CA2381301A1 - Process for the preparation of quasi-crystalline boehmites - Google Patents
Process for the preparation of quasi-crystalline boehmites Download PDFInfo
- Publication number
- CA2381301A1 CA2381301A1 CA002381301A CA2381301A CA2381301A1 CA 2381301 A1 CA2381301 A1 CA 2381301A1 CA 002381301 A CA002381301 A CA 002381301A CA 2381301 A CA2381301 A CA 2381301A CA 2381301 A1 CA2381301 A1 CA 2381301A1
- Authority
- CA
- Canada
- Prior art keywords
- quasi
- preparation
- crystalline
- additives
- crystalline boehmite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/30—Preparation of aluminium oxide or hydroxide by thermal decomposition or by hydrolysis or oxidation of aluminium compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/44—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water
- C01F7/447—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water by wet processes
- C01F7/448—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water by wet processes using superatmospheric pressure, e.g. hydrothermal conversion of gibbsite into boehmite
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
- B01J21/04—Alumina
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/34—Preparation of aluminium hydroxide by precipitation from solutions containing aluminium salts
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/34—Preparation of aluminium hydroxide by precipitation from solutions containing aluminium salts
- C01F7/36—Preparation of aluminium hydroxide by precipitation from solutions containing aluminium salts from organic aluminium salts
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/021—After-treatment of oxides or hydroxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/04—Compounds with a limited amount of crystallinty, e.g. as indicated by a crystallinity index
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
Abstract
The present invention pertains to an improved process for the preparation of quasi-crystalline boehmite. In this improved process a quasi-crystalline boehmite precursor is aged at a pH below 7, preferably under hydrothermal conditions. It was found that when conducting the preparation processes for quasi-crystalline aluminas described in the prior art at a pH below 7 and under hydrothermal conditions instead of the high pH and thermal ageing used in the prior art, QCBs with higher crystallinity are obtained. In the process according to the invention additives may be added to the quasi-crystalline boehmite precursor. This results in a high quality QCB with additives in a homogeneously dispersed state.
Suitable additives are compounds containing elements selected from the group of rare earth metals, alkaline earth metals, transition metals, actinides, silicon, gallium, boron, and phosphorus.
Suitable additives are compounds containing elements selected from the group of rare earth metals, alkaline earth metals, transition metals, actinides, silicon, gallium, boron, and phosphorus.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US37255799A | 1999-08-11 | 1999-08-11 | |
US09/372,557 | 1999-08-11 | ||
PCT/EP2000/007792 WO2001012554A1 (en) | 1999-08-11 | 2000-08-11 | Process for the preparation of quasi-crystalline boehmites |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2381301A1 true CA2381301A1 (en) | 2001-02-22 |
CA2381301C CA2381301C (en) | 2009-01-20 |
Family
ID=23468656
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002381301A Expired - Fee Related CA2381301C (en) | 1999-08-11 | 2000-08-11 | Process for the preparation of quasi-crystalline boehmites |
Country Status (12)
Country | Link |
---|---|
US (1) | US6506358B1 (en) |
EP (1) | EP1200350B1 (en) |
JP (1) | JP2003507299A (en) |
KR (1) | KR100711342B1 (en) |
CN (1) | CN1174922C (en) |
AT (1) | ATE280738T1 (en) |
BR (1) | BR0013135A (en) |
CA (1) | CA2381301C (en) |
DE (1) | DE60015345T2 (en) |
ES (1) | ES2231252T3 (en) |
PT (1) | PT1200350E (en) |
WO (1) | WO2001012554A1 (en) |
Families Citing this family (30)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7208446B2 (en) * | 1999-08-11 | 2007-04-24 | Albemarle Netherlands B. V. | Quasi-crystalline boehmites containing additives |
WO2001012553A1 (en) * | 1999-08-11 | 2001-02-22 | Akzo Nobel N.V. | Process for the preparation of quasi-crystalline boehmites from inexpensive precursors |
US20030180214A1 (en) * | 1999-08-11 | 2003-09-25 | Dennis Stamires | Process for the preparation of quasi-crystalline boehmites |
JP4909497B2 (en) * | 2001-05-10 | 2012-04-04 | アルベマーレ ネザーランズ ビー.ブイ. | Continuous process and equipment for efficient conversion of inorganic solid particles |
US7090824B2 (en) * | 2001-07-27 | 2006-08-15 | Board Of Trustees Of Michigan State University | Mesostructured transition aluminas |
US20050124745A1 (en) * | 2002-04-19 | 2005-06-09 | Saint-Gobain Ceramics & Plastics, Inc. | Flame retardant composites |
US20050227000A1 (en) * | 2004-04-13 | 2005-10-13 | Saint-Gobain Ceramics & Plastics, Inc. | Surface coating solution |
CN1156336C (en) * | 2002-07-12 | 2004-07-07 | 清华大学 | Preparation method of titanium dioxide film photocatalyst loaded on surface of flexible base material |
RU2336935C2 (en) * | 2002-08-13 | 2008-10-27 | Интеркэт, Инк. | Treatment of smoke gases for reduction of nox and co exhausts |
US6964934B2 (en) | 2002-08-28 | 2005-11-15 | Albemarle Netherlands B.V. | Process for the preparation of doped pentasil-type zeolite using doped seeds |
US6969692B2 (en) | 2002-08-28 | 2005-11-29 | Albemarle Netherlands B.V. | Process for the preparation of doped pentasil-type zeolites using a doped reactant |
JP4614354B2 (en) * | 2003-03-10 | 2011-01-19 | 河合石灰工業株式会社 | Heat resistant aluminum hydroxide and method for producing the same |
WO2005051845A2 (en) | 2003-11-26 | 2005-06-09 | Albemarle Netherlands B.V. | Hydrothermal process for the preparation of quasi-crystalline boehmite |
US7431825B2 (en) * | 2003-12-05 | 2008-10-07 | Intercat, Inc. | Gasoline sulfur reduction using hydrotalcite like compounds |
DE102004018336A1 (en) * | 2004-04-15 | 2005-11-10 | Albemarle Corporation | Flame retardant filler for plastics |
TWI342335B (en) * | 2004-06-02 | 2011-05-21 | Intercat Inc | Mixed metal oxide additives |
US20060104895A1 (en) | 2004-11-18 | 2006-05-18 | Saint-Gobain Ceramics & Plastics, Inc. | Transitional alumina particulate materials having controlled morphology and processing for forming same |
DE102006012268A1 (en) * | 2006-03-15 | 2007-09-27 | Nabaltec Ag | Fine crystalline boehmite and process for its preparation |
KR100885309B1 (en) * | 2007-08-24 | 2009-02-24 | 한국화학연구원 | Manufacturing method of high porous alo(oh) gel |
CN101827651B (en) * | 2007-08-29 | 2015-06-10 | 太平洋工业发展公司 | Rare earth alumina particulate manufacturing method and application |
EP2231523A2 (en) * | 2007-12-19 | 2010-09-29 | Saint-Gobain Ceramics & Plastics, Inc. | Aggregates of alumina hydrates |
US8460768B2 (en) | 2008-12-17 | 2013-06-11 | Saint-Gobain Ceramics & Plastics, Inc. | Applications of shaped nano alumina hydrate in inkjet paper |
CA2793668A1 (en) | 2011-10-31 | 2013-04-30 | Bradley J. Crosby | An apparatus and method for construction of structures utilizing insulated concrete forms |
USD713975S1 (en) | 2012-07-30 | 2014-09-23 | Airlite Plastics Co. | Insulative insert for insulated concrete form |
WO2014073228A1 (en) * | 2012-11-06 | 2014-05-15 | 河合石灰工業株式会社 | High thermal conductive boehmite and method for manufacturing same |
US10787827B2 (en) | 2016-11-14 | 2020-09-29 | Airlite Plastics Co. | Concrete form with removable sidewall |
EP3723900A1 (en) | 2017-12-11 | 2020-10-21 | BASF Corporation | Reactive silica-alumina matrix component compositions for bottoms cracking catalysts |
CA3061942A1 (en) | 2018-11-19 | 2020-05-19 | Bradley J. Crosby | Concrete form with removable sidewall |
WO2022155523A1 (en) | 2021-01-15 | 2022-07-21 | Albemarle Corporation | Pseudo solid state crystallization of zeolites and uses therein |
CN116081668B (en) * | 2023-03-06 | 2023-07-25 | 成都超纯应用材料有限责任公司 | Boehmite sol dispersing agent, preparation method and application thereof |
Family Cites Families (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3357791A (en) | 1964-07-20 | 1967-12-12 | Continental Oil Co | Process for producing colloidal-size particles of alumina monohydrate |
US3739062A (en) * | 1970-10-05 | 1973-06-12 | Kaiser Aluminium Chem Corp | Direct conversion of dawsonite to pseudoboehmite |
US4089811A (en) * | 1976-11-01 | 1978-05-16 | Texaco Inc. | Preparation of catalyst support |
US4117105A (en) | 1977-03-21 | 1978-09-26 | Pq Corporation | Process for preparing dispersible boehmite alumina |
JPS5442399A (en) * | 1977-09-10 | 1979-04-04 | Mizusawa Industrial Chem | Superfine powdery hydrated alumina and its manufacturing method |
JPS5527830A (en) * | 1978-08-15 | 1980-02-28 | Chiyoda Chem Eng & Constr Co Ltd | Production of alumina carrier |
FR2449650A1 (en) * | 1979-02-26 | 1980-09-19 | Rhone Poulenc Ind | PROCESS FOR THE PREPARATION OF ALUMINUM AT LEAST PARTIALLY IN THE FORM OF ULTRA-FINE BOEHMITE |
US4318896A (en) * | 1980-04-14 | 1982-03-09 | Uop Inc. | Manufacture of alumina particles |
US4332782A (en) * | 1980-07-28 | 1982-06-01 | Filtrol Corporation | Method of producing pseudoboehmite |
DE3243193A1 (en) * | 1982-11-23 | 1984-05-30 | Degussa Ag, 6000 Frankfurt | WATER-BASED ALUMINUM OXIDE, CONTAINING IN ESSENTIAL PSEUDOBOEHMIT, METHOD FOR THE PRODUCTION AND USE THEREOF |
EP0130835B1 (en) * | 1983-07-01 | 1990-05-02 | Hitachi, Ltd. | High temperature stable catalyst, process for preparing same and process for conducting chemical reaction using same |
JPS6022929A (en) * | 1983-07-15 | 1985-02-05 | Hitachi Ltd | Heat resistant carrier for catalyst |
US5194243A (en) | 1983-09-22 | 1993-03-16 | Aluminum Company Of America | Production of aluminum compound |
US4676928A (en) * | 1986-01-30 | 1987-06-30 | Vista Chemical Company | Process for producing water dispersible alumina |
US4797139A (en) | 1987-08-11 | 1989-01-10 | Norton Company | Boehmite produced by a seeded hydyothermal process and ceramic bodies produced therefrom |
US5837634A (en) * | 1992-11-12 | 1998-11-17 | Condea Vista Company | Process for producing stabilized alumina having enhanced resistance to loss of surface area at high temperatures |
FR2697832B1 (en) | 1992-11-12 | 1994-12-30 | Rhone Poulenc Chimie | Alumina stabilized by lanthanum and its preparation process. |
JPH08268716A (en) * | 1995-03-30 | 1996-10-15 | Japan Energy Corp | Method for controlling particle diameter of pseudo-boehmite powder |
JP3847862B2 (en) * | 1996-10-04 | 2006-11-22 | 株式会社ジャパンエナジー | Pseudoboehmite for catalyst support and method for producing the same |
US6027706A (en) * | 1998-05-05 | 2000-02-22 | Board Of Trustees Operating Michigan State University | Porous aluminum oxide materials prepared by non-ionic surfactant assembly route |
-
2000
- 2000-08-11 US US09/636,694 patent/US6506358B1/en not_active Expired - Fee Related
- 2000-08-11 EP EP20000960436 patent/EP1200350B1/en not_active Revoked
- 2000-08-11 DE DE60015345T patent/DE60015345T2/en not_active Revoked
- 2000-08-11 AT AT00960436T patent/ATE280738T1/en not_active IP Right Cessation
- 2000-08-11 CN CNB00811448XA patent/CN1174922C/en not_active Expired - Fee Related
- 2000-08-11 JP JP2001516859A patent/JP2003507299A/en active Pending
- 2000-08-11 WO PCT/EP2000/007792 patent/WO2001012554A1/en active IP Right Grant
- 2000-08-11 CA CA002381301A patent/CA2381301C/en not_active Expired - Fee Related
- 2000-08-11 ES ES00960436T patent/ES2231252T3/en not_active Expired - Lifetime
- 2000-08-11 PT PT00960436T patent/PT1200350E/en unknown
- 2000-08-11 BR BR0013135-0A patent/BR0013135A/en not_active Application Discontinuation
- 2000-08-11 KR KR1020027001567A patent/KR100711342B1/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
BR0013135A (en) | 2002-04-30 |
PT1200350E (en) | 2005-03-31 |
DE60015345D1 (en) | 2004-12-02 |
EP1200350A1 (en) | 2002-05-02 |
EP1200350B1 (en) | 2004-10-27 |
ES2231252T3 (en) | 2005-05-16 |
DE60015345T2 (en) | 2005-10-20 |
JP2003507299A (en) | 2003-02-25 |
CN1174922C (en) | 2004-11-10 |
KR100711342B1 (en) | 2007-04-27 |
WO2001012554A1 (en) | 2001-02-22 |
CN1368938A (en) | 2002-09-11 |
KR20020026563A (en) | 2002-04-10 |
CA2381301C (en) | 2009-01-20 |
US6506358B1 (en) | 2003-01-14 |
ATE280738T1 (en) | 2004-11-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
EEER | Examination request | ||
MKLA | Lapsed |