CA2447441A1 - Triacylglycerol based candle wax - Google Patents
Triacylglycerol based candle wax Download PDFInfo
- Publication number
- CA2447441A1 CA2447441A1 CA002447441A CA2447441A CA2447441A1 CA 2447441 A1 CA2447441 A1 CA 2447441A1 CA 002447441 A CA002447441 A CA 002447441A CA 2447441 A CA2447441 A CA 2447441A CA 2447441 A1 CA2447441 A1 CA 2447441A1
- Authority
- CA
- Canada
- Prior art keywords
- wax
- triacylglycerol
- fatty acid
- component
- partial ester
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C5/00—Candles
- C11C5/002—Ingredients
Abstract
Candles formed from triacylglycerol-based wax are provided. The wax generally has a melting point of about 130 to 145 ~F (circa 54 to 63 ~C). The wax includes a triacylglycerol component and a polyol partial ester component.
Examples of suitable polyol partial esters include fatty acid monoesters of glycerol and/or sorbitan. The triacylglycerol-based wax typically has an Iodine Value of about 20 to 40. The wax commonly includes at least about 70 wt.% of the triacylglycerol component and about 3 to 30 wt.% of the polyol partial ester component. The triacylglycerol component generally has a fatty acid composition which includes about 50 to 70 wt.% saturated fatty acids and about 30 to 45 wt.% 18:1 fatty acids. Methods of producing the candles from the vegetable oil-based wax are also provided.
Examples of suitable polyol partial esters include fatty acid monoesters of glycerol and/or sorbitan. The triacylglycerol-based wax typically has an Iodine Value of about 20 to 40. The wax commonly includes at least about 70 wt.% of the triacylglycerol component and about 3 to 30 wt.% of the polyol partial ester component. The triacylglycerol component generally has a fatty acid composition which includes about 50 to 70 wt.% saturated fatty acids and about 30 to 45 wt.% 18:1 fatty acids. Methods of producing the candles from the vegetable oil-based wax are also provided.
Claims (34)
1. A triacylglycerol-based candle wax comprising a triacylglycerol component and a polyol fatty acid partial ester component;
wherein the triacylglycerol-based wax has a melting point of about 54°C
to 63°C and an Iodine Value of about 20 to 40.
wherein the triacylglycerol-based wax has a melting point of about 54°C
to 63°C and an Iodine Value of about 20 to 40.
2. The wax of claim 1 wherein the triacylglycerol component has a fatty acid profile including about 30 to 45 wt. % 18:1 fatty acids.
3. The wax of claim 1 comprising at least about 70 wt. % of the triacylglycerol component.
4. The wax of claim 1 comprising about 3 to 30 wt. % of the polyol fatty acid partial ester component.
5. The wax of claim 1 wherein said wax contains no more than about 1.0 wt. %
free fatty acid.
free fatty acid.
6. The wax of claim 1 wherein the triacylglycerol component has an Iodine Value of about 30 to 45.
7. The wax of claim 1 wherein the triacylglycerol component has a fatty acid profile including about 50 to 65 wt. % saturated fatty acids.
8. The wax of claim 1 wherein the polyol fatty acid partial ester component has a fatty acid profile including at least about 90 wt. % fatty acids having 14 to 24 carbon atoms.
9. The wax of claim 1 wherein the polyol fatty acid partial ester component includes one or more partial esters selected from the group consisting of glycerol fatty acid partial esters and sorbitan fatty acid partial esters.
10. The wax of claim 1 wherein the polyol fatty acid partial ester component includes one or more monoesters selected from the group consisting of glycerol fatty acid monoesters, sorbitan fatty acid monoesters and mixtures thereof.
11. The wax of claim 1 wherein the polyol fatty acid partial ester component includes one or more monoesters selected from the group consisting of glycerol monostearate, glycerol monopalmitate, glycerol monooleate, sorbitan monostearate, sorbitan monopalmitate, sorbitan monooleate and mixtures thereof.
12 The wax of claim 1 wherein the polyol fatty acid partial ester component includes one or more esters selected from the group consisting of sorbitan triester of fatty acids having 16 to 18 carbon atoms.
13. The wax of claim 1 wherein the polyol fatty acid partial ester component has an Iodine Value of no more than about 10.
14. The wax of claim 1 wherein the triacylglycerol component has a fatty acid profile including about 8 to 12 wt. % 16:0 fatty acid, about 40 to 45 wt. % 18:1 fatty acids and about 40 to 45 wt. % 18:0 fatty acid.
15. The wax of claim 1 wherein the triacylglycerol component has a fatty acid profile including about 20 to 25 wt. % 16:0 fatty acid; about 40 to 45 wt. % 18:1 fatty acids and about 30 to 35 wt. % 18:0 fatty acid.
16. The wax of claim 1 wherein the triacylglycerol component includes hydrogenated soybean oil, hydrogenated cottonseed oil, hydrogenated sunflower oil, hydrogenated canola oil, hydrogenated corn oil, hydrogenated palm oil, hydrogenated olive oil, hydrogenated peanut oil, hydrogenated safflower oil or a mixture thereof.
17. The wax of claim 1 further comprising a fragrance oil.
18. The wax of claim 1 further comprising a colorant.
19. The wax of claim 1 further comprising a migration inhibitor.
20. The wax of claim 19 wherein the migration inhibitor includes a polymer formed from polymerization of alpha olefins having at least 10 carbon atoms.
21. A triacylglycerol-based candle wax comprising a triacylglycerol component and a polyol fatty acid partial ester component;
wherein the wax has a melting point of about 54°C to 63°C; and the triacylglycerol component has a fatty acid profile including about 50 to 70 wt. %
saturated fatty acids.
wherein the wax has a melting point of about 54°C to 63°C; and the triacylglycerol component has a fatty acid profile including about 50 to 70 wt. %
saturated fatty acids.
22. The wax of claim 21 wherein the triacylglycerol-based wax has an Iodine Value of about 25 to 35.
23. The wax of claim 21 wherein the triacylglycerol component has a fatty acid profile including about 30 to 45 wt. % 18:1 fatty acids.
24. The wax of claim 21 wherein the triacylglycerol component has an Iodine Value of about 30 to 40.
25. A triacylglycerol-based candle wax comprising a triacylglycerol component and a polyol fatty acid partial ester component;
wherein the triacylglycerol-based wax has a melting point of about 54°C
to 63°C; and the triacylglycerol component has a fatty acid profile including about 30 to 45 wt. % 18:1 fatty acids.
wherein the triacylglycerol-based wax has a melting point of about 54°C
to 63°C; and the triacylglycerol component has a fatty acid profile including about 30 to 45 wt. % 18:1 fatty acids.
26. The wax of claim 25 wherein the triacylglycerol component has a fatty acid profile including about 50 to 65 wt. % saturated fatty acids.
27. The wax of claim 25 wherein the triacylglycerol-based wax has an Iodine Value of about 25 to 35.
28. A candle comprising a wick and a triacylglycerol-based wax;
wherein the triacylglycerol-based wax comprises a triacylglycerol component and a polyol fatty acid partial ester component;
wherein the triacylglycerol-based wax has a melting point of about 54°C
to 63°C; and the triacylglycerol component has a fatty acid profile including about 50 to 70 wt. % saturated fatty acids.
wherein the triacylglycerol-based wax comprises a triacylglycerol component and a polyol fatty acid partial ester component;
wherein the triacylglycerol-based wax has a melting point of about 54°C
to 63°C; and the triacylglycerol component has a fatty acid profile including about 50 to 70 wt. % saturated fatty acids.
29. A candle comprising a wick and a triacylglycerol-based wax;
wherein the triacylglycerol-based wax comprises a triacylglycerol component and a polyol fatty acid partial ester component; and the triacylglycerol-based wax has a melting point of about 54°C to 63°C and an Iodine Value of about 20 to 40.
wherein the triacylglycerol-based wax comprises a triacylglycerol component and a polyol fatty acid partial ester component; and the triacylglycerol-based wax has a melting point of about 54°C to 63°C and an Iodine Value of about 20 to 40.
30. A candle comprising a wick and a triacylglycerol-based wax;
wherein the triacylglycerol-based wax comprises a triacylglycerol component and a polyol fatty acid partial ester component; and the triacylglycerol-based wax has a melting point of about 54°C to 63°C;
and the triacylglycerol component has a fatty acid profile including about 30 to 45 wt. % 18:1 fatty acids.
wherein the triacylglycerol-based wax comprises a triacylglycerol component and a polyol fatty acid partial ester component; and the triacylglycerol-based wax has a melting point of about 54°C to 63°C;
and the triacylglycerol component has a fatty acid profile including about 30 to 45 wt. % 18:1 fatty acids.
31. A method of producing a candle comprising:
heating a triacylglycerol-based wax to a molten state;
introducing the molten triacylglycerol-based wax into a mold which includes a wick disposed therein; and solidifying the molten triacylglycerol-based wax in the mold; and removing the solidified triacylglycerol-based wax from the mold;
wherein the triacylglycerol-based wax comprises a triacylglycerol component and a polyol fatty acid partial ester component; and the triacylglycerol-based wax has a melting point of about 54°C to 63°C and an Iodine Value of about 20 to 40.
heating a triacylglycerol-based wax to a molten state;
introducing the molten triacylglycerol-based wax into a mold which includes a wick disposed therein; and solidifying the molten triacylglycerol-based wax in the mold; and removing the solidified triacylglycerol-based wax from the mold;
wherein the triacylglycerol-based wax comprises a triacylglycerol component and a polyol fatty acid partial ester component; and the triacylglycerol-based wax has a melting point of about 54°C to 63°C and an Iodine Value of about 20 to 40.
32. A triacylglycerol-based candle wax comprising at least about 80 wt.
% of a triacylglycerol component and about 3 to 15 wt. % of a glycerol fatty acid monoester component;
wherein the triacylglycerol-based wax has a melting point of about 54°C
to 63°C, an Iodine Value of about 20 to 40 and contains no more than about 1.0 wt.
free fatty acid; and the triacylglycerol component has a fatty acid profile including about 50 to 65 wt. % saturated fatty acids and about 30 to 45 wt. % 18:1 fatty acids.
% of a triacylglycerol component and about 3 to 15 wt. % of a glycerol fatty acid monoester component;
wherein the triacylglycerol-based wax has a melting point of about 54°C
to 63°C, an Iodine Value of about 20 to 40 and contains no more than about 1.0 wt.
free fatty acid; and the triacylglycerol component has a fatty acid profile including about 50 to 65 wt. % saturated fatty acids and about 30 to 45 wt. % 18:1 fatty acids.
33. The wax of claim 32 wherein a glycerol fatty acid monoester has an Iodine Value of no more than about 10 and includes glycerol monostearate, glycerol monopalmitate or a mixture thereof.
34. The wax of claim 32 comprising about 85 to 95 wt. % of the triacylglycerol component and about 5 to 15 wt. % of the glycerol fatty acid monoester component;
wherein the wax has an Iodine Value of about 25 to 30; and the triacylglycerol component has a fatty acid profile including about 30 to 35 wt. % 18:1 fatty acids and about 60 to 65 wt. % saturated fatty acids.
wherein the wax has an Iodine Value of about 25 to 30; and the triacylglycerol component has a fatty acid profile including about 30 to 35 wt. % 18:1 fatty acids and about 60 to 65 wt. % saturated fatty acids.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US09/854,138 | 2001-05-11 | ||
US09/854,138 US6503285B1 (en) | 2001-05-11 | 2001-05-11 | Triacylglycerol based candle wax |
PCT/US2002/015079 WO2002092736A1 (en) | 2001-05-11 | 2002-05-10 | Triacylglycerol based candle wax |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2447441A1 true CA2447441A1 (en) | 2002-11-21 |
CA2447441C CA2447441C (en) | 2010-04-20 |
Family
ID=25317835
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA2447441A Expired - Lifetime CA2447441C (en) | 2001-05-11 | 2002-05-10 | Triacylglycerol based candle wax |
Country Status (6)
Country | Link |
---|---|
US (4) | US6503285B1 (en) |
EP (1) | EP1390460B1 (en) |
AT (1) | ATE478129T1 (en) |
CA (1) | CA2447441C (en) |
DE (1) | DE60237358D1 (en) |
WO (1) | WO2002092736A1 (en) |
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2001
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-
2002
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- 2002-05-10 DE DE60237358T patent/DE60237358D1/de not_active Expired - Lifetime
- 2002-05-10 AT AT02725998T patent/ATE478129T1/en not_active IP Right Cessation
- 2002-05-10 EP EP02725998A patent/EP1390460B1/en not_active Expired - Lifetime
- 2002-05-10 CA CA2447441A patent/CA2447441C/en not_active Expired - Lifetime
- 2002-10-30 US US10/284,272 patent/US6770104B2/en not_active Expired - Lifetime
-
2004
- 2004-06-08 US US10/863,662 patent/US7462205B2/en not_active Expired - Lifetime
-
2008
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102525829A (en) * | 2006-03-07 | 2012-07-04 | 埃莱文斯可更新科学公司 | Compositions comprising metathesized unsaturated polyol esters |
CN102525829B (en) * | 2006-03-07 | 2014-08-06 | 埃莱文斯可更新科学公司 | Compositions comprising metathesized unsaturated polyol esters |
US9668955B2 (en) | 2006-03-07 | 2017-06-06 | Elevance Renewable Sciences, Inc. | Compositions comprising metathesized unsaturated polyol esters |
Also Published As
Publication number | Publication date |
---|---|
US6503285B1 (en) | 2003-01-07 |
DE60237358D1 (en) | 2010-09-30 |
EP1390460B1 (en) | 2010-08-18 |
EP1390460A4 (en) | 2004-10-20 |
US8070833B2 (en) | 2011-12-06 |
US20040221504A1 (en) | 2004-11-11 |
US7462205B2 (en) | 2008-12-09 |
US20090119977A1 (en) | 2009-05-14 |
US6770104B2 (en) | 2004-08-03 |
ATE478129T1 (en) | 2010-09-15 |
EP1390460A1 (en) | 2004-02-25 |
CA2447441C (en) | 2010-04-20 |
US20030110683A1 (en) | 2003-06-19 |
WO2002092736A1 (en) | 2002-11-21 |
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