CA1329872C - Apparatus and method of manufacturing synthetic boards - Google Patents

Apparatus and method of manufacturing synthetic boards

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Publication number
CA1329872C
CA1329872C CA000604623A CA604623A CA1329872C CA 1329872 C CA1329872 C CA 1329872C CA 000604623 A CA000604623 A CA 000604623A CA 604623 A CA604623 A CA 604623A CA 1329872 C CA1329872 C CA 1329872C
Authority
CA
Canada
Prior art keywords
binder
stream
diluent
fibers
mixing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CA000604623A
Other languages
French (fr)
Inventor
David M. Harmon
Ted J. Bauer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Weyerhaeuser NR Co
Original Assignee
Medite Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Medite Corp filed Critical Medite Corp
Application granted granted Critical
Publication of CA1329872C publication Critical patent/CA1329872C/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/41Emulsifying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50Mixing liquids with solids
    • B01F23/59Mixing systems, i.e. flow charts or diagrams
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30Injector mixers
    • B01F25/31Injector mixers in conduits or tubes through which the main component flows
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30Injector mixers
    • B01F25/31Injector mixers in conduits or tubes through which the main component flows
    • B01F25/311Injector mixers in conduits or tubes through which the main component flows for mixing more than two components; Devices specially adapted for generating foam
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30Injector mixers
    • B01F25/31Injector mixers in conduits or tubes through which the main component flows
    • B01F25/314Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced at the circumference of the conduit
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40Static mixers
    • B01F25/42Static mixers in which the mixing is affected by moving the components jointly in changing directions, e.g. in tubes provided with baffles or obstructions
    • B01F25/43Mixing tubes, e.g. wherein the material is moved in a radial or partly reversed direction
    • B01F25/431Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor
    • B01F25/4316Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor the baffles being flat pieces of material, e.g. intermeshing, fixed to the wall or fixed on a central rod
    • B01F25/43161Straight mixing tubes with baffles or obstructions that do not cause substantial pressure drop; Baffles therefor the baffles being flat pieces of material, e.g. intermeshing, fixed to the wall or fixed on a central rod composed of consecutive sections of flat pieces of material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27NMANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
    • B27N1/00Pretreatment of moulding material
    • B27N1/02Mixing the material with binding agent
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27NMANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
    • B27N9/00Arrangements for fireproofing

Abstract

APPARATUS AND METHOD OF
MANUFACTURING SYNTHETIC BOARDS
ABSTRACT OF THE INVENTION
A method and apparatus for producing a synthetic board from cellulosic or lignocellulosic fibers is disclosed wherein a standard isocyanate binder is emulsified and immediately applied to the fibers before consolidation into a finished board product. The apparatus includes an emulsification and application nozzle comprising a diluent inlet, a binder inlet, a mixing section for emulsifying the diluent and the binder, and a spray nozzle for applying the binder/diluent emulsion to the fibers.
The method includes supplying a binder stream, supplying a diluent stream, emulsifying the binder with the diluent and immediately applying the emulsion to the fibers. The method further includes flushing the binder/diluent emulsion using the diluent at the end of a binder application run to prevent curing of the emulsion and clogging of the apparatus. The present invention can be used to apply the binder/diluent emulsion to the fibers either in the blowline or downstream of the blowline, such as in the blender.

Description

l- 132~872 APPARATUS AND MET}IOD OF
MaNUFACTURI~G ~YNTHETIC BOARD~
BACKGROUND OF THE INVENTION
Field of the Invention. The present invention relates to an apparatus and method of manufacturing synthetic boards from cellulosic or lignocellulosic furnish materials using an organic binder.
Description of the Prior Art. Many synthetic board products are manufactured using a thermo~etting binder, heat and pressure to reconsolidate refined cellulosic and/or lignocellulosic furnish materials into a unitary finished board product. Examples of board manufacturing processes are shown in U.S. Patent :
No. 2,757,115 to Heritage and U.S. Patent No.
4,407,771 to Betzner et al. Basically, furnish material, such as wood, is reduced to fibers of the desired si~e by a refiner, mixed with a binder and other chemicals such as release and 6izing agents, partially dewatered, ~ormed into mats and compressed between heated platens in a hot press to ~orm a board product o~ the desired thickness and density. In many current processes, the binder is applied to a rapidly moving stream of the ~ibers as it exits the re~iner, in the so-called "blowline" o~ the process equipment.
Alternatively, the binder may be added in the blender or el~ewhere downstream o~ the re~iner.
A wide variety o~ binder systems have been utilized in the production o~ synthetic boards, including various thermosetting organic binders, such a~ i~ocyanates, polyisocyanates, urea ~ormaldehydes, phenolic~, melamines and various mixtures thereo~.
I~ocyanate and polyl~ocyanate binders have advantages over urea ~ormaldehyde binders in that board6 with - greatly improved weather re~istance can be produced.
3S Proco~sing timo can typically be substantially reduced u~lng l~ocyanate and polyisocyanate binders rather '3~6~ ' ' "
,~', ~ ' .

" , ' ' }~ A
- 2 - 1329~2 than standard phenolic binders. Although specially formulated phenolic binders can decrea~e the processing time, the cost of these specialty binders makes their use less attractive~ Additionally, urea formaldehyde binders tend to produce formaldehydes, and phenolic binders tend to produce both formaldehydes and free phenols around the press area, which can cause significant health problems.
Heretofore, successful application of isocyanate binders in fiberboard manufacture has been limited due to many factors. First, there is often difficulty in achieving adequate distribution at low dosage rates. Second, many systems require the use of an expensive release agent-containing binder or must lS utilize a caul plate system which allows external release agent application. These problems usually result in increased production costs and/or in~erior rinished board product quality.
Many Or the binder systems used today in board manu~acture include an organic isocyanate binder which ie specially mixed with a variety o~ dlluent/extender agent~ to enhance binder distribution. These admixture3 must also have a relatively long pot li~e to avoid premature curing, which can clog the binder 2S delivery system. Un~ortunately, even quite stable admixtures tend to deposit reaction products in process line~ during u~e, and especially when use is interrupted. Both problems u~ually neces~itate expensive machine downtime to unclog or replace components o~ the binder delivery ~ystem.
In ~ystems utilizing isocyanate bindere, the binder i~ typically ~ormulated into an aqueous emuloion long be~ore application to the ~urni~h.
Since the binder i~ highly reactive, the temperature durlng and a~ter emulsi~icatlon must be kept relatlvely low to avoid prereaction o~ the binder '.,' ' " . .' . . .: .: . ::
.

_ 3 _ 1 3 2 9 ~ 72 bef~re it i9 applied to the furnish materials. water-cooled addition devices, such as the nozzle described in U.S. Patent No. 4, 402, 896 to Betzner et al have been used, but require a constant supply of cooling water and are still subject to clogging.
Another problem associated with specialty binders and their mixing equipment is that if the binder is not completely removed from the binder delivery system at the end of a production run, the binder will usually cure and clog the system.
There~ore there is a need for a binder delivery system which a6sure~ that all of the binder is removed there~rom to avoid these problems.
Additionally, release agents are often added 15 to the binder system to avoid sticking of the board to ~-platens or caul plates during proces~ing. However, the~e specially ~ormulated binders are typically proprietary to a particular manu~acturer and are prohibitively expensive for large-scale ~iberboard manu~acturing operations. Accordingly, there ls a need ~or a proces~ and apparatus which can utilize ba~ic non-proprietary isocyanate and other binder compounds and release agents.
It i8 there~ore an ob~ect of the present invention to provide a method o~ producing a synthetic board ~rom cellulosic or lignocellulosic materials whereln standard, nonproprietary, inexpensive and readily available i~ocyanate, polyisocyanate and ~imilar blnder~ can be utilized, thus obviating the noed ~or expen~ive specialty chemical ~ormulations.
It i~ al50 an ob~ect o~ the present invention to provide an apparatu~ ~or producing a synthetic board wherein ~tandard binder~ and release agents can be utilized.
It i~ a further ob~ect o~ the present ~nv-ntlon to provide a method and an apparatu~ ~or - 4 ~ 13~872 forming a binder emulsion immediately upstream from the point of application to the wood fibers, thus allowing the use of isocyanates or polyisocyanates which do not form emulsions having extended stabilities or pot life.
It is also an object of the present invention to provide a method and apparatus for binder application wherein the emulsion is cooled by the diluent.
It is an object of the present invention to provide a method and apparatus for applying the binder which would avoid periodic plugging of the process equipment and the binder system.
It is also an object of the present invention to provide a method and apparatus for flushing the binder from the nozzle at the end of a production run ~o that the binder does not cure within the nozzle and clog the same.
.
SUMMARY OF T~E INVENTION ~ -The present invention is a method and apparatus for producing a synthetic board ~rom cellulosic or lignocellulosic fibers wherein a standard thermosetting binder is emulsi~ied and immediately applied to the fibers before consolidation of the fibers into a finished board product. The apparatus includes a binder emulsification and application nozzle comprising a diluent inlet, a binder inlet, a mixing section for emulsifying the diluent and the binder, and a 6pray nozzle ~or applying the binder/diluent emulsion to the fibers in a riber ~tream upstream o~ the forming mat in the board ~orming proces6. The method includes supplying a binder stream, ~upplying a diluent stream, merging the two 6treams, emulsifying the binder with the diluent and immediately thereafter applying the .`
, . ~

~ 329~72 emulsion to the fiber stream. The method further includes flushing the nozzle with the diluent stream at the end of a production run to remove the binder from the nozzle to prevent curing of the binder emulsion and clogging of the nozzle. In the apparatus of the present invention, the nozzle can be used to apply the emulsified binder to the fiber stream either in the refiner, the blowline or down-stream of the blowline, such as in the blender, of the board forming apparatus.
10 . ', BRIEF DESCRIPTION OF THE DRAWINGS
FIG. l is a schematic diagram showing the process and apparatus in accordance with the present invention.
FIG. 2 is a side view of a nozzle in accordance with the present invention mounted on a blowline of a fiberboard manufacturing process.
FIG. 3 is a schematic view of the nozzle in accordance with the present invention.
FIG. 4, which appears on the same she~t as FIG.
l, illustrates a flow diagram of the manner in which a binder and a diluent can be combined and added to a fiber stream according to the invention.

DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENT
The present invention is intended for use in the production of reconstituted products made from cellulosic or lignocellulosic materials, and in particular, the production of fiberboard from wood fibers. As shown in FIG. l, pieces of wood, such as chips, are fed into a plug feeder 10 for delivery to a digester 12, where they are sub~ected to steam and high pressure to so~ten the chips and break down the lignin therein. The cooked chips are tran~ferred to a refiner 14 where they are separated into their constituent fibers, such as between uni- or bi-directional rotating discs.
The hot and wet ~iber5 exit refiner 14 with steam in a rapidly moving continuous stream which is . '.

,; ;

13~9872 transported through a so-called ~'blowline" 16, where the binder and other desired compounds, such as release and sizing agents, are typically added. The binder is preferably a material selected from the 5 group consisting of monomeric isocyanates, oligomeric --isocyanates, and mixture~ thereof having a functionality of at least 2. In addition, other conventional thermosetting binders may be used. -Aqueous emulsions of the binder and other ~ ;
additives are well-suited to blowline injection for several reasons. First, a large portion of the heat energy available in the blowline is absorbed in -raising the temperature of the applied emulsions since~ ;~
the specific heat of water is higher than many of the other substance~ being added. Second, the water-to-water solvent compatibility between the wood fibers `~
and the additive emulsion is excellent and helps assure good flow and distribution of the binder.
Third, deposits o~ the additive emulsion on the wall oY the blowline are minimized due to the presence oY acontinuous Yilm o~ water condensate, with which the additive emulsions are also compatible. Fourth, the great turbulence within the blowline results in a ~couring action which tends to keep the blowline wall clean, providing those adhering substances are also water compatible. Laetly, the residence time in the blowline iB 80 short that most chemical reactions, ;;~
~uch as curing o~ the binder, have in~u~ficient time and energy to move very Yar toward reaction products.
In the preYerred embodlment oY the present invention, a binder emul~ion and appllcation nozzle a~embly 18 ln accordance with the present invention i8 connec~ed to blowline 16 Yor emulsifying the binder wlth a diluent and applylng the resulting emulsion to the ~iber~ a9 they pa~ through blowline 16. In the prererred embodlment, conventional nozzles 20 and 22 .,:

132~872 are also plumbed to blowline 16 for applying release and sizing agents to the fibers. Alternatively, the binder, release agent and sizing agents may be added at other locations in the process, as will be described bel~w.
Upon entering blowline 16, the steam and the fibers undergo a rapid drop in pressure and temperature, but travel therethrough in less than about 1 second. The velocity of the fibers through a typical blowline has been reported to be approximately 325 feet per second. There is extreme turbulence in blowline 16, which provides excellent mixing of additives, such as the binder, with the fibers.
After exiting blowline 16, the fibers enter a dryer 24 where they are partially dewatered. A first cyclone 26 and an air lock 28 are provided to separate the fiber from the dryer airstream. The fibers next paes to a blender 30 wherein the binder, sizing, release agents or other desired materials can be mixed with the ~ibers, i~ desired. If all desired compounds have already been added, the ~ibers can be directed through a bypass chute 32 and go directly to a second cy¢lone 3g with an air lock 36 and then into a ~iber etorage bin 38. Fiber storage bin 38 provides ribers to one or more rorming head apparatuses 40 which are used to dispense a ~orming mat o~ ~ibers 41 onto a ~orming belt 42. Forming mat 41 is deaerated by one or more prepreeeee 44 and then compressed to the ~inal preseed thickne~ by a hot pr~ss 46 wherein the binder 1~ cured to rorm the desired board product.
In general, the binder can be added to the riber~ in any suitable location in the board rorming apparatus upetream Or ~orming mat 41. Alternatlve locatione where the blnder can be added to the riber~
are designated by daehed arrow~ 17a-d in FIG. 1. For example, the binder may be added using the nozzle - 8 _ 1~29~72 : ~

assembly of the present invention in any of the :
following locations: refiner 14; blender 30; bypass chute 32 or forming head apparatuses 40. Similarly, the sizing and release agents can be added, separately 5 or together, in the various locations in the board: ~ :
forming apparatus, including plug feeder 10, digester 12, refiner 14, blowline 16, blender 30 or bypass chute 32.
Referring to FIGS. 2 and 3, nozzle assembly 18 10 comprises a diluent inlet 52, a binder inlet 54, a mix.-section 56 for emulsifying diluent and binder and a spray nozzle 58 adapted for connection to a blowline.:
16 for spraying the emulsion on the fibers. A stream of water or other diluent is introduced through .
15 diluent inlet 52, and a stream of a binder, which can: :
be isocyanate, polyisocyanate or other suitable thermosetting binder, is introduced through binder ~:
inlet 54.
Diluent inlet 52 includes a coupling 62, such . .
as a quick disconnect coupling shown, ~or connection to a diluent supply line 64 with an appropriate coupling 66 through which water or other suitable diluent is delivered to nozzle assembly 18. A
pressure relie~ check valve 68 ~or diluent inlet 52 is operated by a control spring 70 and is threadedly connected to coupling 62. Diluent check valve 68 prevents back~low from mix section 56 into diluent . :::
supply line 64. In addition, diluent check valve 68 will only open to allow diluent into mix section 56 30 when the pre~sure o~ the water stream is above a ::
certaln mlnimum pres~ure, ~or example, 15 psi. This a~uree that there will be no admixing of water and binder until the water stream has achieved proper operatlng pressure, ~uch as by the use o~ an 35 Approprlat2 metering pump ~not shown). It also ...
as~ures that the ~low o~ d~luent into nozzle assembly .

'' "

: ,.. ..
, ~ .,. :

~ 32~872 g ~ .

18 will stop immediately upon stopping the flow of the diluent stream or upon a drop in the pressure of the stream. Suitable check valves are available from the NuPro Company of Willoughby, Ohio.
Although alternative diluents, such as propylene carbonate or furfural, can be used under various conditions, water has long been used to reduce the viscosity of binders and thus improve distribution. The water also serves as a thermal buffer for the binder. This is particularly significant for those applications utilizing blowline addition of isocyanates. Since there is a constant ~low of relatively cool (less than ambient temperature) diluent water through nozzle assembly 18, the temperature to which the binder is subjected during emulsification is also less than ambient, which prevents precuring. No additional cooling of the emulsion, such as provided by a cooling water jacket, i8 required.
Binder inlet 54 similarly includes a coupling 72 ~or connection to a binder supply line 74 with a coupling 76 through which binder is delivered to nozzle assembly 18. In the pre~erred embodiment, the binder i5 standard technical grade isocyanate or polyisocyanate. A pressure relie~ check valve 78 ~or binder lnlet 54 includes a control spring 80 and is threadedly connected to coupling 72. Binder check valve 78 operates a~ above to prevent back~low ~rom mlx section 56 into binder supply line 74. Binder chec~ valve 78 also prevents the admixing o~ water and binder be~ore the binder stream has achieved its proper operatlng pressure, or i~ the ~low o~ the binder ~tream has been stopped or lf the pressure of th- binder stream drop~ below a proper operating pres~ure.
Additional compounds, such as release agents, ;-- 132~87~

sizing agents, etc., may be applied to the fibers, if desired. Referring to FIG. 4, release agents and `-sizing a~ents may be added, separately or together, to ~ -diluent stream 81a, binder stream 81b, com~ined binder/diluent stream 81c or directly to fiber stream 81d, as shown by dashed lines 82a - 82d, respectively.
If the additional compounds are to be added to combined binder/diluent stream 81c, a third inlet 83 (shown by dashed lines in FIG. 2) can be plumbed to m.ix section 56 of nozzle assembly 18 for introducing such compounds into mix section 56. In this way, the additional compound will be merged with the binder/diluent immediately before application to the fibers.
Mix section 56 includes an intersecting tee 84 which is threadedly attached to the outlets of diluent check valve 68 and binder check valve 78 for receiving the binder stream and the diluent stream. Tee 84 is also threadedly connected to an in-line mix section 85 e~uipped with a plurality of interior baffles 86 which cause mixing and emulsion o~ the binder with the diluent. The exact number and configuration of ba~les 86 has not been ~ound to be critical, as long as su~icient mixing results. A plastic baf~led-style motionless mixer insert sized ~or insertion into in~
line mix section 85 and sold by TAH Industries of ~ ;
Imalyston, New Jer~ey under the name Kinetic Mixer*has been ~ound to give good results. ;
Spray nozzle 58 is threadedly attached to in-llne mix section 85 ~or applying the diluent-binder emulsion to the ~ibers passing through blowline 16.
Spray nozzle 58 is provided with external threads 90 ~or attachment to mating internal threads 92 in wall 94 o~ blowline 16. Spray nozzle 58 is mounted so that only a small tip portion 96 o~ the nozzle 90 extends into blowllne 16 and is subjected to the abrasive - ~Trade-mark ,,,' ' '1 ~, '~"' ~, ...................................................................... .

atmosphere therein. Due to the abrasive atmosphere of blowline 16 and to avoid any possible interaction with the emulsion, it has been determined that spray nozzle 58 should be constructed out of stainless steel or other suitable material.
It has also been determined that a spray nozzle obtained from Spraying Systems Company of -Wheaton, Illinois and sold under the trademark FULW ET
gives good results. This nozzle tip includes an 10 integral interior spiral vane mixer which produces a -full cone spray pattern for good distribution of the emulsion on the fibers. It has also been determined that a nozzle I.D. of 0.245 inches i6 preferred to maintain proper backpressure in nozzle assembly 18.
Nozzle assembly 18 is typically operated at an emulsion ~low rate of approximately 5 gallons per minute and a pressure of between 80 and 125 psi, although some applications may require other application rates and parameter~.
In the pre~erred embodiment, blowline 16 has an interior diameter of about 6 inches. Thus, the di~tance between the point of emulsi~ication o~ the binder and the point o~ application to the ~ibers in blowline 16 is very small, approximately 4 inches.
This relatively short distance help~ assure that the binder emulsion does not cure be~ore application to the ~ibers.
In accordance with the pre~ent ~nvention, a method of and means ~or ~lu~hing binder and emulsion out o$ nozzle assembly 18 are al80 provided. This rlu~hing is necessary to avoid leaving the emulsion in mix ~ection 56 or epray nozzle 58 where it could quiokly cure and plug nozzle as~embly 18. To ~lush nozzl- a~sembly 18 at the end of a production run, the blndor pump ~hould be turned orf to ~top the ~low o~
blnder. Thl3 causes binder check valve 78 to close.
.... .

' ~
- 12 _ 1 32 9~ 72 - -The water stream is allowed to continue to flow for a ~ -few seconds (3-5 seconds) to flush out any residual emulsion. Preferably, the binder stream should be - -shut off before fiber stream flow past spray nozzle 58 has ended to avoid buildup of binder in blowline 16.
Application of the aqueous emulsions of -standard isocyanate and polyisocyanate through nozzle assembly 18 into blowline 16 results in a practical and economical means of producing a superior 10 fiberboard product. The ready availability of the -binders are of great significance to a commercial fiberboard production facility. --Although preferred embodiments of the present invention have been shown, it is obvious than many modifications and variations of the present invention are possible in light of the above teachings. It i8 therefore to be understood that the present invention may be practiced otherwise than as specifically described.

. ~ .

'',"' . .: ' ' ' .
... ~ . ' .., i' ' ' "''',' '."

'" , '

Claims (46)

1. In the production of synthetic boards from cellulosic fibers and a highly reactive multi-part binder system including a binder and a binder diluent, an appar-atus adapted for mixing a binder stream and a diluent stream to form a product stream and applying the resulting product stream to the fibers, the apparatus comprising:
conduit means for transporting a stream of fibers:
binder inlet means adjacent the conduit means for receiving a first stream containing a binder;
diluent inlet means adjacent the conduit means for receiving a second stream containing a diluent;
mixing means including a mixing means inlet fluidly connected to and adjacent the binder inlet means and the diluent inlet means for mixing the first stream and the second stream to produce a third stream containing a product comprising a mixture of the binder and the diluent;
and continuously open mixing means outlet positioned proximate the mixing means and proximate the conduit means and fluidly connected to the mixing means and opening into the interior of the conduit means for immediately applying the third stream to the stream of fibers.
2. In the production of synthetic boards from cellulosic fibers, an apparatus adapted for mixing a binder stream and a diluent stream and applying a product stream to the fibers, the apparatus comprising:
binder inlet means for receiving a first stream containing a binder;
diluent inlet means for receiving a second stream containing a diluent;

mixing means fluidly connected to the binder inlet means and the diluent inlet means for mixing the first stream and the second stream to produce a third stream containing a product comprising the binder and the diluent;
outlet means positioned proximate the mixing means and fluidly connected to the mixing means for immedi-ately applying the third stream to the fibers; and flush means for flushing the mixing means with the second stream after flow of the first stream is stopped.
3. The apparatus of claim 2 wherein the binder inlet means comprises binder control valve means for automatically stopping the flow of the first stream upon a decrease in application pressure thereof.
4. The apparatus of claim 2 wherein the diluent inlet means comprises diluent control valve means for automatically stopping the flow of the second stream upon a decrease in application pressure thereof.
5. The apparatus of claim 2 wherein the mixing means emulsifies the binder and the diluent in the third stream.
6. The apparatus of claim 2 wherein the mixing moans comprises a plurality of baffles.
7. The apparatus of claim 2 wherein the outlet means comprises a spray nozzle.
8. The apparatus of claim 7 wherein the flush means comprises means for first stopping flow of the first stream and then stopping flow of the second stream.
9. The apparatus of claim 7 and further comprising:
supplemental inlet means fluidly connected to the mixing means for receiving a fourth stream, wherein the fourth stream is mixed with the first stream and the second stream in forming the third stream.
10. An apparatus for producing synthetic boards from a cellulosic material, and a highly reactive multi-part binder system including a binder and a diluent com-prising:
refining means for extracting fibers from a cellulosic material;
conduit means connected to the refining means for conveying the fibers along a fiber flow path;
binder application means for mixing a binder and a diluent to form a binder/diluent mixture and immediately mixing the binder/diluent mixture with the fibers in the fiber flow path;
said binder application means including a static in-line mixing section having a continuously open outlet end connected to said conduit means and opening into the interior of the conduit means and a continuously open inlet end, binder inlet means connected to said inlet end, and diluent inlet means connected to said inlet end, such that a binder stream and a diluent stream merge at the inlet end, mix in the mixing section and merge with the fiber stream at the outlet end;
dryer means for partially dewatering the fiber/
binder mixtures;
forming means for creating a mat of the dewatered fiber/binder mixtures; and heated pressing means for compressing the fibers and curing the binder in the mat for forming a consolidated board product.
11. An apparatus for producing synthetic boards from a cellulosic material, comprising:
refining means for extracting fibers from a cellulosic material;
conduit means connected to the refining means for conveying the fibers along a fiber flow path;
binder application means for mixing a binder and a diluent to form a binder/diluent mixture and immediately mixing the binder/diluent mixture with the fibers in the fiber flow path;
dryer means for partially dewatering the fiber/
binder mixture;
forming means for creating a mat of the dewatered fiber/binder mixture;
heated pressing means for compressing the fibers and curing the binder and the mat for forming a consoli-dated board product; and flush means for flushing the binder/diluent mixture from the binder application means at the end of a production run wherein the flush means comprises means for stopping the flow of binder from the first stream and then stopping the flow of diluent from the second stream.
12. The apparatus of claim 11 wherein the binder application means comprises:
binder inlet means for receiving a first stream containing a binder;
diluent inlet means for receiving a second stream containing a diluent;
mixing means fluidly connected to the binder inlet means and the diluent inlet means for mixing the binder and the diluent to produce a mixed product stream thereof; and outlet means positioned proximate the mixing means and fluidly connected to the mixing means for imme-diately applying the emulsion to the fibers in the fiber flow path.
13. The apparatus of claim 12 wherein the binder inlet means comprises binder control valve means for automatically stopping the flow of the binder stream upon a decrease in application pressure thereof.
14. The apparatus of claim 12 wherein the diluent inlet means comprises diluent control valve means for automatically stopping the flow of the diluent stream upon a decrease in application pressure thereof.
15. The apparatus of claim 12 wherein the mixing means comprises an in-line mixer.
16. The apparatus of claim 12 wherein the mixing means comprises a plurality of baffles.
17. The apparatus of claim 12 wherein the outlet means comprises a spray nozzle.
18. The apparatus of claim 11 wherein the binder/diluent mixture is mixed with the fibers upstream of the forming means.
19. The apparatus of claim 11 wherein the conduit means comprises a blender means positioned along the fiber flow path for receiving and mixing the fibers, wherein the binder application means is plumbed to the blender means for applying binder to the fibers therein.
20. The apparatus of claim 11 wherein the conduit means comprises a blowline means wherein the binder application means is plumbed to the blowline means for applying binder to the fibers therein.
21. In the manufacture of synthetic boards from cellulosic fibers, a method of blending a binder with the fibers, the method comprising:
conveying cellulosic fibers in a first stream;
conveying a binder in a second stream;
conveying a diluent in a third stream;
merging the second stream and the third stream to produce a fourth stream;
immediately thereafter merging the fourth stream and the first stream to apply the binder and the diluent to the fibers; and flushing the fourth stream at the end of a production run using the third stream after flow of the second stream is stopped.
22. The method of claim 21 and further compris-ing the step of:
mixing the second stream and the third stream to produce a binder/diluent mixture in the fourth stream.
23. The method of claim 22 and further compris-ing the step of:
emulsifying the binder/diluent mixture immediate-ly before merging the fourth stream with the first stream.
24. The method of claim 23 wherein the binder/
diluent mixture in the fourth stream is emulsified by forcing said stream through a plurality of baffles.
25. The method of claim 21 and further compris-ing the step of:
conveying a release agent in a fifth stream;
merging the fifth stream with the second and third streams immediately before merging the fourth stream and the first stream.
26. The method of claim 21 and further compris-ing the step of:
conveying a sizing agent in a fifth stream;
merging the fifth stream with the second and third streams immediately before merging the fourth stream and the first stream.
27. The method of claim 21 wherein the binder comprises a thermosetting binder.
28. The method of claim 21 wherein the binder comprises a material selected from the group consisting of monomeric isocyanates, oligomeric isocyanates and mixtures thereof having a functionality of at least 2.
29. The method of claim 21 wherein the diluent comprises water.
30. The method of claim 21 wherein the binder comprises a thermosetting binder and the diluent comprises water.
31. A method of producing synthetic boards from a cellulosic material, comprising the steps of:
extracting hot and wet fibers from a cellulosic material;
transporting the hot and wet fibers in a first streams;
transporting separate second and third streams comprising a binder and a diluent, respectively, generally toward the first stream;
merging the second and third streams to form a fourth stream;
emulsifying the binder and the diluent in the fourth stream;

immediately after emulsifying, applying the binder/diluent emulsion in the fourth stream to the hot and wet fibers in the first stream:
partially dewatering the hot and wet fibers;
forming the partially dewatered fibers into a mat;
compressing the mat in a heated press to cure the binder to form a consolidated board product; and flushing the binder/diluent emulsion using the third stream after flow of the second stream is stopped.
32. The method of claim 31 wherein the emulsify-ing step comprises:
conveying the merged binder and diluent in the fourth stream around stationary baffles in the fourth stream to intermix and emulsify the binder and the diluent.
33. The method of claim 31 wherein the binder comprises a thermosetting binder.
34. The method of claim 31 wherein the binder comprises a material selected from the group consisting of monomeric isocyanates, oligomeric isocyanates and mixtures thereof having a functionality of at least 2.
35. The method of claim 31 wherein the diluent comprises water.
36. The method of claim 31 wherein the binder comprises a thermosetting binder and the diluent comprises water.
37. The method of claim 31 wherein the second stream further comprises a sizing agent.
38. The method of claim 31 wherein the second stream further comprises a release agent.
39. The method of claim 31 wherein the third stream further comprises a sizing agent.
40. The method of claim 31 wherein the third stream further comprises a release agent.
41. The apparatus of claim 1 including a binder control valve at the binder inlet means and a diluent control valve at the diluent inlet means, said valves being fluid pressure operated to open by the respective down-stream pressures of said first and second streams of binder and diluent flowing in directions toward said mixing means and thereby allow the first and second streams to flow through the inlet means into said mixing means, said binder and diluent valves being closable, respectively, in res-ponse to a reduction in the downstream pressures applied by said first and second streams.
42. The apparatus of claim 1 wherein said mixing means comprises an in-line static mixer.
43. The apparatus of claim 41 including means for flushing said mixing means comprising means for main-taining downstream pressure on said diluent control valve to maintain the diluent control valve open while reducing the downstream pressure on said binder control valve to close the binder valve.
44. The apparatus of claim 2 wherein said flush means includes a fluid pressure operated binder control valve at the binder inlet means and a fluid pressure operated diluent control valve at the diluent inlet means, said valves being independently operable to open and close upon variations in the applied pressures of said first and second streams.
45. The apparatus of claim 10 including a first check valve at the binder inlet means and a second check valve at the diluent inlet means, the first and second check valves being independently operable under the influ-ence of the binder and diluent streams to permit binder and diluent flow into the mixing section but prevent backflow thereof from the mixing section.
46. The apparatus of claim 45 including flush means for flushing the mixing section, said flush means including the check valves.
CA000604623A 1989-03-20 1989-06-30 Apparatus and method of manufacturing synthetic boards Expired - Lifetime CA1329872C (en)

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IE900910L (en) 1990-09-20
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AU4787890A (en) 1990-09-20
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NZ232036A (en) 1992-07-28
IE62452B1 (en) 1995-02-08
US5093058A (en) 1992-03-03

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