CA2065548A1 - Two-stage dilute acid prehydrolysis of biomass - Google Patents
Two-stage dilute acid prehydrolysis of biomassInfo
- Publication number
- CA2065548A1 CA2065548A1 CA002065548A CA2065548A CA2065548A1 CA 2065548 A1 CA2065548 A1 CA 2065548A1 CA 002065548 A CA002065548 A CA 002065548A CA 2065548 A CA2065548 A CA 2065548A CA 2065548 A1 CA2065548 A1 CA 2065548A1
- Authority
- CA
- Canada
- Prior art keywords
- xylan
- hydrolyzable
- dilute acid
- biomass
- xylose
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/002—Xylose
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
A two-stage dilute acid prehydrolysis process on xylan containing hemicellulose in biomass is effected by: treating feedstock of hemicellulosic material comprising xylan that is slow hydrolyzable and xylan that is fast hydrolyzable under predetermined low temperature conditions with a dilute acid for a residence time sufficient to hydrolyze the fast hydrolyzable xylan to xylose; removing said xylose from said fast hydrolyzable xylan and leaving a residue; and treating said residue having a slow hydrolyzable xylan with a dilute acid under predetermined high temperature conditions for a residence time required to hydrolyze said slow hydrolyzable xylan to xylose.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US681,299 | 1991-04-08 | ||
US07/681,299 US5125977A (en) | 1991-04-08 | 1991-04-08 | Two-stage dilute acid prehydrolysis of biomass |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2065548A1 true CA2065548A1 (en) | 1992-10-09 |
CA2065548C CA2065548C (en) | 2002-02-26 |
Family
ID=24734685
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002065548A Expired - Fee Related CA2065548C (en) | 1991-04-08 | 1992-04-07 | Two-stage dilute acid prehydrolysis of biomass |
Country Status (2)
Country | Link |
---|---|
US (1) | US5125977A (en) |
CA (1) | CA2065548C (en) |
Families Citing this family (50)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5411594A (en) * | 1991-07-08 | 1995-05-02 | Brelsford; Donald L. | Bei hydrolysis process system an improved process for the continuous hydrolysis saccharification of ligno-cellulosics in a two-stage plug-flow-reactor system |
US5424417A (en) * | 1993-09-24 | 1995-06-13 | Midwest Research Institute | Prehydrolysis of lignocellulose |
US5874263A (en) * | 1996-07-31 | 1999-02-23 | The Texas A&M University System | Method and apparatus for producing organic acids |
DE19637909A1 (en) * | 1996-09-18 | 1998-03-19 | Infan Ingenieurgesellschaft Fu | Scrap wood processing by multistage chemical decomposition, saccharification and fermentation |
US6228177B1 (en) | 1996-09-30 | 2001-05-08 | Midwest Research Institute | Aqueous fractionation of biomass based on novel carbohydrate hydrolysis kinetics |
US6022419A (en) * | 1996-09-30 | 2000-02-08 | Midwest Research Institute | Hydrolysis and fractionation of lignocellulosic biomass |
US5814292A (en) * | 1996-12-19 | 1998-09-29 | Energy Research Group | Comprehensive energy producing methods for aqueous phase oxidation |
US6589760B1 (en) | 1999-02-10 | 2003-07-08 | Eastman Chemical Company | Methods of separating a corn fiber lipid fraction from corn fiber |
US6419788B1 (en) | 2000-08-16 | 2002-07-16 | Purevision Technology, Inc. | Method of treating lignocellulosic biomass to produce cellulose |
US7604967B2 (en) * | 2003-03-19 | 2009-10-20 | The Trustees Of Dartmouth College | Lignin-blocking treatment of biomass and uses thereof |
US8580541B2 (en) * | 2003-03-19 | 2013-11-12 | The Trustees Of Dartmouth College | Lignin blockers and uses thereof |
US7812153B2 (en) * | 2004-03-11 | 2010-10-12 | Rayonier Products And Financial Services Company | Process for manufacturing high purity xylose |
AT504715B1 (en) * | 2004-07-16 | 2010-07-15 | Andritz Ag Maschf | METHOD FOR RESOLVING MELIUS-SUBSTANTIAL PAPER |
DK176540B1 (en) | 2004-09-24 | 2008-07-21 | Cambi Bioethanol Aps | Process for the treatment of biomass and organic waste in order to extract desired biologically based products |
BR122014013416B1 (en) | 2005-07-19 | 2018-03-06 | Inbicon A/S | METHOD FOR CONVERSION OF A RAW MATERIAL OF A CELLULOSIS MATERIAL, THE CELLULOSIS MATERIAL UNDERSTANDING AT LEAST CELLULOSE, HEMICELLULOSIS AND ASH, IN WHICH THE CELLULOSTIC MATERIAL IS SUBMITTED TO THE PRE-CULTURE OF THE CURSION CHEMICALS, WHICH MUST BE RECOVERED, AND IN WHICH A NET FRACTION AND A SOLID FIBER FRACTION ARE PRODUCED, THE SOLID FIBER FRACTION SUBMITTED TO ENZYMATIC LIQUIDATION |
CA2631021A1 (en) * | 2005-11-23 | 2007-10-25 | Natureworks Llc | Process for fractionating lignocellulosic biomass into liquid and solid products |
US20110003352A1 (en) * | 2006-04-28 | 2011-01-06 | American Process, Inc. | process for the stepwise treatment of lignocellulosic material to produce reactive chemical feedstocks |
NZ575879A (en) * | 2006-09-01 | 2012-09-28 | Ra Energy Corp | Advanced biorefinery process |
US7815741B2 (en) | 2006-11-03 | 2010-10-19 | Olson David A | Reactor pump for catalyzed hydrolytic splitting of cellulose |
US7815876B2 (en) | 2006-11-03 | 2010-10-19 | Olson David A | Reactor pump for catalyzed hydrolytic splitting of cellulose |
FI121885B (en) * | 2007-11-09 | 2011-05-31 | Chempolis Oy | A process for making a sugar product |
BRPI0915290A2 (en) * | 2008-05-22 | 2016-02-16 | Ted C Lewis | cellulose biomass processing plant and process for treating cellulosic biomass raw material |
US8546560B2 (en) * | 2008-07-16 | 2013-10-01 | Renmatix, Inc. | Solvo-thermal hydrolysis of cellulose |
EP3778717A1 (en) * | 2008-07-16 | 2021-02-17 | Renmatix Inc. | Nano-catalytic-solvo-thermal technology platform bio-refineries |
BRPI0923405B1 (en) | 2008-12-17 | 2018-07-17 | Borregaard As | lignocellulosic biomass conversion. |
EP2403954B1 (en) * | 2009-03-03 | 2015-04-22 | POET Research, Inc. | Method for fermentation of biomass for the production of ethanol |
US7915474B2 (en) * | 2009-04-01 | 2011-03-29 | Earth Renewal Group, Llc | Aqueous phase oxidation process |
US8115047B2 (en) * | 2009-04-01 | 2012-02-14 | Earth Renewal Group, Llc | Aqueous phase oxidation process |
US8481800B2 (en) * | 2009-04-01 | 2013-07-09 | Earth Renewal Group, Llc | Aqueous phase oxidation process |
US7951988B2 (en) * | 2009-04-01 | 2011-05-31 | Earth Renewal Group, Llc | Aqueous phase oxidation process |
US9272936B2 (en) | 2009-04-01 | 2016-03-01 | Earth Renewal Group, Llc | Waste treatment process |
US8168847B2 (en) * | 2009-04-01 | 2012-05-01 | Earth Renewal Group, Llc | Aqueous phase oxidation process |
US8246828B2 (en) | 2009-08-04 | 2012-08-21 | Geosynfuels, Llc | Methods for selectively producing hydrogen and methane from biomass feedstocks using an anaerobic biological system |
CN105525043B (en) | 2010-01-19 | 2021-03-19 | 瑞恩麦特克斯股份有限公司 | Production of fermentable sugars and lignin from biomass using supercritical fluids |
WO2011116320A1 (en) | 2010-03-19 | 2011-09-22 | Poet Research, Inc. | System for treatment of biomass to facilitate the production of ethanol |
CA2795501C (en) | 2010-03-19 | 2019-02-26 | Poet Research, Inc. | System for the treatment of biomass |
CA2824993C (en) | 2011-01-18 | 2019-07-23 | Poet Research, Inc. | Systems and methods for hydrolysis of biomass |
BR112013024925A2 (en) | 2011-04-01 | 2016-12-20 | Univ Limerick | lignocellulose processing |
WO2012151521A2 (en) | 2011-05-04 | 2012-11-08 | Renmatix, Inc. | Multistage cellulose hydrolysis and quench with or without acid |
SG194702A1 (en) | 2011-05-04 | 2013-12-30 | Renmatix Inc | Cellulose hydrolysis with ph adjustment |
US8801859B2 (en) | 2011-05-04 | 2014-08-12 | Renmatix, Inc. | Self-cleaning apparatus and method for thick slurry pressure control |
RU2602068C2 (en) | 2011-05-04 | 2016-11-10 | Ренмэтикс, Инк. | Producing lignin from lignocellulose biomass |
CN103842524A (en) * | 2011-07-07 | 2014-06-04 | 波特研究公司 | Systems and methods for acid recycle |
US8759498B2 (en) | 2011-12-30 | 2014-06-24 | Renmatix, Inc. | Compositions comprising lignin |
BR102013006389A2 (en) | 2012-08-01 | 2015-03-17 | Cnpem Ct Nac De Pesquisa Em En E Materiais | Process for simultaneous conversion of sugarcane bagasse using uhtst reactors |
BR112016002565A2 (en) * | 2013-08-06 | 2017-08-01 | Praj Industries Ltd | ethanol preparation from lignocellulosic materials |
CA2962611A1 (en) | 2014-09-26 | 2016-03-31 | Renmatix, Inc. | Adhesive compositions comprising type-ii cellulose |
EP3176320A1 (en) | 2015-12-03 | 2017-06-07 | Valmet AB | Process to produce a bio-product |
CN108118103A (en) * | 2017-12-20 | 2018-06-05 | 南京林业大学 | The method that a kind of iron ion-acetic acid catalysis directionally hydrolyzing hemicellulose produces xylose |
CN111321182A (en) * | 2020-04-03 | 2020-06-23 | 安徽安生生物化工科技有限责任公司 | Pretreatment method for solid acidolysis of straw |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1190953A (en) * | 1914-09-02 | 1916-07-11 | Raemer Rex Renshaw | Process for making fodder. |
US3132051A (en) * | 1960-06-09 | 1964-05-05 | Ledoga Spa | Continuous process for extracting pentoses from substances containing hemicelluloses |
IT1025544B (en) * | 1973-11-23 | 1978-08-30 | Sued Chemie Ag | PROCESS FOR BREAKING DOWN WOOD OF DAISIES |
BE825980A (en) * | 1974-02-26 | 1975-08-26 | POLYMER SULFONATION PROCESS | |
FI51371C (en) * | 1974-10-04 | 1976-12-10 | Rosenlew Ab Oy W | Method for decomposing a polysaccharide-containing raw material by acid hydrolysis. |
DE2545110C3 (en) * | 1975-10-08 | 1981-09-10 | Süd-Chemie AG, 8000 München | Process for the two-stage digestion of the hemicelluloses of xylan-containing natural products for the purpose of obtaining xylose |
US3990904A (en) * | 1976-05-11 | 1976-11-09 | Sud-Chemie Ag | Method for the preparation of xylose solutions |
GB1548500A (en) * | 1977-05-17 | 1979-07-18 | Inst Voor Bewaring | Process for obtaining xylose by hydrolysis of residues of annuals |
US4556430A (en) * | 1982-09-20 | 1985-12-03 | Trustees Of Dartmouth College | Process for hydrolysis of biomass |
NZ209527A (en) * | 1984-09-13 | 1988-10-28 | Jack Tama Haigh Just | Process for the continuous hydrolysis of cellulose-containing material |
-
1991
- 1991-04-08 US US07/681,299 patent/US5125977A/en not_active Expired - Fee Related
-
1992
- 1992-04-07 CA CA002065548A patent/CA2065548C/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
CA2065548C (en) | 2002-02-26 |
US5125977A (en) | 1992-06-30 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
EEER | Examination request | ||
MKLA | Lapsed |