborn particle diameter of fat;
6, filter can: fats emulsion behind the filtering with microporous membrane in 0.8 μ m aperture, is poured in the 240ml metal can, fill nitrogen, sealing;
7, sterilization: place the rotary steam Sterilization Kettle to sterilize the fats emulsion of filling and sealing, sterilized F0 value 15 minutes 30 minutes for 115 ℃.Promptly get finally 10% purple perilla seed oil lipid emulsion oral beverage products.
Claims (10)
1. purple perilla seed oil lipid emulsion oral solution, beverage, it is characterized in that this prescription is: every 1000ml purple perilla seed oil lipid emulsion oral solution contains refining Purple Perilla Seed Oil 1-50%, emulsifying agent 1.0-15.0%, isotonic regulator 1.0-5.0%, antioxidant 0.01-0.5%, stabilizing agent 0.1-10%, flavor enhancement 0.01-10%, pH conditioning agent are transferred fats emulsion pH to 6.5-8.5, and all the other are sterile pure water.
2. purple perilla seed oil lipid emulsion oral solution according to claim 1, beverage, it is characterized in that described refining Purple Perilla Seed Oil (Perilla Oil) is the herbal seed purple perilla seed of labiate purple perilla (Perilla frutescens L.), press through colding pressing or the refining oily liquids that forms of hot pressing press for extracting juice extraction.
3. purple perilla seed oil lipid emulsion oral solution according to claim 1, beverage is characterized in that described emulsifying agent is a kind of or several in refined lecithin, soybean lecithin, egg yolk lecithin, poloxamer, polyethylene glycol glycerol ester, the polyoxyethylene methyl castor oil ether.
4. purple perilla seed oil lipid emulsion oral solution according to claim 1, beverage is characterized in that described isotonic regulator is a kind of or several in glycerine, sorbierite, the sweet dew alcohol and glucose.
5. purple perilla seed oil lipid emulsion oral solution according to claim 1, beverage is characterized in that described antioxidant is one or more in vitamin E, vitamin C, sodium hydrogensulfite, the natrium adetate.
6. purple perilla seed oil lipid emulsion oral solution according to claim 1, beverage is characterized in that described stabilizing agent is one or more in hydroxy propyl-Beta-cyclodextrine, polyethylene glycol, polyvinylpyrrolidone, hydroxypropyl methylcellulose, the oligomeric generation hydroxypropyl cellulose.
7. purple perilla seed oil lipid emulsion oral solution according to claim 1, beverage, it is characterized in that described pH conditioning agent is one or more mixing materials in hydrochloric acid, NaOH, phosphoric acid, phosphate, citric acid, citrate, acetic acid, the acetate, regulate purple perilla seed oil lipid emulsion oral solution pH scope at 6.5-8.5.
8. purple perilla seed oil lipid emulsion oral solution according to claim 1, beverage, it is characterized in that described flavor enhancement is sodium chloride, wood sugar, lactose, fructose, sucrose, one or more in the flavor enhancements such as A Siba is sweet, Sucralose, honey element, flavoring orange essence, lemon extract, strawberry essence, lychee flavor, fragrant burnt odor essence, flavoring pineapple essence.
9. purple perilla seed oil lipid emulsion oral solution according to claim 1, beverage is characterized in that described preparation technology is:
A) under nitrogen protection, will make with extra care Purple Perilla Seed Oil and be heated to 60-90 ℃, stir the adding emulsifying agent and form oil phase liquid until dissolving;
B) glycerine, antioxidant, stabilizing agent, flavor enhancement are joined in the sterile pure water, stirring and dissolving forms water liquid;
C) under nitrogen protection, in the intensively stirred water liquid of the slow adding of oil phase liquid, strong agitation forms colostric fluid;
D), regulate the pH to 6.5-8.5 of colostric fluid with a spot of pH conditioning agent;
E) use high pressure homogenizer under the pressure of 500-25000psi, with colostrum emulsifying repeatedly, the granularity of prepared fats emulsion is less than 2 microns, and its average particle size range is the 20-500 nanometer;
F) with the filtration sterilization of the process of the fats emulsion behind homogeneous 0.22-0.8 micron microporous membrane filters, in aseptic GMP clean environment, quantitatively pour in the packing container (the glass bottle, mould bottle, PVC bag, non-PVC bag, mould packaging paper product and metal can packing), seal behind the inflated with nitrogen;
G) the fats emulsion goods with package encapsulation place microwave bacteria degermer sterilization or heat sterilization.
10. purple perilla seed oil lipid emulsion oral solution according to claim 1, beverage, it is characterized in that being applied to the healthy food field, make the purple perilla seed oil lipid emulsion oral solution of high concentration, containing Purple Perilla Seed Oil is 5-50%, packing specification is 5-100ml, as trophism functional health drink; The purple perilla seed oil lipid emulsion oral solution of low concentration, containing Purple Perilla Seed Oil is 1-20%, packing specification is 30-5000ml, as dining table beverage and popular drink.
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Cited By (6)
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CN103330255A (en) * | 2012-11-20 | 2013-10-02 | 孙祥东 | Perillaseed health care drink and preparation method thereof |
CN105287715A (en) * | 2015-10-19 | 2016-02-03 | 南昌大学 | Perilla oil oral emulsion with lipid-lowering nutritious function and preparation method thereof |
CN110447886A (en) * | 2019-08-29 | 2019-11-15 | 吉林大学 | Purple perilla black fungus cream and manufacturing method |
CN110585266A (en) * | 2019-09-18 | 2019-12-20 | 广东润和生物科技有限公司 | Application of composition of perilla seed oil and coenzyme Q10 |
CN112715683A (en) * | 2020-12-25 | 2021-04-30 | 华南农业大学 | Preparation method of nobiletin nano emulsion based on functional grease |
CN114224836A (en) * | 2021-12-31 | 2022-03-25 | 安徽全康药业有限公司 | Preparation method of perilla seed oil mixed fat emulsion |
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CN110447886A (en) * | 2019-08-29 | 2019-11-15 | 吉林大学 | Purple perilla black fungus cream and manufacturing method |
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CN112715683A (en) * | 2020-12-25 | 2021-04-30 | 华南农业大学 | Preparation method of nobiletin nano emulsion based on functional grease |
CN114224836A (en) * | 2021-12-31 | 2022-03-25 | 安徽全康药业有限公司 | Preparation method of perilla seed oil mixed fat emulsion |
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Application publication date: 20100901 |